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91. 发明授权

EP1118097B1 VORTEX GAS FLOW INTERFACE FOR ELECTROSPRAY MASS SPECTROMETRY 有权
标题翻译：气体回旋过渡件，电力喷雾质谱
公开(公告)号：EP1118097B1
公开(公告)日：2006-11-22
申请号：EP99954671.6
申请日：1999-09-27
申请人： Varian, Inc.
发明人： WELLS, Gregory, J. , TONG, Roger, C. , YEE, Peter, P.
IPC分类号： H01J49/04
CPC分类号： H01J49/165 , G01N30/7246 , G01N30/7266 , H01J49/049
摘要： An apparatus for efficiently removing a carrier liquid from charged liquid drops formed by electrospray ionization prior to introduction of the drops into a mass spectrometer (209). A central capillary tube (210) connects a region of the low pressure vacuum system containing the mass spectrometer (209) with a region at substantially atmospheric pressure, in which ion formation is produced by electrospray ionization. Heated, drying gas flows through a plurality of vortex forming channels (214) symmetrically disposed about the axis of the central capillary tube (210) which provides an entrance to the spectrometer (209). Gas exiting the vortex forming channels (214) enters tangentially to the inside of a vortex drying tube (222) with a small helix angle, causing the gas to swirl around the tube, forming a vortex. The vortex drying gas flows in a direction that is substantially transverse to the axis of the entrance capillary into the mass spectrometer (209). The vortex gas intersects the electrospray, separating undesired large drops from smaller drops by a vortex gas flow which imparts a centrifugal force to the drops. The largest drops are driven to the wall of the drying tube (222) and caused to fragment into smaller drops by evaporation and collision with the wall (222).

92. 发明公开

EP1118097A1 VORTEX GAS FLOW INTERFACE FOR ELECTROSPRAY MASS SPECTROMETRY 有权
标题翻译：气体回旋过渡件，电力喷雾质谱
公开(公告)号：EP1118097A1
公开(公告)日：2001-07-25
申请号：EP99954671.6
申请日：1999-09-27
申请人： Varian, Inc.
发明人： WELLS, Gregory, J. , TONG, Roger, C. , YEE, Peter, P.
IPC分类号： H01J49/04
CPC分类号： H01J49/165 , G01N30/7246 , G01N30/7266 , H01J49/049
摘要： An apparatus for efficiently removing a carrier liquid from charged liquid drops formed by electrospray ionization prior to introduction of the drops into a mass spectrometer (209). A central capillary tube (210) connects a region of the low pressure vacuum system containing the mass spectrometer (209) with a region at substantially atmospheric pressure, in which ion formation is produced by electrospray ionization. Heated, drying gas flows through a plurality of vortex forming channels (214) symmetrically disposed about the axis of the central capillary tube (210) which provides an entrance to the spectrometer (209). Gas exiting the vortex forming channels (214) enters tangentially to the inside of a vortex drying tube (222) with a small helix angle, causing the gas to swirl around the tube, forming a vortex. The vortex drying gas flows in a direction that is substantially transverse to the axis of the entrance capillary into the mass spectrometer (209). The vortex gas intersects the electrospray, separating undesired large drops from smaller drops by a vortex gas flow which imparts a centrifugal force to the drops. The largest drops are driven to the wall of the drying tube (222) and caused to fragment into smaller drops by evaporation and collision with the wall (222).

93. 发明公开

EP1051603A1 DISPOSITIF POUR LA QUALIFICATION DE PRODUITS CONTENANT DES SUBSTANCES VOLATILES 有权
标题翻译：设备为产品，方便挥发性成分资格
公开(公告)号：EP1051603A1
公开(公告)日：2000-11-15
申请号：EP99901556.3
申请日：1999-01-19
申请人： Zesiger, Thierry
发明人： Zesiger, Thierry
IPC分类号： G01N1/00 , G01N30/18
CPC分类号： G01N35/1079 , G01N30/18 , G01N30/24 , G01N2001/2229 , G01N2030/025 , H01J49/0031 , H01J49/0413 , H01J49/049 , Y10T436/25 , Y10T436/2575
摘要： The invention concerns a device for qualifying products containing volatile substances forming an analyte, comprising a measuring apparatus (2) provided with an enclosure (21a) and an electronic analysing circuit (21b) for defining said analyte characteristics, a pumping system (30) for producing a vacuum inside said enclosure, a sampling chamber (16) wherein the analyte is introduced and a capillary (22) for connecting said chamber (16) to said enclosure (21a). The invention is characterised in that the chamber (16) comprises: a first inlet (18) for introducing the analyte and provided with a sealed plug (27, 60, 62); a second inlet (17) connected to a blow-down gas (11) and provided with a valve (23); and an outlet (19) for evacuating the gas contained in the chamber (16) and likewise provided with a valve (29), and it further comprises a transfer device (35, 32) for introducing the analyte into the chamber and a programmer (15) controlling the analysing circuit (21b), the transfer device (35, 32) and the valves (23, 29), and arranged such that the purge of the chamber (16), the enclosure (21a) and the capillary (22) can be carried out automatically.

94. 发明授权

EP0452930B1 Apparatus for sample ionization and mass spectrometry 失效
标题翻译：设备Probeionisierung和质谱
公开(公告)号：EP0452930B1
公开(公告)日：1996-07-03
申请号：EP91106232.1
申请日：1991-04-18
申请人： HITACHI, LTD.
发明人： Kato, Yoshiaki
IPC分类号： H01J49/04
CPC分类号： H01J49/049 , H01J49/045 , H01J49/145

95. 发明公开

EP0465720A3 Analysenvorrichtung mit elektrothermischem Atomisator und Massenspektrometer zur Atom- und Molekülanalyse 失效
标题翻译：具有电热原子的分析装置和用于原子和分子分析的质谱仪
公开(公告)号：EP0465720A3
公开(公告)日：1992-08-19
申请号：EP90122801.5
申请日：1990-11-29
申请人： SPECTRO ANALYTICAL INSTRUMENTS Gesellschaft für analytische Messgeräte mbH
发明人： Falk, Heinz, Prof. Dr. , Wollnik, Hermann, Prof. Dr.
IPC分类号： H01J49/04
CPC分类号： H01J49/049 , G01N1/22
摘要： Die Erfindung betrifft eine Analysenvorrichtung zur Messung der Konzentrationen von Element- oder Molekülbestandteilen einer festen, flüssigen oder als Aerosol vorliegenden Probe (1), wobei die Probe von einem elektrothermischen Atomisator (2) getrocknet, erforderlichenfalls verascht, verdampft, der Probendampf ionisiert, die gebildeten Ionen in einem Ionenspeicher (7) gesammelt und die gespeicherten Ionen während einer gegen die Speicherzeit möglichst kurzen Zeit einem vorzugsweise simultan arbeitenden Massenspektrometer (8,10) zugeführt und die Häufigkeiten der jeweiligen Ionenmassen gemessen werden.

96. 发明公开

EP0465720A2 Analysenvorrichtung mit elektrothermischem Atomisator und Massenspektrometer zur Atom- und Molekülanalyse 失效
标题翻译： Atomicator和Massenspektrometer zur Atom- undMolekülanalyse。
公开(公告)号：EP0465720A2
公开(公告)日：1992-01-15
申请号：EP90122801.5
申请日：1990-11-29
申请人： SPECTRO ANALYTICAL INSTRUMENTS Gesellschaft für analytische Messgeräte mbH
发明人： Falk, Heinz, Prof. Dr. , Wollnik, Hermann, Prof. Dr.
IPC分类号： H01J49/04
CPC分类号： H01J49/049 , G01N1/22
摘要： Die Erfindung betrifft eine Analysenvorrichtung zur Messung der Konzentrationen von Element- oder Molekülbestandteilen einer festen, flüssigen oder als Aerosol vorliegenden Probe (1), wobei die Probe von einem elektrothermischen Atomisator (2) getrocknet, erforderlichenfalls verascht, verdampft, der Probendampf ionisiert, die gebildeten Ionen in einem Ionenspeicher (7) gesammelt und die gespeicherten Ionen während einer gegen die Speicherzeit möglichst kurzen Zeit einem vorzugsweise simultan arbeitenden Massenspektrometer (8,10) zugeführt und die Häufigkeiten der jeweiligen Ionenmassen gemessen werden.
摘要翻译：本发明涉及一种分析装置，用于测量固体或液体样品或气溶胶形式的样品的元素或分子成分的浓度，样品被电热雾化器干燥，如果需要焚烧并蒸发，样品蒸气被离子化，所形成的离子被收集在离子储存器中，并且储存的离子在与优选同时操作的质谱仪的存储时间尽可能短的时间内进料，离子质量的频率在特定情况下进行测量。 ... ...

97. 发明公开

EP0252758A2 Discharge ionization mass spectrometer 失效
标题翻译： Entladungsionisation-Massenspektrometer。
公开(公告)号：EP0252758A2
公开(公告)日：1988-01-13
申请号：EP87306137.8
申请日：1987-07-10
申请人： FISONS plc
发明人： Bateman, Robert Harold, Dr. , Jones, David Spencer, Dr.
IPC分类号： H01J49/04 , H01J49/12
CPC分类号： H01J49/049 , G01N30/726 , H01J49/0445 , H01J49/12
摘要： The invention provides a mass spectrometer (10) for the analysis of a sample dissolved in a fluid, and in particular a spectrometer for the analysis of high molecular weight compounds in the eluent of a liquid chromatograph.
The fluid to be analyzed is at least partly vaporized and sprayed into the cathode dark space (45) of a glow discharge (46). Ions characteristic of the sample are extracted from the discharge and subsequently mass analyzed. Conveniently, spraying into the cathode dark space (45) is achieved by making the cathode electrode of the discharge comprise the spraying means (38) through which the fluid is sprayed. Little fragmentation of the high mass ions is caused by the process, and the invention extends the range of compounds which can be analyzed in comparison with similar prior art thermospray type mass spectrometers.
摘要翻译：本发明提供了用于分析溶解在流体中的样品的质谱仪（10），特别是用于分析液相色谱仪洗脱液中高分子量化合物的光谱仪。要分析的流体至少部分蒸发并喷射到辉光放电（46）的阴极暗空间（45）中。从放电中提取样品的离子特征，随后进行质量分析。方便地，通过使排放物的阴极电极喷射流体喷射装置（38）来实现向阴极暗空间（45）的喷射。通过该方法引起高质量离子的少量碎裂，并且与现有技术的热喷涂型质谱仪相比，本发明扩展了可分析的化合物的范围。

98. 发明公开

EP0153113A3 Thermospray ion sampling device 失效
标题翻译：热释放离子采样装置
公开(公告)号：EP0153113A3
公开(公告)日：1987-09-23
申请号：EP85300876
申请日：1985-02-08
申请人： FINNIGAN CORPORATION
发明人： McFadden, William H. , Tucker, Michael G.
IPC分类号： H01J49/04
CPC分类号： H01J49/049 , H01J49/0445 , H01J49/067
摘要： The performance of a thermospray ion source for liquid chromatograph/mass spectrometers is improved dramatically by providing a voltage gradient across the thermospray jet stream to increase the efficiency of transferring ions of all maases from the thermospray jet stream to the mass spectrometer, and in particular the intensity of high mass ions relative to low mass ions.

99. 发明公开

EP0153113A2 Thermospray ion sampling device 失效
标题翻译：温泉 - 蒸汽喷雾器Vorrichtung zur Ionenprobeentnahme。
公开(公告)号：EP0153113A2
公开(公告)日：1985-08-28
申请号：EP85300876.1
申请日：1985-02-08
申请人： FINNIGAN CORPORATION
发明人： McFadden, William H. , Tucker, Michael G.
IPC分类号： H01J49/04
CPC分类号： H01J49/049 , H01J49/0445 , H01J49/067
摘要： The performance of a thermospray ion source for liquid chromatograph/mass spectrometers is improved dramatically by providing a voltage gradient across the thermospray jet stream to increase the efficiency of transferring ions of all maases from the thermospray jet stream to the mass spectrometer, and in particular the intensity of high mass ions relative to low mass ions.
摘要翻译：通过在热喷射流中提供电压梯度来提高液相色谱/质谱仪的热喷射离子源的性能，从而提高将所有质量的离子从热喷射流输送到质谱仪的效率，特别是高质量离子相对于低质量离子的强度。

100. 发明专利

JP6270851B2 試料採取熱脱離装置有权
公开(公告)号：JP6270851B2
公开(公告)日：2018-01-31
申请号：JP2015532506
申请日：2013-09-20
申请人：スミスズディテクション−ワトフォードリミテッド
发明人：リーパイパー
IPC分类号： G01N1/00 , G01N1/22
CPC分类号： H01J49/049 , G01N1/02 , G01N1/44 , G01N27/622 , G01N33/227 , G01N2001/028 , H01J49/40

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