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31. 发明授权

US09828290B2 Graphite oxide entrainment in cement and asphalt composite 有权
公开(公告)号：US09828290B2
公开(公告)日：2017-11-28
申请号：US15503171
申请日：2015-08-18
申请人： Garmor Inc.
发明人： Sean Christiansen , David Restrepo , Richard Stoltz , Jeff Bullington
IPC分类号： C04B14/02 , C04B28/04 , C04B14/06 , C01B31/04
CPC分类号： C04B14/026 , C01B31/043 , C01B31/0469 , C01B32/192 , C01B32/198 , C01B32/20 , C04B14/06 , C04B26/26 , C04B28/04 , C04B14/00 , C04B40/0021
摘要： A method of producing dispersed of high quality graphene/graphite oxides in a powder matrix to then be reacted to form a composite. Where the powders have similar hydrophobicity and the graphene/graphite oxides has minimal surface oxidation or minimal epoxy group and where the powders are sonically mixed.

32. 发明申请

US20160244333A1 Environmentally benign production of graphene materials 有权
标题翻译：石墨烯材料的环保生产
公开(公告)号：US20160244333A1
公开(公告)日：2016-08-25
申请号：US14544821
申请日：2015-02-24
申请人： Aruna Zhamu , Bor Z. Jang
发明人： Aruna Zhamu , Bor Z. Jang
IPC分类号： C01B31/04 , C25B1/00
CPC分类号： C01B31/0469 , C01B31/0423 , C01B32/19 , C01B32/225 , C25B1/00
摘要： An intercalated graphite compound composition, comprising a layered graphite with interlayer spaces or interstices and an intercalant residing in at least one of said interstices, wherein said intercalant comprises a carboxylic acid and an oxidant selected from Li2FeO4, Na2FeO4, K2FeO4, LixCoO4, NaxCoO4, KxCoO4, LixNiO4, NaxNiO4, KxNiO4, or a combination thereof. This compound can be produced in an environmentally benign process. The compound can be further treated to produce separate graphene sheets.
摘要翻译：一种插层石墨化合物组合物，其包含层间石墨，具有层间空间或间隙，以及驻留在所述间隙中的至少一个中的插层剂，其中所述插入剂包含羧酸和选自Li 2 FeO 4，Na 2 FeO 4，K 2 FeO 4，Li x CoO 4，NaxCoO 4，K x CoO 4 ，LixNiO4，NaxNiO4，KxNiO4或其组合。该化合物可以以环境友好的方法生产。该化合物可以进一步处理以产生单独的石墨烯片。

33. 发明申请

US20160194207A1 METHOD FOR EXFOLIATING CARBONACEAOUS MATERIALS CONTAINING GRAPHITE, ASSISTED BY A DIELS-ALDER REACTION 有权
标题翻译：用于氧化还原反应的包含石墨的碳质材料的方法
公开(公告)号：US20160194207A1
公开(公告)日：2016-07-07
申请号：US14909012
申请日：2014-07-30
申请人： UNIVERSITÉ DE BORDEAUX , INSTITUT POLYTECHNIQUE DE BORDEAUX , CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE - CNRS
发明人： Dario BASSANI , Jean-Baptiste VERLHAC , Hugo Florian BARES
IPC分类号： C01B31/04 , H01L51/52
CPC分类号： C01B31/0469 , C01B32/19 , C01B32/225 , C01B2204/02 , C01B2204/04 , H01L51/5203 , H01L2251/301
摘要： The present invention relates to a process for exfoliating graphite in carbonaceous materials facilitated by a Diels-Alder reaction, and the applications of same, in particular for producing electronic or microelectronic components such as transparent conductive electrodes. The inventive method comprises a Diels-Alder reaction between a material containing graphite and an anthrone compound represented by formula (I), wherein X, R1, R2, R3 and R4 are as defined in the description, in an organic solvent, in the presence of a base, and subjected to sonication, ball-milling and/or high-shear mixing, at a temperature of between 15° C. and 65° C., to obtain the corresponding graphene Diels-Alder adduct.
摘要翻译：本发明涉及一种通过Diels-Alder反应促进碳质材料中石墨剥离的方法及其应用，特别是用于生产诸如透明导电电极的电子或微电子部件。本发明的方法包括在含有石墨的材料和由式（I）表示的蒽酮化合物之间的Diels-Alder反应，其中X，R1，R2，R3和R4如说明书中所定义，在有机溶剂中，在存在下的基底，并在15℃至65℃的温度下进行超声处理，球磨和/或高剪切混合，以获得相应的石墨烯狄尔斯 - 阿尔德加合物。

34. 发明申请

US20130171055A1 METHOD FOR MAKING GRAPHENE 有权
标题翻译：制作石墨的方法
公开(公告)号：US20130171055A1
公开(公告)日：2013-07-04
申请号：US13554127
申请日：2012-07-20
申请人： XIANG-MING HE , LI WANG , JIAN-JUN LI , JIAN-WEI GUO , WEN-TING SUN , JIAN-GUO REN
发明人： XIANG-MING HE , LI WANG , JIAN-JUN LI , JIAN-WEI GUO , WEN-TING SUN , JIAN-GUO REN
IPC分类号： C01B31/02 , B82Y40/00
CPC分类号： C01B31/0469 , B82Y30/00 , B82Y40/00 , C01B32/19 , C25B1/00 , H01M4/587
摘要： In the method for making graphene, an electrolyte solution is formed by dissolving an electrolyte lithium salt in an organic solvent. Lithium ions are separated out from the electrolyte lithium salt in the electrolyte solution. Metal lithium and graphite are disposed in the electrolyte solution, and the metal lithium and the graphite are in contact with each other. In the electrolyte solution, lithium ions and organic solvent molecules jointly insert between adjacent layers of the graphite to form a graphite intercalation compound. The graphene is peeled off from the graphite intercalation compound.
摘要翻译：在制造石墨烯的方法中，通过将电解质锂盐溶解在有机溶剂中形成电解质溶液。从电解液中的电解质锂盐中分离出锂离子。金属锂和石墨配置在电解液中，金属锂和石墨彼此接触。在电解液中，锂离子和有机溶剂分子在相邻的石墨层之间共同插入以形成石墨插层化合物。石墨烯从石墨插层化合物上剥离出来。

35. 发明申请

US20130001068A1 Production process for chemically functionalized nano graphene materials 有权
公开(公告)号：US20130001068A1
公开(公告)日：2013-01-03
申请号：US13573259
申请日：2012-09-06
申请人： Aruna Zhamu , Bor Z. Jang
发明人： Aruna Zhamu , Bor Z. Jang
IPC分类号： B01J19/10 , B82Y30/00
CPC分类号： C01B31/0469 , B01J19/10 , B82Y30/00 , B82Y40/00 , C01B32/19 , C01B32/194 , C01B32/225
摘要： A combined production-functionalization process for producing a chemically functionalized nano graphene material from a pre-intercalated, oxidized, or halogenated graphite material, comprising: (A) Producing exfoliated graphite from the pre-intercalated, oxidized, or halogenated graphite material, wherein the graphite material is selected from the group consisting of natural graphite, artificial graphite, highly oriented pyrolytic graphite, carbon fiber, graphite fiber, carbon nano-fiber, graphitic nano-fiber, meso-carbon micro-bead, graphitized coke, and combinations thereof; (B) Dispersing the exfoliated graphite and an azide or bi-radical compound in a liquid medium to form a suspension; (C) Subjecting the suspension to ultrasonication with ultrasonic waves of a desired intensity for a length of time sufficient to produce nano graphene platelets and to enable a chemical reaction to occur between the nano graphene platelets and the azide or bi-radical compound to produce the functionalized nano graphene material.

36. 发明申请

US20110017587A1 Production of chemically functionalized nano graphene materials 有权
标题翻译：生产化学官能化纳米石墨烯材料
公开(公告)号：US20110017587A1
公开(公告)日：2011-01-27
申请号：US12460860
申请日：2009-07-27
申请人： Aruna Zhamu , Bor Z. Jang
发明人： Aruna Zhamu , Bor Z. Jang
IPC分类号： B01J19/10
CPC分类号： C01B31/0469 , B01J19/10 , B82Y30/00 , B82Y40/00 , C01B32/19 , C01B32/194 , C01B32/225
摘要： Provided in this invention is a process for producing chemically functionalized nano graphene materials, known as nano graphene platelets (NGPs), graphene nano sheets, or graphene nano ribbons. Subsequently, a polymer can be grafted to a functional group of the resulting functionalized NGPs. In one preferred embodiment, the process comprises (A) dispersing a pristine graphite material and an azide or bi-radical compound in a liquid medium comprising to form a suspension; and (B) subjecting the suspension to direct ultrasonication with to ultrasonic waves of a desired intensity or power level for a length of time sufficient to produce nano graphene platelets and to enable a chemical reaction to occur between the nano graphene platelets and the azide or bi-radical compound to produce the functionalized nano graphene material. Concurrent production and functionalization of NGPs directly from pristine graphitic materials can be achieved in one step and in the same reactor.
摘要翻译：在本发明中提供了一种生产化学官能化的纳米石墨烯材料的方法，称为纳米石墨烯片（NGP），石墨烯纳米片或石墨烯纳米带。随后，可以将聚合物接枝到得到的官能化NGP的官能团上。在一个优选实施方案中，该方法包括（A）将原始石墨材料和叠氮化物或双自由基化合物分散在包含形成悬浮液的液体介质中; 和（B）使悬浮液对所需强度或功率水平的超声波进行超声波处理足够长的时间以产生纳米石墨烯血小板，并使纳米石墨烯血小板和叠氮化物或二氧化钛之间发生化学反应以制备功能化的纳米石墨烯材料。直接来自原始石墨材料的NGP的并行生产和功能化可以在一个步骤和同一个反应器中实现。

37. 发明申请

US20090169467A1 Production of ultra-thin nano-scaled graphene platelets from meso-carbon micro-beads 有权
标题翻译：从中碳微珠生产超薄纳米级石墨烯血小板
公开(公告)号：US20090169467A1
公开(公告)日：2009-07-02
申请号：US12005015
申请日：2007-12-26
申请人： Aruna Zhamu , Jiusheng Guo , Bor Z. Jang
发明人： Aruna Zhamu , Jiusheng Guo , Bor Z. Jang
IPC分类号： C01B31/04
CPC分类号： C01B31/0469 , B82Y30/00 , B82Y40/00 , C01B32/19 , C01B32/22 , C01B2204/04 , C01B2204/32 , C01P2004/03 , C01P2004/32 , C01P2006/12 , C09C1/44 , C09C1/46 , C09C1/565
摘要： A method of producing nano-scaled graphene platelets (NGPs) having an average thickness no greater than 50 nm, typically less than 2 nm, and, in many cases, no greater than 1 nm. The method comprises (a) intercalating a supply of meso-carbon microbeads (MCMBs) to produce intercalated MCMBs; and (b) exfoliating the intercalated MCMBs at a temperature and a pressure for a sufficient period of time to produce the desired NGPs. Optionally, the exfoliated product may be subjected to a mechanical shearing treatment, such as air milling, air jet milling, ball milling, pressurized fluid milling, rotating-blade grinding, or ultrasonicating. The NGPs are excellent reinforcement fillers for a range of matrix materials to produce nanocomposites. Nano-scaled graphene platelets are much lower-cost alternatives to carbon nano-tubes or carbon nano-fibers.
摘要翻译：制备平均厚度不超过50nm，通常小于2nm，并且在许多情况下不大于1nm的纳米级石墨烯片晶（NGP）的方法。该方法包括：（a）插入供应的中碳微珠（MCMB）以产生嵌入的MCMB; 和（b）在温度和压力下将嵌入的MCMBs剥离足够的时间以产生所需的NGP。任选地，剥离的产品可以经受机械剪切处理，例如空气研磨，空气喷射研磨，球磨，加压流体研磨，旋转叶片研磨或超声波处理。 NGP是用于生产纳米复合材料的一系列基质材料的优良增强填料。纳米级石墨烯血小板是碳纳米管或碳纳米纤维成本低廉的替代品。

38. 发明申请

WO2017155665A1 ELECTROCHEMICAL PRODUCTION OF GRAPHENE SHEETS DIRECTLY FROM GRAPHITE MINERAL 审中-公开
标题翻译：从石墨矿物直接电化学生产石墨板材
公开(公告)号：WO2017155665A1
公开(公告)日：2017-09-14
申请号：PCT/US2017/017458
申请日：2017-02-10
申请人： ZHAMU, Aruna , JANG, Bor Z. , ANGSTRON MATERIALS, INC.
发明人： ZHAMU, Aruna , JANG, Bor Z.
IPC分类号： B82Y30/00 , C01B31/04 , C25B1/00
CPC分类号： C01B31/0469 , C01B32/19 , C01B2204/02 , C01B2204/04 , C25B1/00 , C25B9/16
摘要： A method of producing graphene sheets directly from graphite, comprising: (a) forming an intercalated graphite compound by an electrochemical intercalation procedure conducted in an intercalation reactor, containing (i) a liquid solution electrolyte comprising an intercalating agent and a graphene plane-wetting agent dissolved therein; (ii) a working electrode that contains the graphite material powder as an active material; and (iii) a counter-electrode, and wherein a current is imposed upon the working electrode and counter electrode at a current density sufficient for effecting electrochemical intercalation of the intercalating agent and/or wetting agent into interlayer spacing, wherein the wetting agent is selected from melamine, ammonium sulfate, sodium dodecyl sulfate, Na(ethylenediamine), tetraalkyammonium, ammonia, carbamide, hexamethylenetetramine, organic amine, poly(sodium-4-styrene sulfonate), or a combination thereof; and (b) exfoliating and separating the intercalated graphite compound using ultrasonication, thermal shock exposure, and/or a mechanical shearing treatment to produce graphene sheets.
摘要翻译：一种直接由石墨生产石墨烯片的方法，其包括：（a）通过在插层反应器中进行的电化学插层程序形成插层石墨化合物，所述插层反应器包含（i）液体溶液电解质，其包含嵌入试剂和溶解在其中的石墨烯平面润湿剂; （ii）包含石墨材料粉末作为活性材料的工作电极; 和（iii）反电极，并且其中电流以足以实现嵌入剂和/或润湿剂电化学嵌入到层间间隔中的电流密度施加在工作电极和反电极上，其中选择润湿剂三聚氰胺，硫酸铵，十二烷基硫酸钠，Na（乙二胺），四烷基铵，氨，脲，六亚甲基四胺，有机胺，聚（4-苯乙烯磺酸钠）或其组合; 和（b）使用超声波，热冲击暴露和/或机械剪切处理来剥离和分离插层石墨化合物以生产石墨烯片。

39. 发明申请

WO2014200649A1 METHOD OF PRODUCING A GRAPHENE MATERIAL 审中-公开
标题翻译：生产石墨材料的方法
公开(公告)号：WO2014200649A1
公开(公告)日：2014-12-18
申请号：PCT/US2014/037951
申请日：2014-05-14
申请人： GRAFTECH INTERNATIONAL HOLDINGS INC.
发明人： SRIVASTAVA, Iti
IPC分类号： C01B31/04
CPC分类号： C01B31/0469 , C01B32/184 , C01B32/19 , C01B2204/04
摘要： A method of producing graphene powder includes the heat treatment of a graphitizable polymer film to at least 2000 degrees C to form a heat treated film having a substantially turbostratic graphitic structure. The heat treated film is then sheared along a plane substantially parallel to a major surface of the heat treated film to form a particulate having a thickness less than 100 nanometers.
摘要翻译：制造石墨烯粉末的方法包括将可石墨化聚合物膜热处理至少2000℃以形成具有基本上涡旋石墨结构的热处理膜。然后将热处理膜沿着基本上平行于热处理膜的主表面的平面剪切以形成厚度小于100纳米的颗粒。

40. 发明申请

WO2012151433A3 POLYETHYLENE TEREPHTHALATE-GRAPHENE NANOCOMPOSITES 审中-公开
标题翻译：聚乙烯三烯酸盐 - 石墨纳米复合材料
公开(公告)号：WO2012151433A3
公开(公告)日：2013-01-17
申请号：PCT/US2012036376
申请日：2012-05-03
申请人： UNIV OKLAHOMA STATE , HANAN JAY CLARKE
发明人： HANAN JAY CLARKE
IPC分类号： C08L67/03 , B82Y30/00 , C08K3/04
CPC分类号： C08K3/042 , B29C45/0001 , B29C45/0013 , B29K2067/003 , B29K2507/04 , B82Y30/00 , C01B31/0469 , C01B2204/32 , C08J3/22 , C08J2367/02 , C08K3/04 , C08K9/08 , C08K2201/003 , Y10S977/734 , Y10S977/776
摘要： A nanocomposite material comprises polyethylene terephthalate (PET) as a base polymer and a nanoparticle that increases the strength of the base polymer.
摘要翻译：纳米复合材料包括作为基础聚合物的聚对苯二甲酸乙二醇酯（PET）和增加基础聚合物强度的纳米颗粒。

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