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41. 发明授权

US08168308B2 Compound having pyridoindole ring structure having substituted pyridyl group attached thereto, and organic electroluminescence element 有权
标题翻译：具有连接有取代的吡啶基的吡啶并吲哚环结构的化合物和有机电致发光元件
公开(公告)号：US08168308B2
公开(公告)日：2012-05-01
申请号：US12377908
申请日：2007-08-16
申请人： Norimasa Yokoyama , Shuichi Hayashi , Shigeru Kusano
发明人： Norimasa Yokoyama , Shuichi Hayashi , Shigeru Kusano
IPC分类号： H01L51/54 , C07D471/00
CPC分类号： C09K11/06 , C07D471/04 , C07D519/00 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , C09K2211/1044 , H01L51/0072 , H01L51/0081 , H01L51/5048 , H01L51/5096 , H05B33/14 , Y10S428/917
摘要： The present invention is to provide an organic compound having excellent characteristics as a material for an organic EL device having a high efficiency and a high durability, and to provide an organic EL device having a high efficiency and a high durability by using the compound. The invention relates to a compound having a pyridoindole ring structure having a substituted pyridyl group attached thereto, which is represented by the general formula (1); and to an organic electroluminescent device comprising a pair of electrodes and at least one organic layer interposed between the electrodes, wherein at least one of the organic layer(s) contains the compound: wherein Ar represents a substituted or unsubstituted aromatic hydrocarbon group, a substituted or unsubstituted aromatic heterocyclic group, or a substituted or unsubstituted condensed polycyclic aromatic group; R1 to R10 may be the same or different from one another and each independently represents a hydrogen atom, a fluorine atom, a cyano group, an alkyl group, or a substituted or unsubstituted aromatic hydrocarbon group; Z represents a 6-membered aromatic heterocyclic ring containing one nitrogen atom; and m and n each independently represents an integer of 1 to 3, provided that n is 1 when m is 2 or 3.
摘要翻译：本发明提供一种具有优异特性的有机化合物作为具有高效率和高耐久性的有机EL器件的材料，并且通过使用该化合物来提供具有高效率和高耐久性的有机EL器件。本发明涉及具有通式（1）表示的具有取代的吡啶基的吡啶并吲哚环结构的化合物。以及包含一对电极和介于所述电极之间的至少一个有机层的有机电致发光器件，其中所述有机层中的至少一个含有所述化合物：其中Ar表示取代或未取代的芳族烃基，取代的或未取代的芳族杂环基，或取代或未取代的稠合多环芳基; R 1〜R 10可以相同也可以不同，各自独立地表示氢原子，氟原子，氰基，烷基或取代或未取代的芳香族烃基。 Z表示含有一个氮原子的6元芳族杂环; m和n各自独立地表示1〜3的整数，条件是当m为2或3时n为1。

42. 发明申请

US20120012831A1 COMPOUND HAVING BENZOTRIAZOLE RING STRUCTURE AND ORGANIC ELECTROLUMINESCENT ELEMENT 有权
标题翻译：具有苯并噻唑环结构和有机电致发光元件的化合物
公开(公告)号：US20120012831A1
公开(公告)日：2012-01-19
申请号：US13257142
申请日：2010-03-17
申请人： Norimasa Yokoyama , Shuichi Hayashi , Naoaki Kabasawa , Yoshio Taniguchi , Musubu Ichikawa , Shunji Mochiduki
发明人： Norimasa Yokoyama , Shuichi Hayashi , Naoaki Kabasawa , Yoshio Taniguchi , Musubu Ichikawa , Shunji Mochiduki
IPC分类号： H01L51/54 , C07D401/14
CPC分类号： C07D401/14 , C07D401/04 , C07D401/10 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , C09K2211/1059 , H01L51/0072 , H01L51/5048 , H01L51/5096 , H05B33/10 , H05B33/14
摘要： A compound having a benzotriazole ring structure and a formula (1): wherein Ar is a substituted or unsubstituted aromatic hydrocarbon group, aromatic heterocyclic group, or condensed polycyclic aromatic group; A and B are the same as or different from each other and each represent a hydrogen atom or a monovalent group of formula (2), provided that A and B are not simultaneously hydrogen atoms: wherein R1 to R8 are the same as or different and each represent a hydrogen atom, a deuterium atom, a fluorine atom, a chlorine atom, a cyano group, a trifluoromethyl group, a linear or branched alkyl group having 1 to 6 carbon atoms, aromatic hydrocarbon group, a substituted or unsubstituted aromatic heterocyclic group, or condensed polycyclic aromatic group; m is an integer of 0, 1 or 2; X represents a carbon atom or a nitrogen atom; when X is a nitrogen atom, the nitrogen atom does not have substituents or bonding groups of R1, R2, R3 and R4; and when m is 2, a plurality of R1, R2, R3, R4 and X each are the same or different.
摘要翻译：具有苯并三唑环结构的化合物和式（1）：其中Ar是取代或未取代的芳族烃基，芳族杂环基或缩合多环芳基; A和B彼此相同或不同，并且各自表示氢原子或式（2）的一价基团，条件是A和B不同时为氢原子：其中R1至R8相同或不同，各自表示氢原子，氘原子，氟原子，氯原子，氰基，三氟甲基，具有1〜6个碳原子的直链或支链烷基，芳香族烃基，取代或未取代的芳香族杂环基或缩合多环芳基; m是0,1或2的整数; X表示碳原子或氮原子; 当X是氮原子时，氮原子不具有R 1，R 2，R 3和R 4的取代基或键合基团; 当m为2时，多个R 1，R 2，R 3，R 4和X各自相同或不同。

43. 发明申请

US20110272679A1 COMPOUND HAVING TRIAZOLE RING STRUCTURE TO WHICH PYRIDYL GROUP IS BONDED, AND ORGANIC ELECTROLUMINESCENT DEVICE 审中-公开
标题翻译：具有吡啶基组合的三唑环结构的化合物和有机电致发光器件
公开(公告)号：US20110272679A1
公开(公告)日：2011-11-10
申请号：US13138184
申请日：2010-01-19
申请人： Norimasa Yokoyama , Shuichi Hayashi , Yoshio Taniguchi , Musubu Ichikawa , Shinichi Matsuki
发明人： Norimasa Yokoyama , Shuichi Hayashi , Yoshio Taniguchi , Musubu Ichikawa , Shinichi Matsuki
IPC分类号： H01L51/54 , C07D401/14
CPC分类号： C07D403/14 , C07D401/14 , H01L51/0067 , H01L51/0072 , H01L51/5016
摘要： A host compound for a light emitting layer, which is excellent in electron transporting capability and hole blocking capability, has a high triplet excitation level and is capable of completely confining triplet excitons of a phosphorescent material, is provided as a material for an organic electroluminescent device having a high efficiency, and an organic electroluminescent device having a high efficiency and a high luminance is provided by using this compound.The compound having a triazole ring structure to which a pyridyl group substituted with a carbazolyl group is bonded, is represented by the following general formula (1), and the organic electroluminescent device containing a pair of electrodes and at least one organic layer sandwitched therebetween is characterized in that the compound, which is represented by the following general formula (1) and has a triazole ring structure to which a pyridyl group substituted with a carbazolyl group is bonded, is used as a constitutional material of at least one organic layer in the organic electroluminescent device.
摘要翻译：作为有机电致发光器件的材料，提供了具有优异的电子传输能力和空穴阻断能力的发光层的主体化合物，具有高的三线态激发电平并且能够完全限制磷光材料的三线态激子通过使用该化合物，提供高效率和高亮度的有机电致发光元件。具有由咔唑基取代的吡啶基的三唑环结构的化合物由以下通式（1）表示，并且含有一对电极和至少一个有机层在其之间切换的有机电致发光器件是其特征在于，使用下述通式（1）表示的化合物，其具有被咔唑基取代的吡啶基的三唑环结构作为至少一个有机层的结构材料有机电致发光器件。

44. 发明授权

US08053607B2 Method for producing polyether-polyol having narrow molecular weight distribution 有权
标题翻译：制备分子量分布窄的聚醚多元醇的方法
公开(公告)号：US08053607B2
公开(公告)日：2011-11-08
申请号：US10739122
申请日：2003-12-19
申请人： Kazuaki Okabe , Hiroshi Nakaoka , Ikuhiko Kanehira
发明人： Kazuaki Okabe , Hiroshi Nakaoka , Ikuhiko Kanehira
IPC分类号： C07C41/38 , C07C41/34 , C07C41/01 , C07C43/00 , C07C43/10
CPC分类号： C08G65/30 , C08G65/20
摘要： A method for producing a polyether-polyol having a narrow molecular weight distribution, which comprises carrying out selective fractional extraction of the low-molecular weight component from a polyether-polyol (A) having an average molecular weight of from 500 to 4500 represented by formula (1): HO—[(CH2)4O]n—[(CR1R2)pO]q—H (1) wherein R1 and R2, which may be the same or different, each represents a hydrogen atom or a linear or branched alkyl group having from 1 to 5 carbon atoms; n indicates a positive integer; p indicates an integer of from 1 to 8; and q indicates 0 or a positive integer, by the use of an aqueous solution (C) containing from 15 to 70 wt % sulfuric acid at a room temperature to 100° C., to thereby suitably determine the amount of the aqueous sulfuric acid solution to the overall organic layer and the sulfuric acid concentration in accordance with the molecular weight and molecular weight distribution of the intended polyether-polyol to be fractionally extracted.
摘要翻译：一种具有窄分子量分布的聚醚多元醇的制造方法，其特征在于，进行由式（A）表示的平均分子量为500〜4500的聚醚多元醇（A）的低分子量成分的选择性分级萃取（1）：HO - [（CH 2）4 O] n - [（CR 1 R 2）p O] q -H（1）其中R 1和R 2可以相同或不同，表示氢原子或直链或支链烷基具有1至5个碳原子的基团; n表示正整数; p表示1〜8的整数， q为0或正整数时，通过使用含有15〜70重量％硫酸的水溶液（C），在室温〜100℃下，适当地测定硫酸水溶液的量根据分数提取的目标聚醚 - 多元醇的分子量和分子量分布，计算总有机层和硫酸浓度。

45. 发明授权

US08053092B2 m-carbazolylphenyl compounds 有权
标题翻译：间 - 咔唑基苯基化合物
公开(公告)号：US08053092B2
公开(公告)日：2011-11-08
申请号：US12097159
申请日：2006-12-12
申请人： Tetsuzo Miki , Norimasa Yokoyama , Shigeru Kusano , Chihaya Adachi
发明人： Tetsuzo Miki , Norimasa Yokoyama , Shigeru Kusano , Chihaya Adachi
IPC分类号： H01L51/54 , H01J1/63 , C07D403/10 , C07D403/12
CPC分类号： C07D209/86 , C09K11/06 , C09K2211/1007 , C09K2211/1014 , C09K2211/1029 , H01L51/0061 , H01L51/0071 , H01L51/0072 , H01L51/0085 , H01L51/5016 , H01L51/5048 , H05B33/14 , Y10S428/917
摘要： An object of the present invention is to provide a host compound in an emission layer, which has a high excited triplet level and completely confines triplet excitons of an phosphorescence-emitting substance. The invention relates to a compound containing an m-carbazolylphenyl group, which is represented by the following general formula (1): wherein A represents a nitrogen atom, an amino group to which a substituted or unsubstituted aromatic hydrocarbon group is bonded, a substituted or unsubstituted aromatic hydrocarbon group, a substituted or unsubstituted aromatic heterocyclic group, or a substituted or unsubstituted condensed polycyclic aromatic group; n represents an integer of 2 to 4; R1 and R2 may be the same or different and represent each an arbitrary substituent; and m and o represent each an integer of 0 to 4.
摘要翻译：本发明的目的是提供一种具有高激发三重态的发射层中的主体化合物，并且完全限制磷光发射物质的三线态激子。本发明涉及含有间 - 咔唑基苯基的化合物，其由下列通式（1）表示：其中A表示氮原子，取代或未取代的芳族烃基键合的氨基，取代或未取代的取代的芳香族烃基，取代或未取代的芳香族杂环基或取代或未取代的稠合多环芳香族基; n表示2〜4的整数， R1和R2可以相同或不同，表示任意的取代基; m和o表示0〜4的整数。

46. 发明申请

US20110168942A1 CARBON FIBROUS AGGREGATOR, METHOD FOR MANUFACTURING THEREOF, AND COMPOSITE MATERIAL INCLUDING THEREOF 失效
标题翻译：碳纤维聚集体，其制造方法及其复合材料
公开(公告)号：US20110168942A1
公开(公告)日：2011-07-14
申请号：US13006892
申请日：2011-01-14
申请人： Yoshinori HITOE , Jun SUZUKI
发明人： Yoshinori HITOE , Jun SUZUKI
IPC分类号： C09K5/00
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/16 , C01P2002/82 , C08J5/042 , C08J5/047 , C08J5/10 , C22C49/14 , D01F9/127 , Y10T428/249924 , Y10T428/2927 , Y10T428/298 , Y10T428/2982 , Y10T428/30
摘要： Disclosed is a carbon fibrous aggregator obtained by a chemical vapor phase growing method, which comprises plural granular parts, and plural carbon fibers which are mutually independently extended outwardly from their respective granular parts so that each granular part is associated with two or more of carbon fibers, wherein the carbon fibers show a three dimensional expansion in all; and which show a three dimensional network structure of the carbon fibers at least in a part by a state that at least a part of the plural carbon fibers extended from one granular part is linked with another granular part; wherein mean length of carbon fibers which link two granular parts together is of 3.0-20.0 μm, and wherein a coefficient of variation, CV, ((standard deviation/mean value)×100) which is obtained on a determination of outer diameter distribution of the carbon fibers which constitute the aggregator of carbon fiber is not more than 30%.
摘要翻译：公开了一种通过化学气相生长法获得的碳纤维聚集体，其包括多个颗粒部分和从它们各自的颗粒部分相互独立地向外延伸的多个碳纤维，使得每个颗粒部分与两个或更多个碳纤维相关联其中碳纤维全部呈三维膨胀; 并且至少部分地通过从一个颗粒部分延伸的多个碳纤维的至少一部分与另一个颗粒部分连接的状态来显示碳纤维的三维网状结构; 其中将两个颗粒部分连接在一起的碳纤维的平均长度为3.0-20.0μm，并且其中在确定外径分布时获得的变异系数CV（（标准偏差/平均值）×100）构成碳纤维聚集体的碳纤维不大于30％。

47. 发明申请

US20110006291A1 COMPOUND HAVING SUBSTITUTED PYRIDYL GROUP AND PYRIDOINDOLE RING STRUCTURE LINKED THROUGH PHENYLENE GROUP, AND ORGANIC ELECTROLUMINESCENT DEVICE 有权
标题翻译：具有取代的吡啶基的化合物和通过苯乙烯基团连接的吡啶环结构和有机电致发光器件
公开(公告)号：US20110006291A1
公开(公告)日：2011-01-13
申请号：US12865736
申请日：2009-01-30
申请人： Norimasa Yokoyama , Shuichi Hayashi , Sawa Izumi , Shigeru Kusano
发明人： Norimasa Yokoyama , Shuichi Hayashi , Sawa Izumi , Shigeru Kusano
IPC分类号： H01L51/54 , C07D471/04
CPC分类号： C07D471/04 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , H01L51/0052 , H01L51/0072 , H01L51/5012 , H01L51/5048
摘要： Objects of the present invention are to provide an organic compound having excellent properties, which is excellent in electron-injecting/transporting performances, has hole-blocking ability and is highly stable in a thin-film state, as a material for an organic electroluminescent device having a high efficiency and a high durability; and to provide an organic electroluminescent device having a high efficiency and a high durability using the compound. The invention relates to a compound having a substituted pyridyl group and a pyridoindole ring structure linked through a phenylene group, which is represented by the general formula (1); and an organic EL device comprising a pair of electrodes and at least one organic layer interposed between the electrodes, wherein the at least one organic layer contains the compound: wherein Ar represents a substituted or unsubstituted aromatic hydrocarbon group, a substituted or unsubstituted aromatic heterocyclic group, or a substituted or unsubstituted condensed polycyclic aromatic group; R1 to R14 may be the same or different from each other and each represents a hydrogen atom, a fluorine atom, a chlorine atom, a cyano group, a trifluoromethyl group, a linear or branched alkyl group having 1 to 6 carbon atoms, a substituted or unsubstituted aromatic hydrocarbon group, a substituted or unsubstituted aromatic heterocyclic group, or a substituted or unsubstituted condensed polycyclic aromatic group; n represents an integer of 1 to 3; and W, X, Y, and Z respectively represent a carbon atom or a nitrogen atom, provided that only one of W, X, Y, and Z represents a nitrogen atom, and the nitrogen atom does not have the substituent of R7, R8, R9, or R10).
摘要翻译：本发明的目的是提供具有优异的电子注入/传输性能的具有优异的性能的有机化合物，具有空穴阻挡能力并且在薄膜状态下是高度稳定的，作为有机电致发光器件的材料具有高效率和高耐久性; 并提供使用该化合物具有高效率和高耐久性的有机电致发光器件。本发明涉及由通式（1）表示的具有取代的吡啶基和通过亚苯基连接的吡啶并吲哚环结构的化合物。以及包含一对电极和插入在所述电极之间的至少一个有机层的有机EL器件，其中所述至少一个有机层包含化合物：其中Ar表示取代或未取代的芳香族烃基，取代或未取代的芳族杂环基，或取代或未取代的稠合多环芳基; R 1〜R 14可以相同也可以不同，表示氢原子，氟原子，氯原子，氰基，三氟甲基，碳原子数1〜6的直链或支链烷基，取代基或未取代的芳香族烃基，取代或未取代的芳香族杂环基或取代或未取代的稠合多环芳香族基; n表示1〜3的整数， W，X，Y和Z分别表示碳原子或氮原子，只要W，X，Y和Z中只有一个表示氮原子，氮原子不具有R7，R8的取代基，R9或R10）。

48. 发明授权

US07862905B2 Arylamine compound and organic electroluminescent device 有权
标题翻译：芳胺化合物和有机电致发光器件
公开(公告)号：US07862905B2
公开(公告)日：2011-01-04
申请号：US10594239
申请日：2005-03-25
申请人： Tetsuzo Miki , Naohiro Tarumoto , Yoshio Taniguchi , Musubu Ichikawa
发明人： Tetsuzo Miki , Naohiro Tarumoto , Yoshio Taniguchi , Musubu Ichikawa
IPC分类号： H01J1/63
CPC分类号： C09K11/06 , C07C211/54 , C07D209/86 , C09K2211/1014 , H01L2251/5384 , H05B33/14
摘要： The present invention provides an arylamine compound having a molecular weight of from 1500 to 6000 represented by the general formula (1): According to the present invention, there can be provided an arylamine compound having excellent hole injection and transporting characteristics and being capable of forming a stable thin film. By using the compound, emission efficiency and durability of conventional organic EL devices can remarkably be improved.
摘要翻译：本发明提供由通式（1）表示的分子量为1500〜6000的芳基胺化合物：根据本发明，可以提供具有优异的空穴注入和输送特性并能够形成的芳基胺化合物一个稳定的薄膜。通过使用该化合物，可以显着提高常规有机EL器件的发光效率和耐久性。

49. 发明授权

US07807274B2 Tetramine compound and organic EL device 有权
标题翻译：四胺化合物和有机EL器件
公开(公告)号：US07807274B2
公开(公告)日：2010-10-05
申请号：US10584140
申请日：2004-12-24
申请人： Shigeru Kusano , Makoto Koike , Atsushi Takesue , Mitsutoshi Anzai
发明人： Shigeru Kusano , Makoto Koike , Atsushi Takesue , Mitsutoshi Anzai
IPC分类号： H01L51/50
CPC分类号： C07C211/54 , C09K11/06 , C09K2211/1014 , H01L51/0059 , H01L51/0081 , H01L51/5048 , H01L2251/308 , H05B33/14 , Y10S428/917
摘要： The present invention provides a tetramine compound represented by the following general formula (1): wherein R1, R2 and R3, which may be the same or different, each represents a hydrogen atom, a tertiary alkyl group having 4 to 8 carbon atoms, an unsubstituted aryl group or an aryl group substituted with a tertiary alkyl group having 4 to 8 carbon atoms, and n represents 3 or 4. According to the invention, there can be provided a material suitable as a material for an organic EL element requiring luminous stability at the time of high temperature driving which has been the largest problem of the conventional organic EL element. Further, an organic EL element containing the above-mentioned tetramine compound and a method for producing the above-mentioned tetramine compound are also disclosed.
摘要翻译：本发明提供由以下通式（1）表示的四胺化合物：其中可以相同或不同的R 1，R 2和R 3各自表示氢原子，具有4至8个碳原子的叔烷基，未取代的芳基或被碳原子数为4〜8的叔烷基取代的芳基，n表示3或4.根据本发明，可以提供适合作为需要发光稳定性的有机EL元件的材料的材料在传统的有机EL元件的最大问题的高温驱动时，此外，还公开了含有上述四胺化合物的有机EL元件和上述四胺化合物的制造方法。

50. 发明申请

US20090278442A1 ARYLAMINE COMPOUND AND ORGANIC ELECTROLUMINESCENCE DEVICE 有权
标题翻译：芳基胺化合物和有机电致发光器件
公开(公告)号：US20090278442A1
公开(公告)日：2009-11-12
申请号：US12065417
申请日：2006-08-31
申请人： Tetsuzo Miki , Norimasa Yokoyama , Yoshio Taniguchi , Musubu Ichikawa
发明人： Tetsuzo Miki , Norimasa Yokoyama , Yoshio Taniguchi , Musubu Ichikawa
IPC分类号： H01J1/63 , C07C211/50
CPC分类号： C07C211/54 , C07C211/58 , C09K11/06 , C09K2211/1007 , C09K2211/1014 , C09K2211/1029 , H01L51/0059 , H01L51/006 , H01L51/0072 , H01L51/0081 , H01L51/0095 , H01L51/5048 , H01L2251/308 , H05B33/14 , Y02P20/582 , Y10S428/917
摘要： Objects of the invention are to provide a compound of a single molecular species having excellent hole injection/transport property suitable for highly efficient and highly durable organic EL device and excellent amorphousness, and provide a highly efficient and highly durable organic EL device using the compound. This invention relates to an arylamine compound having a molecular weight of 1,500 to 6,000 represented by the following general formula (1), and to an organic electroluminescence device having a pair of electrodes and at least one organic layer sandwiched therebetween, wherein the compound is used as a constituting material of the at least one organic layer: wherein X represents a single bond, CH or CH2, or N or NH; Ar1 and Ar2 are respectively the same and each represents a substituted or unsubstituted phenylene group, biphenylene group, or terphenylene group; R1, R2, R3, and R4 each independently represents an aryl group, wherein the aryl group may be substituted by a diarylamine group in such a manner as to form a triphenylamine partial structure, and the aryl group at the terminal may be substituted, by repetition, by a diarylamino group in such a manner as to form a triphenylamine-like partial structure; m represents an integer of 0 to 2; and n represents 0 or 1.
摘要翻译：本发明的目的是提供具有优异的空穴注入/传输性能的化合物，该化合物适用于高效高效耐用的有机EL器件和优异的无定形性，并提供使用该化合物的高效率和高度耐用的有机EL器件。本发明涉及由以下通式（1）表示的分子量为1,500至6,000的芳基胺化合物以及夹在其间的具有一对电极和至少一个有机层的有机电致发光器件，其中使用该化合物作为所述至少一种有机层的构成材料：其中X表示单键，CH或CH 2，或N或NH; Ar 1和Ar 2分别相同，各自表示取代或未取代的亚苯基，亚联苯基或三亚苯基; R1，R2，R3和R4各自独立地表示芳基，其中芳基可以以形成三苯胺部分结构的方式被二芳基胺基取代，并且末端的芳基可以被以形成三苯胺样部分结构的方式由二芳基氨基重复; m表示0〜2的整数。 n表示0或1。

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