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41. 发明授权

US4900402A Pervaporation process of separating a liquid mixture 失效
标题翻译：分离液体混合物的渗透蒸发过程
公开(公告)号：US4900402A
公开(公告)日：1990-02-13
申请号：US29911
申请日：1987-03-25
申请人： Jurgen Kaschemekat , Frank Schutt , Axel Wenzlaff
发明人： Jurgen Kaschemekat , Frank Schutt , Axel Wenzlaff
IPC分类号： B01D3/00 , B01D3/14 , B01D3/42 , B01D5/00 , B01D17/00 , B01D61/00 , B01D61/36 , B01D71/00 , C07C29/76 , C07C31/08 , C12L11/00 , C12P7/06
CPC分类号： B01D61/362 , B01D2317/025 , Y02E50/17 , Y10S159/27 , Y10S203/14 , Y10S203/17
摘要： A pervaporation process for separating at least one component from a mixture of liquids, for example for separating ethanol from a fermentation mass, by a series of three separation steps: separating the mixture by a first pervaporation to form a first permeate vapor enriched in the component to be separated; fractionating the first permeate vapor, for example by temperature condensation, to form a high concentration fraction twice enriched in the component to be separated; and either distilling the high concentration fraction or a second pervaporation to form a distillate or retentate liquid thrice enriched in the component to be separated.
摘要翻译：一种用于从液体混合物中分离至少一种组分的渗透蒸发过程，例如通过一系列三个分离步骤分离乙醇：将第一渗透蒸发分离混合物以形成富含组分的第一渗透气体被分开将第一渗透蒸气分馏，例如通过温度冷凝，以形成两倍于要分离的组分的高浓度分数; 并且蒸馏高浓度馏分或第二渗透蒸发以形成富含待分离组分的馏出物或滞留物液体三倍。

42. 发明授权

US4843170A Process for producing vinyl acetate 失效
标题翻译：乙酸乙烯酯的制造方法
公开(公告)号：US4843170A
公开(公告)日：1989-06-27
申请号：US466653
申请日：1983-02-15
申请人： Tomiya Isshiki , Yasuhiko Kijima , Akira Ito , Kenji Ishii
发明人： Tomiya Isshiki , Yasuhiko Kijima , Akira Ito , Kenji Ishii
IPC分类号： C07C67/36 , C07C31/08 , C07C53/08 , C07C67/297 , C07C69/15
CPC分类号： C07C67/297 , C07C51/09 , C07C51/56 , C07C67/00 , C07C67/24 , C07C67/36
摘要： A process is disclosed for producing vinyl acetate from methanol, carbon monoxide and hydrogen which comprises the following five steps:(a) methanol is hydrocarbonylated in a hydrocarbonylation zone to produce ethanol, acetaldehyde, methyl acetate and dimethylacetal, and the products are separated in a separation zone;(b) methyl acetate is carbonylated in a carbonylation zone to produce acetic anhydride;(c) the acetaldehyde and dimethylacetal produced in the step (a) and the acetic anhydride produced in the step (b) are converted to ethylidene diacetate and methyl acetate; (d) the ethylidene diacetate produced in the step (c) is thermally decomposed to vinyl acetate and acetic acid, and the products are separated in a separation zone; and(e) the methyl acetate produced and separated in the step (a), (c) or (d) is supplied to the carbonylation step (b).
摘要翻译：公开了一种从甲醇，一氧化碳和氢气生产乙酸乙烯酯的方法，其包括以下五个步骤：（a）在烃基化区域中甲醇被烃化生成乙醇，乙醛，乙酸甲酯和二甲基缩醛，并将产物分离成分离区; （b）乙酸甲酯在羰基化区羰基化，生成乙酸酐; （c）将步骤（a）中生成的乙醛和二甲基缩醛和步骤（b）中生产的乙酸酐转化为乙二乙酸乙酯和乙酸甲酯; （d）将步骤（c）中生产的亚乙基双乙酸酯热分解成乙酸乙烯酯和乙酸，并将产物在分离区中分离; 和（e）在步骤（a），（c）或（d）中产生和分离的乙酸甲酯被供应到羰基化步骤（b）。

43. 发明授权

US4777303A Alcohols production by hydrogenation of carboxylic acids 失效
标题翻译：醇通过氢化羧酸生产
公开(公告)号：US4777303A
公开(公告)日：1988-10-11
申请号：US848998
申请日：1986-04-07
申请人： Melanie Kitson , Peter S. Williams
发明人： Melanie Kitson , Peter S. Williams
IPC分类号： C07C27/04 , B01J23/00 , B01J23/656 , C07B61/00 , C07C27/00 , C07C29/136 , C07C29/149 , C07C31/08 , C07C31/10 , C07C67/00 , C07C67/08
CPC分类号： C07C29/149 , Y10S502/525
摘要： An alcohol and/or a carboxylic acid ester is (are) produced from a C.sub.2 to C.sub.12 carboxylic acid by contacting the carboxylic acid at elevated temperature and pressure with hydrogen in the presence of a heterogeneous catalyst characterized in that the catalyst comprises a first component which is either molybdenum or tungsten and a second component which is a noble metal of Group VIII of the Periodic Table of the Elements, optionally on a support, for example a high surface area graphitized carbon.
摘要翻译：通过在多相催化剂的存在下使升高的温度和压力下的羧酸与氢接触，由C2-C12羧酸制备醇和/或羧酸酯，其特征在于催化剂包含第一组分，是钼或钨，第二组分是元素周期表第VIII族的贵金属，任选地在载体上，例如高表面积石墨化碳。

44. 发明授权

US4654321A Upgrading synthesis gas catalyst 失效
标题翻译：升级合成气催化剂
公开(公告)号：US4654321A
公开(公告)日：1987-03-31
申请号：US633137
申请日：1984-07-23
申请人： Frederick A. Pesa , Anne M. Graham
发明人： Frederick A. Pesa , Anne M. Graham
IPC分类号： B01J23/89 , B01J27/24 , C07C1/04 , C07C9/00 , C07C31/04 , C07C31/08 , C07C51/10 , B01J23/72 , B01J23/00 , C07C27/00
CPC分类号： C07C51/10 , B01J23/89 , B01J23/8946 , B01J27/24 , C07C1/0435 , C07C1/0485 , C07C31/04 , C07C31/08 , C07C9/00 , C07C2521/04 , C07C2521/08 , C07C2521/12 , C07C2521/16 , C07C2523/04 , C07C2523/42 , C07C2523/46 , C07C2523/72 , C07C2523/89 , C07C2527/224 , C07C2527/24 , Y02P20/52
摘要： A process is provided for the upgrading of synthesis gas to hydrocarbons and oxygenated hydrocarbons, particularly olefins and carboxylic acids by contacting synthesis gas with catalysts comprising the mixed oxides of ruthenium, copper, an alkali or alkaline earth metal, and optionally a metal selected from Ce, Cr, Fe, Mn, Mo, Th, Zn or mixtures thereof. The synthesis gas upgrading product may be contacted with a hydrogenation catalyst to provide alkanes, alcohols and esters, useful for fuels.
摘要翻译：提供了一种通过使合成气与包含钌，铜，碱金属或碱土金属的混合氧化物的催化剂和任选的选自Ce的金属的催化剂将合成气升级成烃和含氧烃，特别是烯烃和羧酸的方法，Cr，Fe，Mn，Mo，Th，Zn或其混合物。合成气改质产物可以与氢化催化剂接触以提供可用于燃料的烷烃，醇和酯。

45. 发明授权

US4568699A Process for producing oxygen-containing hydrocarbon compounds 失效
标题翻译：含氧烃化合物的制造方法
公开(公告)号：US4568699A
公开(公告)日：1986-02-04
申请号：US739317
申请日：1985-05-30
申请人： Ken-ichi Sano , Yukimitsu Mita , Shinya Matsuhira , Tetsuo Nakajo , Hitoshi Iijima
发明人： Ken-ichi Sano , Yukimitsu Mita , Shinya Matsuhira , Tetsuo Nakajo , Hitoshi Iijima
IPC分类号： B01J23/00 , C07B61/00 , C07C27/00 , C07C27/06 , C07C29/15 , C07C29/158 , C07C31/08 , C07C45/00 , C07C45/49 , C07C47/06 , C07C51/00 , C07C51/10 , C07C53/08 , C07C67/00
CPC分类号： C07C45/49 , C07C29/158 , C07C51/10 , Y02P20/52
摘要： A catalyst comprising a combination of rhodium, iridium and lithium supported on a carrier having a specific surface area of more than 150 m.sup.2 /g is disclosed for producing two carbon atom oxygenerated compounds from carbon monoxide. The catalyst has high catalytic activity and high selectivity to acetic acid.
摘要翻译：公开了一种催化剂，其包含负载在比表面积大于150m 2 / g的载体上的铑，铱和锂的组合，用于由一氧化碳制备两种碳原子氧化合物。催化剂具有高催化活性和对乙酸的高选择性。

46. 发明授权

US4540836A Hemologation of alkanols 失效
标题翻译：链烷醇的血液学
公开(公告)号：US4540836A
公开(公告)日：1985-09-10
申请号：US643835
申请日：1984-08-24
申请人： Donald M. Fenton
发明人： Donald M. Fenton
IPC分类号： C07C29/32 , C07C29/00 , C07C31/08 , C07C31/20 , C07C33/22
CPC分类号： C07C29/32 , C12C11/02
摘要： This invention provides a process for converting alkanols into higher alkanols, e.g. methanol into ethanol, by contacting a basic solution comprising said alkanol in the absence of added hydrogen, with a catalyst comprising a lanthanum moiety. Preferably said catalyst further comprises a rhodium or a ruthenium moiety in combination with said lanthanum moiety. This invention further provides a novel heterogeneous catalyst system adapted for alkanol homologation, which comprises lanthanum hydroxide and a rhodium or ruthenium moiety, e.g. RhCl.sub.3 or RuCl.sub.3.
摘要翻译：本发明提供了将链烷醇转化成高级链烷醇的方法，例如通过在不存在加氢的情况下将包含所述链烷醇的碱性溶液与包含镧部分的催化剂接触，将甲醇转化成乙醇。优选地，所述催化剂还包含与所述镧部分组合的铑或钌部分。本发明还提供了一种适用于链烷醇同系的新型多相催化剂体系，其包括氢氧化镧和铑或钌部分，例如氢氧化镧。 RhCl3或RuCl3。

47. 发明授权

US4487614A Adsorption separation cycle 失效
标题翻译：吸附分离循环
公开(公告)号：US4487614A
公开(公告)日：1984-12-11
申请号：US552337
申请日：1983-11-16
申请人： Carmen M. Yon
发明人： Carmen M. Yon
IPC分类号： B01D15/02 , B01D53/04 , B01D53/047 , C07C29/76 , C07C31/08
CPC分类号： B01D53/261 , B01D53/047 , C07C29/76 , B01D2253/108 , B01D2253/308 , B01D2257/70 , B01D2257/702 , B01D2257/80 , B01D2259/40052 , B01D2259/40056 , B01D2259/4006 , B01D2259/40081 , B01D2259/65
摘要： In a fixed-bed vapor phase adsorption cycle for bulk separations wherein the heat front generated by the exothermic heat of adsorption is maintained in the bed either in or behind the mass transfer zone, and is subsequently utilized in the purge desorption/regeneration of the bed, improved efficiency and enhanced versatility with respect to the degree of product purity is obtained by treating the regeneration purge gas with a portion of the purified product.
摘要翻译：在用于批量分离的固定床气相吸附循环中，其中通过吸附放热产生的热前沿在质量传递区内或之后保持在床中，并随后用于床的吹扫解吸/再生通过用纯化产物的一部分处理再生吹扫气体可以获得相对于产品纯度的提高的效率和增强的多功能性。

48. 发明授权

US4442228A Process for the manufacture of ethanol from synthesis gas 失效
标题翻译：从合成气制造乙醇的方法
公开(公告)号：US4442228A
公开(公告)日：1984-04-10
申请号：US443131
申请日：1982-11-19
申请人： Ernst I. Leupold , Hans-Joachim Schmidt , Friedrich Wunder , Hans-Jurgen Arpe , Horst Hachenberg
发明人： Ernst I. Leupold , Hans-Joachim Schmidt , Friedrich Wunder , Hans-Jurgen Arpe , Horst Hachenberg
IPC分类号： C07C27/06 , B01J23/00 , B01J23/46 , B01J23/54 , B01J23/56 , C07B61/00 , C07C27/00 , C07C29/15 , C07C29/153 , C07C29/157 , C07C29/158 , C07C31/08 , C07C45/49 , C07C51/12 , C07C67/00
CPC分类号： C07C45/49 , B01J23/464 , B01J23/56 , C07C29/158 , C07C51/12
摘要： Ethanol is manufactured by reaction of carbon monoxide with hydrogen on a supported rhodium catalyst containing as cocatalyst at least one of the elements zirconium, hafnium, lanthanum, platinum, chromium and mercury.
摘要翻译：乙醇通过一氧化碳与氢气在负载的铑催化剂上反应制得，该催化剂含有至少一种元素锆，铪，镧，铂，铬和汞作为助催化剂。

49. 发明授权

US4421939A Production of ethanol from acetic acid 失效
标题翻译：从乙酸生产乙醇
公开(公告)号：US4421939A
公开(公告)日：1983-12-20
申请号：US434562
申请日：1982-10-15
申请人： Ben W. Kiff , David J. Schreck
发明人： Ben W. Kiff , David J. Schreck
IPC分类号： C07C29/136 , B01J31/00 , C07C1/24 , C07C27/00 , C07C29/149 , C07C31/08 , C07C67/00
CPC分类号： C07C29/149 , C07C1/24 , C07C67/04 , C07C2521/02 , C07C2527/173
摘要： Ethanol is produced from acetic acid by esterifying the acetic acid with an olefin having at least 4 carbon atoms, hydrogenating the ester obtained into ethanol and a higher alcohol having at least 4 carbon atoms, removing the ethanol, dehydrating the higher alcohol back to the original olefin and recycling the olefin to esterify the acetic acid.
摘要翻译：乙酸通过用具有至少4个碳原子的烯烃酯化乙酸来制备乙醇，将得到的酯氢化成乙醇和具有至少4个碳原子的高级醇，除去乙醇，使高级醇脱水回原来烯烃并再循环烯烃以酯化乙酸。

50. 发明授权

US4405409A Method and apparatus for dehydrating mixtures of organic liquids and water 失效
标题翻译：有机液体和水的混合物脱水的方法和装置
公开(公告)号：US4405409A
公开(公告)日：1983-09-20
申请号：US308560
申请日：1981-10-05
申请人： Gunter Tusel , Achim Ballweg
发明人： Gunter Tusel , Achim Ballweg
IPC分类号： B01D3/00 , B01D3/14 , B01D3/32 , B01D17/00 , B01D61/36 , C07C29/76 , C07C29/80 , C07C31/08 , C07C31/10 , B01D13/00
CPC分类号： B01D61/364 , B01D3/14 , B01D3/322 , C07C29/76 , C07C29/80
摘要： A method and apparatus for dehydrating mixtures of organic liquids and water comprising consecutive distillation and membrane permeation, wherein at least a portion of the material retained by the separator is passed into indirect heat exchange relationship within the distillation column and recycled to the separator to provide the heat input required for the permeation process.
摘要翻译：一种用于使有机液体和水的混合物脱水的方法和装置，其包括连续的蒸馏和膜渗透，其中由分离器保留的材料的至少一部分在蒸馏塔内被传递到间接的热交换关系中并再循环到分离器中，渗透过程所需的热量输入。

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