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81. 发明授权

US06933257B2 Sol-gel derived porous microcomposite of perfluorinated ion-exchange polymer and metal oxide 失效
公开(公告)号：US06933257B2
公开(公告)日：2005-08-23
申请号：US10680334
申请日：2003-10-07
申请人： Mark Andrew Harmer , Qun Sun
发明人： Mark Andrew Harmer , Qun Sun
IPC分类号： C08J5/20 , B01J21/08 , B01J31/08 , B01J31/10 , B01J31/16 , B01J31/24 , B01J31/40 , B01J35/10 , C07B61/00 , C07C2/02 , C07C2/08 , C07C2/66 , C07C5/22 , C07C5/25 , C07C11/02 , C07C15/46 , C07C41/30 , C07C45/46 , C07C49/784 , C07C67/04 , C07C69/145 , C07C201/08 , C07C205/06 , C08G65/02 , C08G65/20 , B01J20/34 , B01J20/26
CPC分类号： B01J21/08 , B01J31/10 , B01J31/165 , B01J31/2419 , B01J31/4007 , B01J35/10 , B01J35/1019 , B01J35/1023 , B01J35/1038 , B01J35/1042 , B01J35/1047 , B01J35/1057 , B01J35/1061 , B01J35/1066 , B01J35/1071 , B01J35/109 , B01J2231/10 , B01J2231/323 , B01J2231/4205 , B01J2231/52 , B01J2231/54 , B01J2531/38 , B01J2531/821 , B01J2531/825 , B01J2531/842 , B01J2531/847 , C07C2/02 , C07C2/66 , C07C5/2266 , C07C5/2273 , C07C5/2562 , C07C41/30 , C07C45/46 , C07C67/04 , C07C201/08 , C07C2521/04 , C07C2521/06 , C07C2521/08 , C07C2521/12 , C07C2523/10 , C07C2523/14 , C07C2523/26 , C07C2523/28 , C07C2523/745 , C07C2531/08 , C07C2531/10 , C07C2531/20 , C07C2531/26 , C07C2531/34 , Y02P20/584 , C07C11/02 , C07C49/784 , C07C69/013 , C07C69/14 , C07C205/06 , C07C43/263
摘要： Porous microcomposites have been prepared from perfluorinated ion-exchange polymer and metal oxides such as silica using the sol-gel process. Such microcomposites possess high surface area and exhibit extremely high catalytic activity.

82. 发明授权

US06784331B2 Sol-gel derived porous microcomposite of perfluorinated ion-exchange polymer and metal oxide 失效
公开(公告)号：US06784331B2
公开(公告)日：2004-08-31
申请号：US10680816
申请日：2003-10-07
申请人： Mark Andrew Harmer , Qun Sun
发明人： Mark Andrew Harmer , Qun Sun
IPC分类号： C07C1328
CPC分类号： B01J21/08 , B01J31/10 , B01J31/165 , B01J31/2419 , B01J31/4007 , B01J35/10 , B01J35/1019 , B01J35/1023 , B01J35/1038 , B01J35/1042 , B01J35/1047 , B01J35/1057 , B01J35/1061 , B01J35/1066 , B01J35/1071 , B01J35/109 , B01J2231/10 , B01J2231/323 , B01J2231/4205 , B01J2231/52 , B01J2231/54 , B01J2531/38 , B01J2531/821 , B01J2531/825 , B01J2531/842 , B01J2531/847 , C07C2/02 , C07C2/66 , C07C5/2266 , C07C5/2273 , C07C5/2562 , C07C41/30 , C07C45/46 , C07C67/04 , C07C201/08 , C07C2521/04 , C07C2521/06 , C07C2521/08 , C07C2521/12 , C07C2523/10 , C07C2523/14 , C07C2523/26 , C07C2523/28 , C07C2523/745 , C07C2531/08 , C07C2531/10 , C07C2531/20 , C07C2531/26 , C07C2531/34 , Y02P20/584 , C07C11/02 , C07C49/784 , C07C69/013 , C07C69/14 , C07C205/06 , C07C43/263
摘要： Porous microcomposites have been prepared from perfluorinated ion-exchange polymer and metal oxides such as silica using the sol-gel process. Such microcomposites possess high surface area and exhibit extremely high catalytic activity.

83. 发明申请

US20030176729A1 Sol-gel derived porous microcomposite of perfluorinated ion-exchange polymer and metal oxide 失效
公开(公告)号：US20030176729A1
公开(公告)日：2003-09-18
申请号：US10322786
申请日：2002-12-18
发明人： Mark Andrew Harmer , Qun Sun
IPC分类号： C07C21/08 , C07C067/04 , B01J031/00
CPC分类号： B01J21/08 , B01J31/10 , B01J31/165 , B01J31/2419 , B01J31/4007 , B01J35/10 , B01J35/1019 , B01J35/1023 , B01J35/1038 , B01J35/1042 , B01J35/1047 , B01J35/1057 , B01J35/1061 , B01J35/1066 , B01J35/1071 , B01J35/109 , B01J2231/10 , B01J2231/323 , B01J2231/4205 , B01J2231/52 , B01J2231/54 , B01J2531/38 , B01J2531/821 , B01J2531/825 , B01J2531/842 , B01J2531/847 , C07C2/02 , C07C2/66 , C07C5/2266 , C07C5/2273 , C07C5/2562 , C07C41/30 , C07C45/46 , C07C67/04 , C07C201/08 , C07C2521/04 , C07C2521/06 , C07C2521/08 , C07C2521/12 , C07C2523/10 , C07C2523/14 , C07C2523/26 , C07C2523/28 , C07C2523/745 , C07C2531/08 , C07C2531/10 , C07C2531/20 , C07C2531/26 , C07C2531/34 , Y02P20/584 , C07C11/02 , C07C49/784 , C07C69/013 , C07C69/14 , C07C205/06 , C07C43/263
摘要： Porous microcomposites have been prepared from perfluorinated ion-exchange polymer and metal oxides such as silica using the sol-gel process. Such microcomposites possess high surface area and exhibit extremely high catalytic activity.

84. 发明申请

US20020022733A1 Synthesis of ruthenium of osmium metathesis catalysts 有权
标题翻译：锇复分解催化剂钌的合成
公开(公告)号：US20020022733A1
公开(公告)日：2002-02-21
申请号：US09967198
申请日：2001-09-28
申请人： California Institute of Technology
发明人： Robert H. Grubbs , Tomas R. Belderrain , Seth N. Brown , Thomas E. Wilhelm
IPC分类号： C07F015/00
CPC分类号： B01J31/2404 , B01J31/2265 , B01J31/2295 , B01J31/24 , B01J2231/14 , B01J2231/54 , B01J2231/543 , B01J2531/821 , B01J2531/825 , C07F15/002 , C07F15/0046
摘要： The present invention relates to the synthesis of highly active ruthenium and osmium carbene metathesis catalyst in good yield from readily available starting materials. The catalysts that may be synthesized are of the general formula 1 wherein: M is ruthenium or osmium; X and X1 are independently any anionic ligand; L and L1 are any neutral electron donor ligand; and, R and R1 are each hydrogen or one of the following substituent groups: C2-C20 alkenyl, C2-C20 alkynyl, C1-C20 alkyl, aryl, C1-C20 carboxylate, C1-C20 alkoxy, C2-C20 alkenyloxy, C2-C20 alkynyloxy, aryloxy, C2-C20 alkoxycarbonyl, C1-C20 alkylthio, C1-C20 alkylsulfonyl and C1-C20 alkylsulfinyl. Optionally, the substituent group may be substituted with one or more groups selected from C1-C5 alkyl, halogen, C1-C5alkoxy, and aryl. When the substitute aryl group is phenyl, it may be further substituted with one or more groups selected from a halogen, a C1-C5 alkyl, or a C1-C5 alkoxy. Specific synthetic protocols for vinyl alkylidene catalysts wherein R is hydrogen and R1 is nullCHCR12R13 and non-vinyl alkylidene catalysts are also disclosed. In addition to the ease of synthesis (typically a one-step synthesis), the reactions generally may be run at or above room temperature and the resulting products usually may be used without extensive post synthesis purification.
摘要翻译：本发明涉及从容易获得的原料合成高活性钌和碳卡因复分解催化剂的良好产率。可以合成的催化剂具有以下通式：其中：M是钌或锇; X和X1独立地为任何阴离子配体; L和L1是任何中性电子给体配体; C 1 -C 20烷基，C 1 -C 20烷基，C 1 -C 20烷基，C 1 -C 20羧酸酯，C 1 -C 20烷氧基，C 2 -C 20链烯氧基，C 2 -C 20炔基， C20炔氧基，芳氧基，C2-C20烷氧基羰基，C1-C20烷硫基，C1-C20烷基磺酰基和C1-C20烷基亚磺酰基。任选地，取代基可以被一个或多个选自C 1 -C 5烷基，卤素，C 1 -C 5烷氧基和芳基的基团取代。当取代芳基为苯基时，可以进一步被一个或多个选自卤素，C 1 -C 5烷基或C 1 -C 5烷氧基的基团取代。还公开了其中R为氢且R 1为-CHCR 12 R 13的乙烯基亚烷基催化剂和非乙烯基亚烷基催化剂的具体合成方案。除了易于合成（通常是一步合成）之外，反应通常可以在室温或更高的温度下进行，所得产物通常可以在没有广泛的后合成纯化的情况下使用。

85. 发明专利

TW201233441A 烯烴置換方法及包含鎢氟鍵之催化劑 OLEFIN METATHESIS PROCESS AND CATALYST CONTAINING TUNGSTEN FLUORINE BONDS 失效
简体标题：烯烃置换方法及包含钨氟键之催化剂 OLEFIN METATHESIS PROCESS AND CATALYST CONTAINING TUNGSTEN FLUORINE BONDS
公开(公告)号：TW201233441A
公开(公告)日：2012-08-16
申请号：TW100148707
申请日：2011-12-26
申请人：環球油類產品有限公司
发明人：陶菲克摩斯塔法 , 瑪佐爾艾提恩 , 尼可拉斯克理司多佛P , 巴塞特珍瑪莉
IPC分类号： B01J , C07C
CPC分类号： C07C6/04 , B01J21/08 , B01J31/122 , B01J35/1014 , B01J35/1019 , B01J37/031 , B01J37/035 , B01J2231/54 , B01J2531/66 , C07C2531/22 , Y02P20/52 , Y02P30/42 , C07C11/06
摘要：本發明已研發出通常且尤其用於自乙烯及丁烯產生丙烯之烯烴置換之方法及催化劑。該催化劑含有包含至少一個鎢-氟鍵之鎢金屬化合物，其分散或接枝於載體上。該催化劑之具體實例係接枝於二氧化矽載體上之化合物WOF(CH2CMe3)3。
简体摘要：本发明已研发出通常且尤其用于自乙烯及丁烯产生丙烯之烯烃置换之方法及催化剂。该催化剂含有包含至少一个钨-氟键之钨金属化合物，其分散或接枝于载体上。该催化剂之具体实例系接枝于二氧化硅载体上之化合物WOF(CH2CMe3)3。

86. 发明专利

TW461891B 與雜環碳烯類之金屬錯合物失效
简体标题：与杂环碳烯类之金属错合物
公开(公告)号：TW461891B
公开(公告)日：2001-11-01
申请号：TW084112914
申请日：1995-12-05
申请人：西蘭尼斯公司
发明人：賀曼 , 艾利生 , 菲斯查爾 , 科查爾 , 歐菲爾
IPC分类号： C07F
CPC分类号： C07F15/0086 , B01J31/2265 , B01J31/2273 , B01J31/2295 , B01J2231/54 , B01J2531/822 , B01J2531/824 , B01J2531/827 , B01J2531/828 , C07F15/002 , C07F15/0033 , C07F15/0046 , C07F15/006 , C07F15/0073
摘要：本發明係關於周期表第8、9、10族元素，與雜環碳烯類做為配合基之新穎錯合物。
简体摘要：本发明系关于周期表第8、9、10族元素，与杂环碳烯类做为配合基之新颖错合物。

87. 发明专利

TW201605540A 穩定之錸系異相催化劑及其應用审中-公开
简体标题：稳定之铼系异相催化剂及其应用
公开(公告)号：TW201605540A
公开(公告)日：2016-02-16
申请号：TW104125214
申请日：2015-08-04
申请人： SCG化學股份有限公司 , SCG CHEMICALS COMPANY LIMITED
发明人：蘇里葉康奇特 , SURIYE, KONGKIAT , 馮沙瓦特維那 , PHONGSAWAT, WEENA , 珍沙瑞蘇克安納特 , JANTHARASUK, AMNART
IPC分类号： B01J35/02 , B01J23/36 , B01J33/00 , B01J19/18 , B01J8/02 , C07C6/04 , C07C11/06
CPC分类号： B01J23/36 , B01J2231/54 , C07C6/04 , C07C2521/04 , C07C2521/06 , C07C2521/16 , C07C2521/18 , C07C2523/08 , C07C2523/14 , C07C2523/36 , C07C2527/04 , C07C2527/22 , C07C2529/06 , C07C2531/12 , Y02P20/52 , C07C11/06
摘要：本發明係關於一種穩定之錸系異相催化劑，其係由一製程所獲得，該製程包含將一錸系異相催化劑與一穩定劑於0至100℃之溫度下接觸，該穩定劑包含一脂族烴化合物；以及其應用。
简体摘要：本发明系关于一种稳定之铼系异相催化剂，其系由一制程所获得，该制程包含将一铼系异相催化剂与一稳定剂于0至100℃之温度下接触，该稳定剂包含一脂族烃化合物；以及其应用。

88. 发明授权

US09713808B2 Highly Z-selective olefin metathesis 有权
公开(公告)号：US09713808B2
公开(公告)日：2017-07-25
申请号：US14797834
申请日：2015-07-13
申请人： Massachusetts Institute of Technology , Trustees of Boston College
发明人： Richard R. Schrock , Annie J. King , Yu Zhao , Margaret M. Flook , Amir H. Hoveyda
IPC分类号： C07F11/00 , B01J31/18 , B01J31/22 , C07C6/04 , C07C41/30 , C07C67/475 , C07C209/68 , C07C303/40 , C07F7/08 , C07C209/64 , C07F5/02
CPC分类号： B01J31/2295 , B01J31/1805 , B01J31/181 , B01J31/1825 , B01J31/2226 , B01J31/2265 , B01J31/2278 , B01J2231/54 , B01J2231/543 , B01J2531/0266 , B01J2531/0288 , B01J2531/64 , B01J2531/66 , B01J2540/225 , B01J2540/40 , C07B2200/09 , C07C6/04 , C07C41/30 , C07C67/475 , C07C209/64 , C07C209/68 , C07C303/40 , C07C2531/18 , C07C2531/22 , C07C2601/14 , C07C2601/16 , C07C2602/10 , C07F5/025 , C07F7/083 , C07F11/00 , C07F11/005 , C07C13/28 , C07C11/02 , C07C15/50 , C07C43/166 , C07C69/593 , C07C311/18 , C07C211/53
摘要： The present invention relates generally to catalysts and processes for the Z-selective formation of internal olefin(s) from terminal olefin(s) via homo-metathesis reactions.

89. 发明授权

US09481627B2 Methods for suppressing isomerization of olefin metathesis products 有权
公开(公告)号：US09481627B2
公开(公告)日：2016-11-01
申请号：US14840679
申请日：2015-08-31
申请人： Elevance Renewable Sciences, Inc.
发明人： Bruce E. Firth , Sharon E. Kirk
IPC分类号： C07C51/31 , C07C7/20 , C11B1/10 , C11B3/00 , C11C3/10 , C07C51/50 , C11B5/00
CPC分类号： C07C51/313 , B01J2231/54 , C07C7/20 , C07C51/50 , C11B1/10 , C11B3/006 , C11B5/00 , C11B5/0007 , C11B5/0014 , C11B5/0028 , C11C3/10 , Y10S502/52 , C07C11/02
摘要： A method for suppressing isomerization of an olefin metathesis product produced in a metathesis reaction includes adding an isomerization suppression agent to a mixture that includes the olefin metathesis product and residual metathesis catalyst from the metathesis reaction under conditions that are sufficient to passivate at least a portion of the residual metathesis catalyst. The isomerization suppression agent includes (i) a salt and/or an ester of a phosphorous oxo acid, and/or (ii) a derivative of the phosphorous oxo acid in which at least one P—H bond has been replaced by a P—C bond, and/or (iii) a salt and/or an ester of the derivative. Methods of refining natural oils are described.

90. 发明授权

US09409850B2 Metathesis depolymerization using acrylates 有权
标题翻译：使用丙烯酸酯的复分解聚
公开(公告)号：US09409850B2
公开(公告)日：2016-08-09
申请号：US14422740
申请日：2013-08-20
申请人： UNIVERSITY OF FLORIDA RESEARCH FOUNDATION, INC.
发明人： Kenneth Boone Wagener , Michael Schulz
IPC分类号： C07C51/60 , C07C57/04 , C07C67/475 , C08F236/02 , C08F8/50 , B01J31/12
CPC分类号： C07C51/60 , B01J31/2265 , B01J31/2273 , B01J31/2278 , B01J31/24 , B01J2231/54 , B01J2531/821 , C07C4/22 , C07C51/62 , C07C67/475 , C08F236/02 , C07C69/602 , C07C57/66 , C07C69/593
摘要： Olefin metathesis between an acrylate monomer and a polyene comprising molecule or polymer is employed as a method of cross-metathesizing or depolymerizing the molecule. The metathesis reaction forms a telechelic acrylate molecule that is a monomer, oligomer or polymer. The telechelic acrylate molecule can be employed as a monomer for condensation polymerization.
摘要翻译：使用丙烯酸酯单体和含多烯的分子或聚合物之间的烯烃复分解作为分子的交叉分解或解聚的方法。复分解反应形成作为单体，低聚物或聚合物的遥爪丙烯酸酯分子。丙烯酸遥爪分子可用作缩聚单体。

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