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    • 34. 发明申请
    • METHODS AND APPARATUS FOR PERFORMING CHROMATOGRAPHY AND MASS SPECTROSCOPY WITH SUPERCRITICAL FLUID SAMPLES
    • 用超临界流体样品进行色谱和质谱分析的方法和装置
    • US20080296492A1
    • 2008-12-04
    • US12127313
    • 2008-05-27
    • Joseph A. Jarrell
    • Joseph A. Jarrell
    • B01D59/44
    • G01N30/724G01N30/7246H01J49/165B01D15/40
    • Embodiments of the present invention are directed to devices and methods for receiving NSC Fluids having at least one analyte from a chromatograph and directing analyte ions into the vacuum regions of a mass spectrometer. The device has a housing having at least one wall defining a chamber, sample inlet, an ionization media inlet and an outlet. The sample inlet has a position in communication with a chromatograph receiving a NSC Fluid. The sample inlet receives the NSC Fluid and directs the NSC Fluid into the chamber to form a sample jet of NSC Fluid. The ionization media inlet is placed in fluid communication with a source of ionization media and directs the ionization media into the chamber and the sample jet to create analyte ions. The analyte ions are received in the mass spectrometer vacuum region orifice.
    • 本发明的实施方案涉及用于接收具有来自色谱仪的至少一种分析物并将分析物离子导入质谱仪的真空区域的NSC流体的装置和方法。 该装置具有壳体,该壳体具有限定腔室,样品入口,离子化介质入口和出口的至少一个壁。 样品入口具有与接收NSC流体的色谱仪连通的位置。 样品入口接收NSC流体并将NSC流体引导到室中以形成NSC Fluid的样品射流。 离子化介质入口与离子化介质源流体连通,并将电离介质引导到室中,并将样品射流引导以产生分析物离子。 分析离子被接收在质谱仪真空区域孔中。