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71. 发明授权

US06960331B2 Methods of making lithium metal cathode active materials 有权
标题翻译：制备锂金属正极活性物质的方法
公开(公告)号：US06960331B2
公开(公告)日：2005-11-01
申请号：US10683643
申请日：2003-10-09
申请人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
发明人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
IPC分类号： C01B25/00 , C01B25/45 , C01B25/455 , C01G31/00 , H01M4/02 , H01M4/48 , H01M4/485 , H01M4/50 , H01M4/505 , H01M4/52 , H01M4/525 , H01M4/58 , H01M10/052 , H01M10/36 , C01B15/16
CPC分类号： H01M10/052 , C01B25/45 , C01B25/455 , C01G31/006 , C01G37/006 , C01G49/009 , C01P2002/72 , C01P2006/40 , H01M4/02 , H01M4/485 , H01M4/505 , H01M4/525 , H01M4/5825 , H01M2004/028
摘要： The invention provides a novel method for making lithium mixed metal materials in electrochemical cells. The lithium mixed metal materials comprise lithium and at least one other metal besides lithium. The invention involves the reaction of a metal compound, a phosphate compound, with a reducing agent to reduce the metal and form a metal phosphate. The invention also includes methods of making lithium metal oxides involving reaction of a lithium compound, a metal oxide with a reducing agent.
摘要翻译：本发明提供了一种在电化学电池中制备锂复合金属材料的新方法。锂混合金属材料除锂之外还包含锂和至少一种其它金属。本发明涉及金属化合物，磷酸盐化合物与还原剂的反应，以还原金属并形成金属磷酸盐。本发明还包括制造涉及锂化合物，金属氧化物与还原剂的反应的锂金属氧化物的方法。

72. 发明申请

US20050164084A1 Secondary battery electrode active materials and methods for making the same 失效
标题翻译：二次电池电极的活性物质及其制造方法
公开(公告)号：US20050164084A1
公开(公告)日：2005-07-28
申请号：US10763890
申请日：2004-01-22
申请人： George Adamson , Jeremy Barker , M. Saidi
发明人： George Adamson , Jeremy Barker , M. Saidi
IPC分类号： H01M4/136 , H01M4/32 , H01M4/34 , H01M4/36 , H01M4/58 , H01M6/16 , H01M6/18 , H01M10/0525 , H01M10/36
CPC分类号： H01M10/0525 , H01M4/136 , H01M4/5825
摘要： The invention provides an electrochemical cell which includes a first electrode and a second electrode which is a counter electrode to said first electrode, and an electrolyte material interposed there between. The first electrode comprises an electrode active material represented by the general nominal formula Aa[Mm,MIn,MIIo](XY4)dZe, wherein at least one of M, MI and MII is a redox active element, 0
摘要翻译：本发明提供了一种电化学电池，其包括第一电极和第二电极，第二电极是与所述第一电极对置的电极，以及介于其间的电解质材料。第一电极包括由通式A表示的电极活性材料，其中M 1，M 2，其中M，MI和MII中的至少一个是氧化还原活性元素，0（↓）其中V（M）为M的价态，V（MI）为V（M）的化合价态，其中V（M）为 MI和V（MII）是MII的化合价态。

73. 发明授权

US06869547B2 Stabilized electrochemical cell active material 失效
标题翻译：稳定的电化学电池活性材料
公开(公告)号：US06869547B2
公开(公告)日：2005-03-22
申请号：US09974043
申请日：2001-10-09
申请人： Jeremy Barker , M. Yazid Saldi , Jeffrey L. Swoyer
发明人： Jeremy Barker , M. Yazid Saldi , Jeffrey L. Swoyer
IPC分类号： C01G45/00 , C01G45/12 , H01M4/50 , H01M4/505 , H01M4/62 , H01M10/0525 , H01M10/0567 , H01M10/36 , H01M4/02
CPC分类号： H01M4/505 , C01G45/1242 , C01G45/125 , C01G45/1257 , C01P2002/32 , C01P2002/72 , C01P2002/77 , C01P2004/80 , C01P2004/84 , C01P2006/12 , C01P2006/40 , H01M4/62 , H01M10/0525 , H01M10/0567
摘要： Stabilized lithiated manganese oxide (LMO) is prepared by reacting cubic spinel lithium manganese oxide particles and particles of an alkali metal compound in air for a time and at a temperature sufficient to decompose at least a portion of the alkali metal compound, providing a treated lithium manganese oxide. The reaction product is characterized as particles having a core or bulk structure of cubic spinel lithium manganese oxide and a surface region which is enriched in Mn+4 relative to the bulk. X-ray diffraction data and x-ray photoelectron spectroscopy data are consistent with the structure of the stabilized LMO being a central bulk of cubic spinel lithium manganese oxide with a surface layer or region comprising A2MnO3, where A is an alkali metal. Electrochemical cells containing the stabilized LMO of the invention have improved charging and discharging characteristics and maintain integrity over a prolonged life cycle. The electrochemical cells are stabilized against decomposition of cell components, including electrode and electrolyte components.
摘要翻译：通过使立方尖晶石锂锰氧化物颗粒和碱金属化合物颗粒在空气中反应一段时间并在足以分解至少一部分碱金属化合物的温度下制备稳定的锂化锰氧化物（LMO），从而提供处理过的锂氧化锰。反应产物的特征在于具有立方尖晶石锂锰氧化物的核心或体积结构的颗粒和相对于体积富含Mn +4的表面区域。 X射线衍射数据和X射线光电子能谱数据与稳定的LMO的结构一致，稳定的LMO是具有包含A2MnO3的表面层或区域的立方尖晶石锂锰氧化物的中心体，其中A是碱金属。包含本发明的稳定的LMO的电化学电池具有改善的充电和放电特性并且在延长的寿命周期内保持完整性。电化学电池被稳定以防止细胞成分的分解，包括电极和电解质组分。

74. 发明授权

US06720112B2 Lithium cell based on lithiated transition metal titanates 失效
标题翻译：锂电池基于锂化过渡金属钛酸盐
公开(公告)号：US06720112B2
公开(公告)日：2004-04-13
申请号：US09969440
申请日：2001-10-02
申请人： Jeremy Barker , M. Yazid Saidi , Jeffrey L. Swoyer
发明人： Jeremy Barker , M. Yazid Saidi , Jeffrey L. Swoyer
IPC分类号： H01M448
CPC分类号： H01M4/485 , C01G23/003 , C01G31/006 , C01G45/006 , C01G49/009 , C01G51/42 , C01G53/42 , C01P2002/32 , C01P2002/72 , C01P2002/76 , C01P2002/77 , C01P2004/41 , C01P2006/40 , C01P2006/60 , H01M4/136 , H01M4/5825 , H01M4/587 , H01M10/0525 , H01M10/446
摘要： An electrochemical active material contains a lithiated zirconium, titanium, or mixed titanium/zirconium oxide. The oxide can be represented by the formula LiM′M″XO4, where M′ is a transition metal, M″ is an optional three valent non-transition metal, and X is zirconium, titanium, or a combination of the two. Preferably, M′ is nickel, cobalt, iron, manganese, vanadium, copper, chromium, molybdenum, niobium, or combinations thereof. The active material provides a useful composite electrode when combined with a polymeric binder and electrically conductive material. The active material can be made into a cathode for use in a secondary electrochemical cell. Rechargeable batteries may be made by connecting a number of such electrochemical cells.
摘要翻译：电化学活性材料含有锂化锆，钛或混合的钛/锆氧化物。氧化物可以由式LiM'M'XO4表示，其中M'是过渡金属，M“是任选的三价非过渡金属，X是锆，钛或两者的组合。优选地，M'是镍，钴，铁，锰，钒，铜，铬，钼，铌或其组合。当与聚合物粘合剂和导电材料组合时，活性材料提供有用的复合电极。活性材料可以制成用于二次电化学电池的阴极。可以通过连接多个这样的电化学电池来制造可充电电池。

75. 发明授权

US06720110B2 Lithium-containing phosphates, method of preparation, and uses thereof 有权
标题翻译：含锂磷酸盐，制备方法及其用途
公开(公告)号：US06720110B2
公开(公告)日：2004-04-13
申请号：US09776843
申请日：2001-02-05
申请人： Jeremy Barker , M. Yazid Saidi
发明人： Jeremy Barker , M. Yazid Saidi
IPC分类号： H01M458
CPC分类号： H01M10/0525 , C01B25/45 , H01M4/0459 , H01M4/5825 , H01M10/05 , H01M2004/027 , H01M2004/028
摘要： The invention provides an electrochemical cell which comprises a first electrode and a second electrode which is a counter electrode to said first electrode. The first electrode comprises a phosphorous compound of the nominal general formula Li3E′aE″b(PO4)3, desirably at least one E is a metal; and preferably, Li3M′M″(PO4)3. E′ and E″ are the same or different from one another. Where E′ and E″ are the same, they are preferably metals having more than one oxidation state. Where E′ and E″ are different from one another, they are preferably selected from the group of metals where at least one of E′ and E″ has more than one oxidation state.
摘要翻译：本发明提供了一种电化学电池，其包括第一电极和作为与所述第一电极相对的电极的第二电极。第一电极包括标称通式为Li 3 E''E'b（PO 4）3的磷化合物，理想的是至少一个E是金属; 优选Li 3 M'M“（PO 4）3。 E'和E“彼此相同或不同。当E'和E“相同时，它们优选为具有多于一种氧化态的金属。其中E'和E“彼此不同，它们优选选自E'和E”中的至少一个具有多于一个氧化态的金属组。

76. 发明授权

US06702961B2 Preparation of lithium-containing materials 有权
标题翻译：含锂材料的制备
公开(公告)号：US06702961B2
公开(公告)日：2004-03-09
申请号：US10461842
申请日：2003-06-13
申请人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
发明人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
IPC分类号： H01M458
CPC分类号： H01M4/5825 , C01B25/37 , C01B25/45 , C01G21/00 , C01G31/00 , C01G39/00 , C01P2006/40 , H01M4/13 , H01M4/131 , H01M4/136 , H01M4/1391 , H01M4/1397 , H01M4/485 , H01M4/505 , H01M4/525 , H01M4/582 , H01M6/40 , H01M10/052 , H01M10/0525 , H01M10/0566 , Y10T29/10 , Y10T156/1002
摘要： The invention provides novel lithium-mixed metal materials which, upon electrochemical interaction, release lithium ions, and are capable of reversibly cycling lithium ions. The invention provides a rechargeable lithium battery which comprises an electrode formed from the novel lithium-mixed metal materials. Methods for making the novel lithium-mixed metal materials and methods for using such lithium-mixed metal materials in electrochemical cells are also provided. The lithium-mixed metal materials comprise lithium and at least one other metal besides lithium. Preferred materials are lithium-mixed metal phosphates which contain lithium and two other metals besides lithium.
摘要翻译：本发明提供新的锂混合金属材料，其在电化学相互作用时释放锂离子，并且能够可逆地循环锂离子。本发明提供一种可再充电锂电池，其包括由新型锂混合金属材料形成的电极。还提供了制备新的锂复合金属材料的方法和在电化学电池中使用这种锂混合金属材料的方法。锂混合金属材料除锂之外还包含锂和至少一种其它金属。优选的材料是除了锂之外还含有锂和另外两种金属的锂混合金属磷酸盐。

77. 发明授权

US06387568B1 Lithium metal fluorophosphate materials and preparation thereof 有权
标题翻译：锂金属氟磷酸盐材料及其制备
公开(公告)号：US06387568B1
公开(公告)日：2002-05-14
申请号：US09559861
申请日：2000-04-27
申请人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
发明人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
IPC分类号： H01M458
CPC分类号： H01M4/136 , C01B25/455 , H01M4/58 , H01M4/5825 , H01M10/0525 , H01M2004/028
摘要： The invention provides new and novel lithium-metal-fluorophosphates which, upon electrochemical interaction, release lithium ions, and are capable of reversibly cycling lithium ions. The invention provides a rechargeable lithium battery which comprises an electrode formed from the novel lithium-metal-fluorophosphates. The lithium-metal-fluorophosphates comprise lithium and at least one other metal besides lithium.
摘要翻译：本发明提供了新的和新型的锂 - 金属 - 氟磷酸盐，其在电化学相互作用时释放锂离子，并且能够可逆地循环锂离子。本发明提供一种可充电锂电池，其包括由新型锂金属 - 氟磷酸盐形成的电极。除了锂之外，锂金属 - 氟磷酸盐还包含锂和至少一种其它金属。

78. 发明授权

US06203946B1 Lithium-containing phosphates, method of preparation, and uses thereof 有权
公开(公告)号：US06203946B1
公开(公告)日：2001-03-20
申请号：US09204944
申请日：1998-12-03
申请人： Jeremy Barker , M. Yazid Saidi
发明人： Jeremy Barker , M. Yazid Saidi
IPC分类号： H01M458
CPC分类号： H01M10/0525 , C01B25/45 , H01M4/0459 , H01M4/5825 , H01M10/05 , H01M2004/027 , H01M2004/028
摘要： The invention provides an electrochemical cell which comprises a first electrode and a second electrode which is a counter electrode to said first electrode. The first electrode comprises a phosphorous compound of the nominal general formula Li3E′aE″b(PO4)3, desirably at least one E is a metal; and preferably, Li3M′M″(PO4)3. E′ and E″ are the same or different from one another. Where E′ and E″ are the same, they are preferably metals having more than one oxidation state. Where E′ and E″ are different from one another, they are preferably selected from the group of metals where at least one of E′ and E″ has more than one oxidation state.

79. 发明授权

US5869207A Stabilized electrochemical cell 失效
标题翻译：稳定电化学电池
公开(公告)号：US5869207A
公开(公告)日：1999-02-09
申请号：US762081
申请日：1996-12-09
申请人： M. Yazid Saidi , Chariclea Scordilis-Kelley , Jeremy Barker
发明人： M. Yazid Saidi , Chariclea Scordilis-Kelley , Jeremy Barker
IPC分类号： C01G45/00 , H01M4/50 , H01M4/505 , H01M4/62 , H01M10/0525 , H01M10/0567 , H01M10/36
CPC分类号： H01M4/505 , C01G45/1221 , C01G45/1242 , H01M10/0567 , H01M4/62 , C01P2006/40 , H01M10/0525
摘要： The present invention provides a novel composition and method for preventing decomposition of one or more electrochemical cell components comprising an electrode having an active material, and an electrolyte. The method of the invention, for the first time, effectively overcomes problems which arise between the interaction of cell components and contaminate water retained in a cell. Such contaminate water reacts with the electrolyte which comprises a salt of lithium in a solvent. Solubilizing of the salt in solution with attendant interaction between the salt and water causes formation of hydrogen-containing acids. The method of the invention effectively blocks decomposition of a lithium metal oxide cathode active material, and particularly lithium manganese oxide (LMO, nominally LiMn.sub.2 O.sub.4). Such decomposition is prevented by including in the cell a basic compound which forms an electron donor species in the electrolyte solution; and by neutralizing at least a portion of the acid by reacting the donor species with the hydrogen-containing acids thereby preventing decomposition of the lithium manganese oxide by the acid. The preservation of the lithium manganese oxide prevents degradation of other cell components by other mechanism.
摘要翻译：本发明提供一种用于防止一种或多种电化学电池元件分解的新型组合物和方法，所述电化学电池组件包括具有活性材料的电极和电解质。本发明的方法第一次有效地克服了细胞成分的相互作用和污染细胞中残留的水之间产生的问题。这种污染水与包含锂在溶剂中的盐的电解质反应。溶解盐中的盐与盐和水之间伴随的相互作用引起含氢酸的形成。本发明的方法有效地阻止锂金属氧化物正极活性物质，特别是锰酸锂（LMO，名义上是LiMn 2 O 4）的分解。通过在电解液中包含在电解质溶液中形成电子供体物质的碱性化合物来防止这种分解; 并且通过使供体物质与含氢酸反应从而中和酸的至少一部分，从而防止酸分解锰酸锂。锂锰氧化物的保存通过其他机理防止其他电池组分的降解。

80. 发明授权

US5789110A Cathode-active material blends comprising Li.sub.x Mn.sub.2 O.sub.4 (0<x.ltoreq.2) 失效
标题翻译：包含LixMn2O4（0
公开(公告)号：US5789110A
公开(公告)日：1998-08-04
申请号：US723241
申请日：1996-09-27
申请人： Mohamed-Yazid Saidi , Jeremy Barker , Eileen S. Saidi
发明人： Mohamed-Yazid Saidi , Jeremy Barker , Eileen S. Saidi
IPC分类号： H01M4/131 , H01M4/133 , H01M4/36 , H01M4/48 , H01M4/485 , H01M4/50 , H01M4/505 , H01M4/52 , H01M4/525 , H01M4/58 , H01M4/587 , H01M10/0525 , H01M10/0565 , H01M10/058 , H01M10/36
CPC分类号： H01M4/485 , H01M10/0525 , H01M10/058 , H01M4/364 , H01M4/505 , H01M4/525 , H01M4/5825 , H01M4/587 , H01M10/0565 , H01M4/131 , H01M4/133 , Y02T10/7011
摘要： A solid secondary lithium electrochemical cell comprises a physical mixture of Li.sub.x n.sub.2 O.sub.4 (spinel) (0
摘要翻译：固体二次锂电化学电池包括Lixn2O4（尖晶石）（0

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