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    • 33. 发明申请
    • Nanotube/matrix composites and methods of production and use
    • 纳米管/基体复合材料及其生产和使用方法
    • US20070104947A1
    • 2007-05-10
    • US11357644
    • 2006-02-17
    • Robert Shambaugh
    • Robert Shambaugh
    • B82B3/00D01F1/10D01F6/06D02G3/00
    • B82Y30/00Y10S977/753Y10S977/842Y10T428/2904Y10T428/2913
    • A nanotube/matrix composite mixture, and a method of producing it, which can be used to form a composite material such as a drawn fiber having an increased strength over a drawn fiber formed from the matrix material alone. Nanotubes are combined with a solvent material to form a nanotube/solvent mixture. The nanotube/solvent mixture is mixed, for example by sonication, such that the nanotubes are uniformly dispersed in the nanotube/solvent mixture. An amount of a matrix material (with or without a solvent) is then combined with the nanotube/solvent mixture to form a nanotube/solvent/matrix mixture. The matrix material is polyethylene. The nanotube/solvent mixture and the matrix material are mixed such that the nanotubes are maintained in uniformly dispersed state in the nanotube/solvent/matrix mixture, for example by continued sonication after the nanotubes and matrix material are combined. The solvent material is then substantially removed from the nanotube/solvent/matrix mixture to form the nanotube/matrix composite mixture, which can then be used in a commercial process to produce a composite material such as drawn fiber, as produced, for example, by melt spinning.
    • 纳米管/基质复合混合物及其制造方法,其可用于形成复合材料,例如拉伸纤维,该拉伸纤维的强度比单独由基质材料形成的拉伸纤维强。 将纳米管与溶剂材料组合以形成纳米管/溶剂混合物。 将纳米管/溶剂混合物例如通过超声处理混合,使得纳米管均匀地分散在纳米管/溶剂混合物中。 然后将一定量的基质材料(含或不含溶剂)与纳米管/溶剂混合物组合以形成纳米管/溶剂/基质混合物。 基质材料是聚乙烯。 将纳米管/溶剂混合物和基质材料混合,使得纳米管在纳米管/溶剂/基质混合物中保持均匀分散状态,例如在纳米管和基体材料组合之后通过继续超声处理。 然后将溶剂材料从纳米管/溶剂/基质混合物中基本上除去,形成纳米管/基质复合混合物,然后可将其用于商业过程中,以生产复合材料如拉伸纤维,例如通过 熔融纺丝。
    • 34. 发明授权
    • Syndiotactic polypropylene fibers
    • US07025919B2
    • 2006-04-11
    • US10112520
    • 2002-03-28
    • Mohan GownderJay Nguyen
    • Mohan GownderJay Nguyen
    • D01D5/16D01F6/06
    • D01F6/06
    • A process for the production of partially oriented polypropylene fibers from syndiotactic polypropylene. Syndiotactic polypropylene is heated to a molten state and extruded to form a fiber preform. The fiber preform is spun at a forward spinning speed within the range of about 700–3500 meters per minute to produce a partially oriented fiber. The partially oriented fiber is wound without further substantial orientation of the fiber at a draw ratio of less than 1.5. By operating at a forward spinning speed of about 700 meters per minute or more, the partially oriented fiber has a greater tenacity than would be observed for a fiber formed from a corresponding spun isotactic polypropylene. The fiber preform is spun at a forward spinning speed of at least 100 meters per minute to provide a tenacity on the order of about 2 grams per denier or more. The fiber preform may be spun at a forward spinning speed of at least 1500 meters per minute to provide a tenacity of about 3 grams per denier.