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1. 发明申请

US20080004394A1 Method of providing repellency 审中-公开
公开(公告)号：US20080004394A1
公开(公告)日：2008-01-03
申请号：US11479904
申请日：2006-06-30
申请人： Stefan Reinartz , Peter Michael Murphy , Andrew Joseph McCall , Gerald Oronde Brown
发明人： Stefan Reinartz , Peter Michael Murphy , Andrew Joseph McCall , Gerald Oronde Brown
IPC分类号： C09D5/02
CPC分类号： C08G73/02 , C08F220/18 , C08F220/22 , C08G61/124 , C08G61/125 , C09D133/16 , D06M15/263 , D06M15/277 , D06M15/285 , D06M15/576
摘要： A method of providing water repellency, alcohol repellency, oil repellency, and soil resistance to substrates comprising contacting said substrate with a composition comprising a copolymer having repeating units of Formula 1 in any sequence: [Rf(CH2)kOC(O)NH(CH2)kOC(O)C(T)CH2]m—[Wq]p—Formula 1 wherein Rf is a straight or branched perfluoroalkyl group having from about 2 to about 8 carbon atoms, or a mixture thereof, which is optionally interrupted by at least one oxygen atom, each k is independently a positive integer from 1 to about 6, T is hydrogen or methyl, m is a positive integer, q is zero or a positive integer, p is zero or a positive integer, and W is or or —[R1—X—Y—C(O)—CZ-CH2]—, wherein X is an organic divalent linking group having from about 1 to about 20 carbon atoms, optionally containing a triazole, oxygen, nitrogen, or sulfur, or a combination thereof, Y is O or N(R) wherein R is H or C1 to C20 alkyl, Z is H, a straight or branched alkyl group having from about 1 to about 4 carbon atoms, or halide, Rx is C(O)O(R1), C(O)N(R2)2, OC(O)(R1), SO2(R1), C6(R3)gH(5-g), O(R1), halide, or R1; each R1 is independently H, CnH2n+1, CnH2n—CH(O)CH2, [CH2CH2O]iR4, [CnC2n]N(R4)2 or [CnH2n]CnF2n+1, n is 1 to about 40, R4 is H or CsH2s+1, s=0 to about 40, i=1 to about 200, each R2 is independently H, or CtH2t+1 wherein t is 1 to 20, each R3 is independently R4, COOR1, halogen, N(R1)2, OR1, SO2NHR1, CH═CH2, or SO3M, g is 1 to 5, and M is H, alkali metal salt, alkaline earth metal salt, or ammonium.

2. 发明申请

US20090148653A1 FLUOROPOLYMER EMULSIONS 审中-公开
标题翻译：氟聚乳酸
公开(公告)号：US20090148653A1
公开(公告)日：2009-06-11
申请号：US12237446
申请日：2008-09-25
申请人： Gerald Oronde Brown , Peter Michael Murphy , Ying Wang
发明人： Gerald Oronde Brown , Peter Michael Murphy , Ying Wang
IPC分类号： B32B5/02 , C08L67/06 , C08L81/00 , C08L79/02 , D03D27/00 , B32B27/10 , C08L77/00 , C08L63/00 , C08L83/00
CPC分类号： C08F220/24 , C08F2/44 , Y10T428/23986 , Y10T428/249921 , Y10T428/3154 , Y10T428/31993 , Y10T442/20 , Y10T442/2172
摘要： A fluoropolymer composition comprising monomers copolymerized in the following percentages by weight: (a) from about 20% to about 95% of a fluoroalkyl monomer, or mixture of monomers, of formula (I) Rf1-L-X—C(O)—C(R)═CH2 (I) whereinRf1 is a monovalent, partially or fully fluorinated, linear or branched, alkyl radical having from about 2 to about 100 carbon atoms; optionally interrupted by 1 to about 50 oxygen atoms; wherein the ratio of carbon atoms to oxygen atoms is at least about 2:1 and no oxygen atoms are bonded to each other;L is a linear or branched divalent linking group having 1 to about 20 carbon atoms; optionally interrupted by 1 to about 4 hetero-radicals selected from the group consisting or —O—, —NR1—, —S—, —SO—, —SO2—, —N(R1)C(O)—; wherein R1 is H or C1 to C6 alkyl;X is —O—, —NR1—, or —S—;R is hydrogen, Cl, F or CH3; (b) from about 5% to about 80% of at least one of: (i) an alkyl(meth)acrylate monomer having a linear, branched or cyclic alkyl group of from about 6 to about 18 carbons; or (ii) one or more ionizable water solvatable monomers; and (c) from about 0.05% to about 2% polymerizable nanoparticles.
摘要翻译：一种含氟聚合物组合物，其包含按以下重量百分比共聚的单体：（a）约20％至约95％的式（I）的氟代烷基单体或单体混合物<？在线公式描述=“In 线型式“end =”lead“→Rf1-LXC（O）-C（R）-CH2（I）<βin-line-formula description =”In-line Formulas“end =”tail“？>其中 Rf1是具有约2至约100个碳原子的单价，部分或完全氟化的直链或支链烷基; 任选地被1至约50个氧原子中断; 其中碳原子与氧原子的比例为至少约2:1且没有氧原子彼此键合; L是具有1至约20个碳原子的直链或支链二价连接基团; 任选地被1至大约4个选自以下的杂原子中断：-NR 1 - ， - S - ， - SO - ， - SO 2 - ， - N（R 1）C（O） - ; 其中R1是H或C1-C6烷基; X是-O-，-NR1-或-S-; R是氢，Cl，F或CH 3; （b）约5％至约80％的至少一种：（i）具有约6至约18个碳原子的直链，支链或环状烷基的（甲基）丙烯酸烷基酯单体; 或（ii）一种或多种可离子化的水可溶性单体; 和（c）约0.05％至约2％的可聚合纳米颗粒。

3. 发明申请

US20090149096A1 FLUOROPOLYMER EMULSIONS 有权
标题翻译：氟聚乳酸
公开(公告)号：US20090149096A1
公开(公告)日：2009-06-11
申请号：US12268470
申请日：2008-11-11
申请人： Gerald Oronde Brown , Peter Michael Murphy , Ying Wang
发明人： Gerald Oronde Brown , Peter Michael Murphy , Ying Wang
IPC分类号： B32B27/12 , B32B27/04 , B32B27/00 , C08F220/24
CPC分类号： C08F220/24 , C08F2/44 , Y10T428/23986 , Y10T428/249921 , Y10T428/3154 , Y10T428/31993 , Y10T442/20 , Y10T442/2172
摘要： A fluoropolymer composition comprising monomers copolymerized in the following percentages by weight: (a) from about 20% to about 95% of a fluoroalkyl monomer, or mixture of monomers, (b) from about 5% to about 80% of at least one of: (i) an alkyl (meth)acrylate monomer having a linear, branched or cyclic alkyl group of from about 6 to about 18 carbons; or (ii) one or more ionizable water solvatable monomers; and (c) from about 0.05% to about 2% non-fluorinated polymerizable nanoparticles.
摘要翻译：一种含氟聚合物组合物，其包含按以下重量百分比共聚的单体：（a）约20％至约95％的氟烷基单体或单体混合物，（b）约5％至约80％：（i）具有约6至约18个碳原子的直链，支链或环状烷基的（甲基）丙烯酸烷基酯单体; 或（ii）一种或多种可离子化的水可溶性单体; 和（c）约0.05％至约2％的非氟化可聚合纳米颗粒。

4. 发明授权

US08314037B2 Fluoropolymer emulsions 有权
标题翻译：含氟聚合物乳液
公开(公告)号：US08314037B2
公开(公告)日：2012-11-20
申请号：US12268470
申请日：2008-11-11
申请人： Gerald Oronde Brown , Peter Michael Murphy , Ying Wang
发明人： Gerald Oronde Brown , Peter Michael Murphy , Ying Wang
IPC分类号： B32B5/02 , B32B27/00 , C08F18/20 , A01K1/015
CPC分类号： C08F220/24 , C08F2/44 , Y10T428/23986 , Y10T428/249921 , Y10T428/3154 , Y10T428/31993 , Y10T442/20 , Y10T442/2172
摘要： A fluoropolymer composition comprising monomers copolymerized in the following percentages by weight: (a) from about 20% to about 95% of a fluoroalkyl monomer, or mixture of monomers, (b) from about 5% to about 80% of at least one of: (i) an alkyl (meth)acrylate monomer having a linear, branched or cyclic alkyl group of from about 6 to about 18 carbons; or (ii) one or more ionizable water solvatable monomers; and (c) from about 0.05% to about 2% non-fluorinated polymerizable nanoparticles.
摘要翻译：一种含氟聚合物组合物，其包含按以下重量百分比共聚的单体：（a）约20％至约95％的氟烷基单体或单体混合物，（b）约5％至约80％：（i）具有约6至约18个碳原子的直链，支链或环状烷基的（甲基）丙烯酸烷基酯单体; 或（ii）一种或多种可离子化的水可溶性单体; 和（c）约0.05％至约2％的非氟化可聚合纳米颗粒。

5. 发明申请

US20080146758A1 Low temperature cure repellents 审中-公开
标题翻译：低温固化驱避剂
公开(公告)号：US20080146758A1
公开(公告)日：2008-06-19
申请号：US11638916
申请日：2006-12-14
申请人： Peter Michael Murphy , Richard H. Goldbaum , Andrew Joseph McCall , Carolyn Sue Yatsko
发明人： Peter Michael Murphy , Richard H. Goldbaum , Andrew Joseph McCall , Carolyn Sue Yatsko
IPC分类号： C08F220/22 , B32B27/04 , B05D3/00
CPC分类号： D06M15/277 , D06M15/233 , D06M15/248 , D06M15/263 , D06M15/333 , D06M2200/12 , Y10T442/2164
摘要： An improved method for treating fibrous substrates with a copolymer containing a fluorinated acrylate or fluorinated methacrylate to provide water repellency and alcohol repellency wherein the improvement comprises contacting the substrate with a composition of particular fluorinated copolymers followed by drying or curing without heating.
摘要翻译：一种利用含有氟化丙烯酸酯或氟化甲基丙烯酸酯的共聚物处理纤维基材以提供拒水性和拒酒性的改进方法，其中改进包括使基材与特定氟化共聚物的组合物接触，然后在不加热的情况下进行干燥或固化。

6. 发明申请

US20090117795A1 LOW TEMPERATURE CURE REPELLENTS 审中-公开
标题翻译：低温固化剂
公开(公告)号：US20090117795A1
公开(公告)日：2009-05-07
申请号：US12327200
申请日：2008-12-03
申请人： Peter Michael Murphy , Richard H. Goldbaum , Andrew Joseph McCall , Carolyn Sue Yatsko
发明人： Peter Michael Murphy , Richard H. Goldbaum , Andrew Joseph McCall , Carolyn Sue Yatsko
IPC分类号： B32B27/12 , B05D3/00
CPC分类号： D06M15/233 , D06M15/248 , D06M15/263 , D06M15/277 , D06M15/333 , D06M2200/12 , Y10T442/2164
摘要： An improved method for treating fibrous substrates with a copolymer containing a fluorinated acrylate or fluorinated methacrylate to provide water repellency and alcohol repellency wherein the improvement comprises contacting the substrate with a composition of particular fluorinated copolymers followed by drying at ambient temperature or curing at ambient temperature.
摘要翻译：一种用含氟化丙烯酸酯或氟化甲基丙烯酸酯的共聚物处理纤维基材的改进方法，以提供拒水性和醇排斥性，其中改进包括使基材与特定氟化共聚物的组合物接触，然后在环境温度下干燥或在环境温度下固化。

7. 发明申请

US20090110840A1 Hydrophillic fluorinated soil resist copolymers 审中-公开
标题翻译：亲水性氟化土壤抗菌共聚物
公开(公告)号：US20090110840A1
公开(公告)日：2009-04-30
申请号：US11977188
申请日：2007-10-24
申请人： Peter Michael Murphy , Stefan Reinartz
发明人： Peter Michael Murphy , Stefan Reinartz
IPC分类号： B32B27/28 , B05D1/02 , C08G69/26 , B05D1/18
CPC分类号： C08F214/186 , C08F214/18 , C08F220/06 , D06M15/263 , D06M15/277 , D06M15/576
摘要： A copolymer of Formula I —[Rf-Q-OC(O)NHC(CH3)2C6H4C(CH3)CH2—]x−[CH2C(R)(COOH)—]y— (I) whereinRf is a straight or branched perfluoroalkyl group having from about 2 to about 8 carbon atoms, or a mixture thereof, which is optionally interrupted by at least one oxygen atom,Q is alkylene of 1 to about 15 carbon atoms, hydroxyalkylene of from about 2 to about 15 carbon atoms, —O(CnH2n)—, —(CH2CF2)m(CH2)n—, —OCHFCF2(CH2)n—, —CONR1(CnH2n)—, —(CnH2n)OCONR1(CnH2n)—, (—CONR1CH2)2CH—, —SO2N(R1)(CnH2n)—, or —(CnH2n)SO2N(R1)(CnH2n)—,each R1 is independently H or alkyl of 1 to about 4 carbon atoms,each n is independently 1 to about 15,each m is independently 1 to about 4, andR is H or CH3,x is a positive integer, andy is a positive integer,and a method of its use for imparting soil resistance to substrates while imparting minimal water repellency is disclosed.
摘要翻译：式I的共聚物<？in-line-formula description =“In-line Formulas”end =“lead”→[Rf-Q-OC（O）NHC（CH3）2C6H4C（CH3）CH2-] x- [CH2C（R）（COOH） - ] y-（I）<？在线公式描述=“在线公式”end =“tail”？>其中Rf是直链或支链全氟烷基，至约8个碳原子，或其混合物，其任选被至少一个氧原子间隔，Q为1至约15个碳原子的亚烷基，约2至约15个碳原子的羟基亚烷基，-O（C n H 2n） - ， - （CH 2 CF 2）m（CH 2）n - ，-OCHFCF 2（CH 2）n - ， - CONR 1（C n H 2n） - ， - （C n H 2n）OCONR 1（C n H 2n） - ，（-CONR1CH 2）2 CH-， - SO 2 N（R 1） C n H 2n） - 或 - （C n H 2n）SO 2 N（R 1）（C n H 2n） - ，每个R 1独立地为H或1至约4个碳原子的烷基，每个n独立地为1至约15，m各自独立地为1至约4 并且R为H或CH 3，x为正整数，y为正整数，并且公开了用于赋予基材耐污性同时赋予极小斥水性的方法。

8. 发明授权

US07816005B2 Copolymers for stain resistance 失效
公开(公告)号：US07816005B2
公开(公告)日：2010-10-19
申请号：US12774979
申请日：2010-05-06
申请人： Timothy Edward Hopkins , Stephen Ernest Jacobson , Melea Rena Langley , Peter Michael Murphy
发明人： Timothy Edward Hopkins , Stephen Ernest Jacobson , Melea Rena Langley , Peter Michael Murphy
IPC分类号： B32B27/08 , B05D3/00
CPC分类号： D06M15/263 , C08F8/44 , C09D135/00 , D06M15/227 , D06M15/233 , D06M15/285 , D06M15/29 , D06M15/295 , D06M15/3562 , D06M2200/01 , Y10T428/23986 , Y10T428/2933 , Y10T428/2938 , Y10T428/2967 , Y10T428/3175 , Y10T428/31797 , Y10T428/31855 , Y10T428/3188 , Y10T428/31895 , Y10T428/31909 , Y10T428/31928 , Y10T442/2279 , C08F8/32 , C08F212/08 , C08F222/06 , C08F210/14
摘要： A method for imparting resistance to staining to a substrate comprising contacting the substrate with a copolymer comprising the monomers of Formula wherein D is at least one vinyl monomer selected from the group consisting of aryl olefin, alpha olefin and diene, each M is independently H, Ca, Mg, Al, Na, or K, each R1 is independently H, C1-C6 alkyl, or C1-C6 hydroxyalkyl, each R2 is independently linear or branched C1-C12 alkyl, C1-C6 hydroxyalkyl, C6F5, arylalkyl, C6H4OH, R3COOH, or R3SO3H, or R1 and R2 are linked together to form a morpholino or pyrrolidino ring, R3 is linear or branched C1-C12 alkyl, CH(COOH)CH2CH2, C6H4, or C6H3(OH), h1+h2 is h, h is a positive integer, k is zero or a positive integer, i and j are each independently zero or a positive integer, provided that the total of 1) h÷(k+h+i+j) is from about 0.005 to about 0.7, 2) k÷(k+h+i+j) is from about 0.3 to about 0.6, 3) [i+j]÷(k+h+i+j) is 0 to about 0.6, and provided that the sum of 1)+2)+3) is 1.0, said monomers occurring in any sequence.

9. 发明授权

US07815690B2 Perfluoroamidated and hydrolyzed maleic anhydride copolymers 失效
标题翻译：全氟酰胺化和水解马来酸酐共聚物
公开(公告)号：US07815690B2
公开(公告)日：2010-10-19
申请号：US12620773
申请日：2009-11-18
申请人： Stephen Ernest Jacobson , Peter Michael Murphy , Melea Rena Langley
发明人： Stephen Ernest Jacobson , Peter Michael Murphy , Melea Rena Langley
IPC分类号： D06M15/263 , D06M15/277 , D06M15/285
CPC分类号： D06M15/295 , C08F8/00 , Y10T428/23986 , Y10T428/2933 , Y10T428/31725 , Y10T428/31786 , Y10T442/20 , C08F222/06
摘要： A composition which provides stain resistance and soil resistance to substrates comprising a copolymer of Formula 1 is disclosed, wherein D, M, R, Rf, x, k, h, i and j are defined as in claim 1.
摘要翻译：公开了一种对包含式1的共聚物的基材提供抗污性和耐污性的组合物，其中D，M，R，R f，x，k，h，i和j如权利要求1中所定义。

10. 发明申请

US20100004482A1 FLUORINATED ESTERS 失效
标题翻译：氟化酯
公开(公告)号：US20100004482A1
公开(公告)日：2010-01-07
申请号：US12165824
申请日：2008-07-01
申请人： Peter Michael Murphy , Tracy Hewat
发明人： Peter Michael Murphy , Tracy Hewat
IPC分类号： C07C69/63
CPC分类号： C07C69/65 , C07C69/657 , C07C235/08
摘要： A compound comprising Formula 2A, 2B, or 2C (Ra—O—CO—)2Y Formula 2A Ra—O—CO—Y—CO—O—(CH2CH2)Rf Formula 2B Ra—O—CO—Y—CO—O—R Formula 2C wherein Ra is the group (i) Rf(CH2CF2)d—(CgH2g)—; (ii) RfOCF2CF2—(CgH2g)—; (iii) RfOCFHCF2O(CH2CH2O)v—(CgH2g)—; (iv) RfOCFHCF2O(CwH2w)—; (v) RfOCF(CF3)CONH—(CgH2g)—; or (vi) Rf(CH2)h[(CF2CF2)i(CH2CH2)j]k; each Rf is independently CcF(2c+1); c is 2 to about 6; d is 1 to about 3; g is 1 to 4; v is 1 to about 4; w is from about 3 to about 12; h is 1 to about 6; i, j, and k are each independently 1, 2, or 3, or a mixture thereof; provided that the total number of carbon atoms in group (vi) is from about 8 to about 22; Y is a linear or branched diradical having olefinic unsaturation of the formula —CeH(2e−2)— wherein e is 2 or 3; R is H or a linear or branched alkyl group CbH(2b+1)—; and b is from 1 to about 18.
摘要翻译：包含式2A，2B或2C（Ra-O-CO-）2Y的化合物式2A Ra-O-CO-Y-CO-O-（CH2CH2）Rf式2B Ra-O-CO-Y-CO-OR 式（Ⅱ）其中Ra是基团（ⅰ）Rf（CH2CF2）d-（CgH2g） - ; （ⅱ）RfOCF2CF2-（CgH2g） - ; （iii）RfOCFHCF2O（CH2CH2O）v-（CgH2g） - ; （iv）RfOCFHCF2O（CwH2w） - ; （v）RfOCF（CF 3）CONH-（CgH2g） - ; 或（vi）Rf（CH 2）h [（CF 2 CF 2）i（CH 2 CH 2）j] k; 每个Rf独立地为CcF（2c + 1）; c为2至约6; d为1〜3; g为1〜4; v为1至约4; w为约3至约12; h为1〜6; i，j和k各自独立地为1,2或3，或其混合物; 组（vi）中的碳原子总数为约8至约22; Y是具有式-CeH（2e-2） - 烯烃不饱和键的直链或支链双基，其中e为2或3; R是H或直链或支链烷基CbH（2b + 1） - ; b为1至约18。

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