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81. 发明授权

US4921505A Process for the preparation of new crystal modification of an azo dyestuff 失效
标题翻译：制备偶氮染料新结晶改性的方法
公开(公告)号：US4921505A
公开(公告)日：1990-05-01
申请号：US283470
申请日：1988-12-12
申请人： Gunther Effenberger , Hubert Kruse
发明人： Gunther Effenberger , Hubert Kruse
IPC分类号： C09B67/48 , C09B67/00 , C09B67/10 , D06P1/18
CPC分类号： C09B67/0015 , C09B67/0029 , Y10S8/922 , Y10S8/924
摘要： In the process for the preparation of the dyestuff of the formula I ##STR1## by diazotization and coupling, the aqueous suspension present when the coupling has ended is heated to temperatures of 50.degree. C. up to the boiling point of the aqueous phase in the presence of a dispersing agent.
摘要翻译：在通过重氮化和偶联制备式I的染料的方法中，当偶联已经结束时存在的水性悬浮液被加热到50℃的温度直至水溶液的沸点在分散剂存在下进行。

82. 发明授权

US4460375A Dyeing-stable monoazo dyestuff, a process for its preparation, and its use 失效
标题翻译：染色稳定的单偶氮染料，其制备方法及其用途
公开(公告)号：US4460375A
公开(公告)日：1984-07-17
申请号：US551271
申请日：1983-11-14
申请人： Karl Sommer , Manfred Schneider , Rudolf Schickfluss
发明人： Karl Sommer , Manfred Schneider , Rudolf Schickfluss
IPC分类号： C09B67/48 , C09B29/08 , C09B29/085 , C09B67/00 , C09B67/10
CPC分类号： C09B29/081 , C09B29/0834 , C09B67/0015 , C09B67/0029 , Y10S8/921 , Y10S8/922
摘要： A dyeing-stable modification (.beta.-modification) of the dyestuff of the formula (I) ##STR1## which has the X-ray diffraction diagram shown in FIG. 1 and having the characteristic reflections at the following glancing angles and relative intensities:______________________________________ [.theta.] 2.74 4.27 4.70 5.50 8.74 11.24 12.44 relative 100 72 40 23 27 32 26 intensity ______________________________________ a process for its preparation by heating the dyestuff of said formula (I) of the dyeing-unstable .alpha.-modification, characterized by an X-ray diffraction diagram having the characteristic reflections at the following glancing angles and relative intensities______________________________________ [.theta.] 3.55 4.15 5.35 9.45 10.41 12.71 13.89 relative 42 100 35 24 34 94 48 intensity ______________________________________ at temperatures of 60.degree. to 120.degree. C. in an organic solvent, and its use for dyeing fiber materials made of cellulose esters or synthetic linear polyesters.
摘要翻译：具有图1所示的X射线衍射图的式（I）染料的染色稳定性改性（β-改性）图像（I）。具有以下扫掠角度和相对强度的特征反射：-θ2.74 4.27 4.70 5.50 8.74 11.24 12.44相对100 72 40 23 27 32 26 - 强度 - 通过加热所述式（I）染色不稳定的α-改性，其特征在于具有以下扫掠角度的特征反射和相对强度的X射线衍射图-θ3.55 4.15 5.35 9.45 10.41 12.71 13.89相对值42 100 35 24 34 94 48-密度 - 在有机溶剂中在60℃至120℃的温度下，以及其用于由纤维素酯或合成线性聚酯制成的纤维材料的染色用途。

83. 发明授权

US4327999A Disperse dye stable to dyeing, and its use for dyeing synthetic and semi-synthetic fibre materials 失效
标题翻译：分散染料稳定染色，用于染色合成纤维和半合成纤维材料
公开(公告)号：US4327999A
公开(公告)日：1982-05-04
申请号：US221596
申请日：1980-12-31
申请人： Stefan Koller , Peter Eugster , Suresh C. Agarwal
发明人： Stefan Koller , Peter Eugster , Suresh C. Agarwal
IPC分类号： C09B29/085 , C09B29/08 , C09B67/00 , C09B67/10 , C09B67/48
CPC分类号： C09B67/0015 , C09B29/0813 , C09B67/0029
摘要： It is possible by heating at temperatures of between 65.degree. and 200.degree. C. to convert the known .alpha.-modification of the azo dye of the formula ##STR1## which is unstable to dyeing, completely into the .beta.-modification which is stable to dyeing. The modification transformation can be performed either with the solid dye or with a suspension thereof in an organic, preferably aromatic, solvent.The novel dye modification is stable in dispersion under dyeing conditions, and shows no tendency to flocculate.
摘要翻译：可以通过在65℃和200℃之间的温度下加热而将对染色不稳定的式“IMAGE”的偶氮染料的已知α-改性完全转化成对染色稳定的β-修饰。改性转化可以用固体染料或其悬浮液在有机，优选芳族溶剂中进行。新型染料改性在染色条件下分散稳定，不发生絮凝倾向。

84. 发明申请

US20100178607A1 Method for the Production of Pure C.I. Pigment Orange 74 失效
标题翻译：纯C.I.生产方法颜料橙74
公开(公告)号：US20100178607A1
公开(公告)日：2010-07-15
申请号：US12663637
申请日：2008-05-21
申请人： Thomas Hundsdorf , Willi Rauschmann
发明人： Thomas Hundsdorf , Willi Rauschmann
IPC分类号： C09B67/54 , C09D7/12 , C09D11/02 , G03G9/09
CPC分类号： C09B67/0015 , C09B67/0002 , C09B67/0089 , C09B67/0096 , C09D7/41 , C09D11/322
摘要： The invention relates to a method for conditioning and purifying pigment orange 74. The method is characterized in that the aqueous suspension of the raw pigment, optionally after adding an organic solvent from the group comprising isobutanol, chlorobenzene and o-dichlorobenzene, is subjected to a finishing treatment, the organic solvent is optionally removed using a distillation process, the remaining aqueous pigment suspension is mixed with a non-ionic surfactant and is heated to a temperature ranging from 30 to 100° C. and the pigment is then filtered off.
摘要翻译：本发明涉及一种用于调理和纯化颜料橙74的方法。该方法的特征在于，任选地在从异丁醇，氯苯和邻二氯苯组中加入有机溶剂之后，将原料颜料的水悬浮液经受使用蒸馏方法任选地除去有机溶剂，将剩余的水性颜料悬浮液与非离子表面活性剂混合并加热至30至100℃的温度，然后滤出颜料。

85. 发明申请

US20090241800A1 METHOD OF PRODUCING AN ORGANIC PIGMENT FINE PARTICLE DISPERSION, AND INK-JET RECORDING INK AND PAINT USING THE ORGANIC PIGMENT FINE PARTICLE OBTAINED BY THE SAME 审中-公开
标题翻译：生产有机颜料微粒分散体的方法，以及使用由其获得的有机颜料微粒的喷墨记录油墨和油漆
公开(公告)号：US20090241800A1
公开(公告)日：2009-10-01
申请号：US12407384
申请日：2009-03-19
申请人： Hirokazu Kyota
发明人： Hirokazu Kyota
IPC分类号： C09D11/02 , C04B16/00
CPC分类号： C09B67/0091 , C09B67/0014 , C09B67/0015 , C09B67/0086 , C09B67/009 , C09B67/0096 , C09D7/41 , C09D7/80 , C09D11/322
摘要： A method of producing an organic pigment fine particle dispersion, including feeding at least three liquids, which are a solution containing an organic pigment dissolved in an organic solvent in the presence of an alkali, a solution containing a dispersant, and an aqueous medium, into separate channels and bringing the at least three liquids into junction with each other in a channel simultaneously to produce fine particles of the organic pigment.
摘要翻译：一种生产有机颜料微粒分散体的方法，包括将至少三种液体进料，所述液体是在碱的存在下含有溶解在有机溶剂中的有机颜料的溶液，含有分散剂和水性介质的溶液，单独的通道并且使至少三种液体在通道中彼此连接以同时产生有机颜料的细颗粒。

86. 发明授权

US07160371B2 Method of improving pigment fluorescence 失效
标题翻译：改善色素荧光的方法
公开(公告)号：US07160371B2
公开(公告)日：2007-01-09
申请号：US11136644
申请日：2005-05-24
申请人： Iain Frank Fraser , Sharon Kathleen Wilson , Ian Alexander Macpherson
发明人： Iain Frank Fraser , Sharon Kathleen Wilson , Ian Alexander Macpherson
IPC分类号： C09K11/00 , C09D5/00
CPC分类号： C09B41/005 , C09B67/0015
摘要： A process for the preparation of organic pigments with enhanced fluorescence, which process comprises treating said pigments with a surfactant, and to the fluorescent organic pigments obtained by said process. The pigments according to the present invention can be used in marking applications, wherein durable fluorescence is required.
摘要翻译：一种制备具有增强荧光的有机颜料的方法，该方法包括用表面活性剂处理所述颜料，以及通过所述方法获得的荧光有机颜料。根据本发明的颜料可用于标记用途，其中需要持久的荧光。

87. 发明授权

US07019121B2 Process for conditioning azo pigments 失效
标题翻译：调节偶氮颜料的方法
公开(公告)号：US07019121B2
公开(公告)日：2006-03-28
申请号：US10751162
申请日：2003-12-31
申请人： Edward H. Sung , George H. Robertson , Humberto A. Velasquez
发明人： Edward H. Sung , George H. Robertson , Humberto A. Velasquez
IPC分类号： C09B67/20 , C09D11/02
CPC分类号： C09B67/0015
摘要： A process for conditioning azo pigment with surfactants of ethoxylate alkyl phenols in the presence of a strong alkali in the aqueous condition.
摘要翻译：一种在水性条件下在强碱存在下用乙氧基化烷基酚表面活性剂处理偶氮颜料的方法。

88. 发明申请

US20050218378A1 Method of improving pigment fluorescence 失效
公开(公告)号：US20050218378A1
公开(公告)日：2005-10-06
申请号：US11136644
申请日：2005-05-24
申请人： Iain Fraser , Sharon Wilson , Ian Macpherson
发明人： Iain Fraser , Sharon Wilson , Ian Macpherson
IPC分类号： C09K11/06 , C09B35/033 , C09B35/10 , C09B41/00 , C09B67/00 , C09B67/08 , C09B67/10 , C09B67/20 , C09D11/00
CPC分类号： C09B41/005 , C09B67/0015
摘要： A process for the preparation of organic pigments with enhanced fluorescence, which process comprises treating said pigments with a surfactant, and to the fluorescent organic pigments obtained by said process. The pigments according to the present invention can be used in marking applications, wherein durable fluorescence is required.

89. 发明授权

US06784231B2 Pigment, method for producing pigment, pigment dispersion, and electrostatic image developing powder toner 有权
标题翻译：颜料，颜料的制造方法，颜料分散体和静电图像显影粉末调色剂
公开(公告)号：US06784231B2
公开(公告)日：2004-08-31
申请号：US10100063
申请日：2002-03-19
申请人： Katsunori Shimada , Junko Sunouchi
发明人： Katsunori Shimada , Junko Sunouchi
IPC分类号： C09B3522
CPC分类号： C09B67/0015 , C09B67/0028 , G03G9/091
摘要： A pigment having weak dispersion force to be readily dispersed in a medium to be colored from which an excellent yellow image having superior transparency can be produced. The pigment includes a compound having the same chemical formula as C.I. Pigment Yellow 180. The BET specific surface area based on the nitrogen absorption process of the pigment is 20-100 m2/g, and the ratio of the absolute strength of X-ray diffraction at Bragg angle 2&thgr;=17.5°±0.2° to the absolute strength of X-ray diffraction at Bragg angle 2&thgr;=18.2°±0.2° of the pigment in a powder X-ray diffraction diagram using a CuK&agr; characteristic X-ray is less than 1.8/1.0. The present invention also provides a dispersion including the pigment and a thermoplastic resin having excellent transparency and color strength.
摘要翻译：具有弱分散力的颜料容易分散在待着色的介质中，由此可以制备出具有优异的透明度的黄色图像。颜料包括具有与C.I.相同化学式的化合物。颜料黄180.基于颜料的氮吸收过程的BET比表面积为20-100m 2 / g，布拉格角2θ= 17.5°±0.2°的X射线衍射绝对强度的比例 °与使用CuKalpha特征X射线的粉末X射线衍射图中的颜料的布拉格角2θ= 18.2°±0.2°的X射线衍射的绝对强度小于1.8 / 1.0。本发明还提供了包含颜料和具有优异的透明性和着色强度的热塑性树脂的分散体。

90. 发明授权

US06673906B1 &bgr; modified monoazo dye resistant to dyeing, its preparation and use 失效
标题翻译： β改性单偶氮染料耐染色，其制备和使用
公开(公告)号：US06673906B1
公开(公告)日：2004-01-06
申请号：US08584776
申请日：1996-01-11
申请人： Ulrich Bühler
发明人： Ulrich Bühler
IPC分类号： C09B29085
CPC分类号： C09B43/42 , C09B67/0015 , C09B67/0029
摘要： The present invention relates to the &bgr; modification of the dye of the formula I
摘要翻译：本发明涉及式I染料的β改性

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