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71. 发明授权

US5419890A Use of organic solvents in the synthesis of V.sub.6 O.sub.13+x [0<x.ltoreq.2] 失效
标题翻译：在合成V6O13 + x [0
公开(公告)号：US5419890A
公开(公告)日：1995-05-30
申请号：US260130
申请日：1994-06-14
申请人： M. Yazid Saidi
发明人： M. Yazid Saidi
IPC分类号： C01G31/02 , H01M4/131 , H01M4/48 , H01M4/485 , H01M10/052 , H01M10/0565 , H01M10/36 , H01M4/58
CPC分类号： H01M4/485 , C01G31/02 , C01P2002/72 , C01P2004/03 , C01P2004/61 , H01M10/052 , H01M10/0565 , H01M4/131 , H01M4/661 , Y02P70/54
摘要： A method of making non-stoichiometric vanadium oxides V.sub.6 O.sub.13+x by treatment with H.sub.2 O.sub.2 in an organic medium.
摘要翻译：通过在有机介质中用H 2 O 2处理制备非化学计量的钒氧化物V6O13 + x的方法。

72. 发明授权

US5824120A Electrically conductive adhesion promoters for current collectors 失效
标题翻译：用于集电器的导电粘合促进剂
公开(公告)号：US5824120A
公开(公告)日：1998-10-20
申请号：US634752
申请日：1996-04-10
申请人： Porter H. Mitchell , M. Yazid Saidi
发明人： Porter H. Mitchell , M. Yazid Saidi
IPC分类号： H01M4/13 , H01M4/62 , H01M4/66 , H01M4/60
CPC分类号： H01M4/13 , H01M4/667 , H01M4/04 , H01M4/621 , H01M4/668 , Y10T29/49108 , Y10T29/49114
摘要： A method of preparing an electrochemical cell wherein the composite electrode material adheres to the metal current collector to create good electrical contact is provided. The electrode/current collector comprises a current collector, a layer of an electrically conductive adhesion promoter formed on at least one surface of the current collector which comprises an electrically conductive material and an adhesive polymer; and a composite electrode selected from the group consisting of composite cathode and composite anode, wherein the thickness of said electrically conductive adhesive promoter is sufficient to bind the composite electrode to said current collector.
摘要翻译：提供了一种制备电化学电池的方法，其中复合电极材料粘附到金属集电器以产生良好的电接触。电极/集电器包括集电器，形成在集电器的至少一个表面上的导电粘合促进层，其包括导电材料和粘合剂聚合物; 以及选自复合阴极和复合阳极的复合电极，其中所述导电粘合剂助剂的厚度足以将复合电极结合到所述集电器。

73. 发明授权

US5770018A Method for preparing lithium manganese oxide compounds 失效
标题翻译：锰酸锂化合物的制备方法
公开(公告)号：US5770018A
公开(公告)日：1998-06-23
申请号：US630303
申请日：1996-04-10
申请人： M. Yazid Saidi
发明人： M. Yazid Saidi
IPC分类号： C01G45/00 , H01M4/133 , H01M4/1393 , H01M4/50 , H01M4/505 , H01M4/62 , H01M10/0525 , H01M10/36 , C07C1/00 , C01D1/00 , C01G45/12
CPC分类号： H01M4/505 , C01G45/1242 , H01M4/623 , C01P2002/32 , C01P2002/77 , C01P2006/40 , H01M10/0525 , H01M4/133 , H01M4/1393 , H01M4/625
摘要： The present invention provides a method of preparing an intercalation compound of the nominal general formula Li.sub.x Mn.sub.2 O.sub.4, where x is greater than 0 and less than 2, which comprises providing a manganese compound and a lithium compound and mixing such compounds in proportion which provides the desired amount of x demonstrated by the nominal general formula. The mixed compounds are then irradiated with electromagnetic radiation, desirably microwave frequency or infrared radiation whereby manganese, lithium, and oxygen combine to form the Li.sub.x Mn.sub.2 O.sub.4 having the desired quantity x of lithium. It is desired that the heating by radiation be conducted in air. Preferably, the radiation is microwave radiation and such radiation is at a frequency which causes atomic bonds to vibrate within at least a portion of the precursor compounds and/or the solvent contained in the mixture.
摘要翻译：本发明提供了制备标称通式为LixMn 2 O 4的嵌入化合物的方法，其中x大于0且小于2，其包括提供锰化合物和锂化合物，并将这些化合物按比例混合，提供所需量的x通过标称通用方程式证明。然后用电磁辐射，理想的微波频率或红外辐射照射混合的化合物，由此锰，锂和氧结合形成具有所需量x的锂的LixMn2O4。希望通过辐射进行加热在空气中进行。优选地，辐射是微波辐射，并且这种辐射的频率使得原子键在至少一部分前体化合物和/或混合物中包含的溶剂中振动。

74. 发明授权

US5545496A Process for producing filament-like vanadium oxide for use in solid state rechargeable electrochemical cells and the use thereof as a cathode in electrochemical cells 失效
标题翻译：生产用于固态可再充电电化学电池的长丝状氧化钒的方法及其在电化学电池中作为阴极的用途
公开(公告)号：US5545496A
公开(公告)日：1996-08-13
申请号：US271341
申请日：1994-07-06
申请人： On-Kok Chang , M. Yazid Saidi
发明人： On-Kok Chang , M. Yazid Saidi
IPC分类号： C01G31/02 , H01M4/131 , H01M4/1391 , H01M4/48 , H01M4/485 , H01M6/18 , H01M10/052 , H01M10/36 , H01M4/22
CPC分类号： H01M4/485 , C01G31/02 , C01P2002/10 , C01P2004/03 , C01P2004/10 , C01P2004/50 , C01P2006/10 , C01P2006/80 , H01M10/052 , H01M4/131 , H01M4/1391 , H01M6/181 , Y10T29/49108
摘要： The present invention provides a novel process for synthesizing vanadium oxide V.sub.6 O.sub.13 with a filament-like morphology by thermally decomposing ammonium metavanadate NH.sub.4 VO.sub.3 in the presence of a compound which sublimes upon heating. The reaction is carried out in an inert gas flow. The V.sub.6 O.sub.13 synthesized according to this invention can be used as cathode active material in electrochemical batteries.
摘要翻译：本发明提供了通过在加热下升华的化合物存在下热分解偏钒酸铵NH4VO3来合成具有丝状形态的氧化钒V6O13的新方法。反应在惰性气体流中进行。根据本发明合成的V6O13可用作电化学电池中的阴极活性材料。

75. 发明申请

US20150123028A1 Manganese Phosphates and Related Electrode Active Materials 有权
标题翻译：锰磷酸盐和相关电极活性材料
公开(公告)号：US20150123028A1
公开(公告)日：2015-05-07
申请号：US14071884
申请日：2013-11-05
申请人： Haitao Huang , M. Yazid Saidi
发明人： Haitao Huang , M. Yazid Saidi
IPC分类号： H01M4/58
CPC分类号： H01M4/5825 , C01B25/26 , C01B25/45 , H01M10/052 , H01M10/0525
摘要： The invention provides electrode active materials comprising lithium or other alkali metals, manganese, a +3 oxidation state metal ion, and optionally other metals, and a phosphate moiety. Such electrode active materials include those of the formula: AaMnbMIcMIIdMIIIePO4 wherein (a) A is selected from the group consisting of Li, Na, K, and mixtures thereof, and 0
摘要翻译：本发明提供了包含锂或其它碱金属，锰，+3氧化态金属离子和任选的其它金属以及磷酸盐部分的电极活性材料。这种电极活性材料包括下式的那些：AaMnbMIcMIIdMIIIePO4，其中（a）A选自Li，Na，K及其混合物，0

76. 发明授权

US08318352B2 Batteries comprising alkali-transition metal phosphates and preferred electrolytes 失效
标题翻译：包含碱金属过渡金属磷酸盐和优选的电解质的电池
公开(公告)号：US08318352B2
公开(公告)日：2012-11-27
申请号：US11080605
申请日：2005-03-15
申请人： M. Yazid Saidi , Haitao Huang , James K. Pugh
发明人： M. Yazid Saidi , Haitao Huang , James K. Pugh
IPC分类号： H01M4/52
CPC分类号： H01M10/0569 , H01M4/0471 , H01M4/136 , H01M4/56 , H01M4/5815 , H01M4/582 , H01M4/5825 , H01M4/622 , H01M4/623 , H01M4/624 , H01M4/625 , H01M10/0525 , H01M10/0568 , H01M2004/027
摘要： A secondary electrochemical cell is described having (a) a first electrode comprising an active material of the formula LiaCoeFefM1gM2hM3iXY4, (b) a second electrode which is a counter-electrode to said first electrode; and (c) an electrolyte comprising an electrolyte salt, a cyclic ester and a carbonate selected from the group consisting of alkyl carbonates, alkylene carbonates, and mixtures thereof.
摘要翻译：描述了二次电化学电池，其具有（a）第一电极，其包含式为LiaCoeFefM1gM2hM3iXY4的活性材料，（b）第二电极，其是与所述第一电极相对的电极; 和（c）包含电解质盐，环状酯和选自碳酸烷基酯，碳酸亚烷基酯及其混合物的碳酸盐的电解质。

77. 发明申请

US20100304196A1 Secondary Electrochemical Cell 审中-公开
标题翻译：二次电化学电池
公开(公告)号：US20100304196A1
公开(公告)日：2010-12-02
申请号：US11561295
申请日：2006-11-17
申请人： M. Yazid Saidi , Eileen Saidi , Jeffery L. Swoyer , Jung Souh
发明人： M. Yazid Saidi , Eileen Saidi , Jeffery L. Swoyer , Jung Souh
IPC分类号： H01M6/10
CPC分类号： H01M4/58 , H01M2/022 , H01M4/131 , H01M4/133 , H01M4/136 , H01M4/5825 , H01M4/587 , H01M4/623 , H01M10/0525 , H01M2004/021
摘要： The invention provides a cylindrical electrochemical cell which includes a first electrode and a second electrode which is a counter electrode to the first electrode, and an electrolyte. The first electrode includes a polyanion-based electrode active material.
摘要翻译：本发明提供了一种圆柱形电化学电池，其包括第一电极和作为与第一电极相对的第二电极和电解质。第一电极包括聚阴离子基电极活性材料。

78. 发明申请

US20090233178A1 LITHIUM-ION BATTERIES 审中-公开
标题翻译：锂离子电池
公开(公告)号：US20090233178A1
公开(公告)日：2009-09-17
申请号：US12047505
申请日：2008-03-13
申请人： M. Yazid Saidi , Haitao Huang
发明人： M. Yazid Saidi , Haitao Huang
IPC分类号： H01M10/40
CPC分类号： H01M4/587 , H01M4/1393 , H01M4/364 , H01M4/5825 , H01M4/621 , H01M4/622 , H01M10/0525 , H01M10/0568 , H01M10/0569 , H01M2300/0037
摘要： The present invention is based on the discovery that certain types of synthetic graphite exhibit superior rate capabilities when used in batteries or cells employing lithium metal phosphate cathodes. Additionally, it has been found that the use of dimethyl carbonate and/or ethyl methyl carbonate in the electrolyte when used in such graphite/lithium methyl phosphate batteries or cells facilitates the discharge reactions on both the cathode and the anode and in particular especially improves the rate capability of the graphite anode.
摘要翻译：本发明是基于以下发现：当使用在使用锂金属磷酸盐阴极的电池或电池中时，某些类型的合成石墨表现出优异的速率能力。此外，已经发现，当用于这种石墨/磷酸甲酯磷酸盐电池或电池中时，在电解质中使用碳酸二甲酯和/或碳酸甲乙酯有助于阴极和阳极上的放电反应，特别是改善了石墨阳极的速率能力。

79. 发明申请

US20070259265A1 SECONDARY ELECTROCHEMICAL CELL HAVING A NOVEL ELECTRODE ACTIVE MATERIAL 审中-公开
标题翻译：具有新型电极活性材料的二次电化学电池
公开(公告)号：US20070259265A1
公开(公告)日：2007-11-08
申请号：US11742059
申请日：2007-04-30
申请人： M. Yazid Saidi , Haitao Huang
发明人： M. Yazid Saidi , Haitao Huang
IPC分类号： H01M4/48 , H01M4/58 , H01M4/50
CPC分类号： H01M4/505 , H01M4/485 , H01M4/525 , H01M4/587 , H01M10/0525
摘要： The invention provides a novel polyanion-based electrode active material for use in a secondary or rechargeable electrochemical cell having a first electrode, a second electrode and an electrolyte.
摘要翻译：本发明提供了一种用于具有第一电极，第二电极和电解质的次级或可再充电电化学电池的新型聚阴离子基电极活性材料。

80. 发明授权

US07060238B2 Synthesis of metal phosphates 失效
标题翻译：金属磷酸盐的合成
公开(公告)号：US07060238B2
公开(公告)日：2006-06-13
申请号：US10794327
申请日：2004-03-04
申请人： M. Yazid Saidi , Haitao Huang
发明人： M. Yazid Saidi , Haitao Huang
IPC分类号： C01B25/45 , H01M4/58
CPC分类号： H01M4/5825 , C01B25/45 , H01M10/052
摘要： The present invention relates to a method for preparing a metal phosphate which comprises milling in a carbonaceous vessel a lithium source, a phosphate source, such as LiH2PO4, and a metal oxide containing a metal ion wherein the metal ion is capable of being reduced, to produced a milled mixture and heating the milled mixture in an inert atmosphere at a temperature and for a time sufficient to form a metal phosphate wherein the metal ion of the metal oxide is reduced in oxidation state without the direct addition of a reducing agent to the starting materials. In another embodiment the present invention relates to a method for preparing a mixed metal phosphate which comprises milling a lithium source and a phosphate source, such as LiH2PO4, a metal oxide and another metal compound wherein at least one of the metal compounds contains a metal ion capable of being reduced to produce a milled mixture and heating the resulting milled mixture in an inert atmosphere at a temperature and for a time sufficient to form a mixed metal phosphate, wherein the oxidation state of at least one of the metal ions is reduced in oxidation state without the direct addition of a reducing agent to the reactants. It is another object of the invention to provide electrochemically active materials produced by said methods.
摘要翻译：本发明涉及一种制备金属磷酸盐的方法，其包括在碳质容器中研磨锂源，磷酸盐源，例如LiH 2 PO 4，和含有金属离子的金属氧化物，其中能够还原金属离子，以制备研磨的混合物，并在惰性气氛中在足以形成金属磷酸盐的温度和时间下加热研磨的混合物，其中金属的金属离子氧化物在氧化状态下降低，而没有将还原剂直接加入原料中。在另一个实施方案中，本发明涉及一种制备混合金属磷酸盐的方法，该方法包括将锂源和磷酸盐源如LiH 2 PO 4，氧化物和另一种金属化合物，其中至少一种金属化合物含有能够还原的金属离子以产生研磨的混合物，并将所得研磨的混合物在惰性气氛中在足以形成混合金属磷酸盐的温度和时间其中至少一种金属离子的氧化态在氧化状态下降低，而没有将还原剂直接加入到反应物中。本发明的另一个目的是提供通过所述方法生产的电化学活性材料。

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