
基本信息:
- 专利标题: 一种四氧化三铁纳米粒子的制备方法
- 专利标题(英):Preparing method of ferroferric oxide nanometer particles
- 申请号:CN201410053833.4 申请日:2014-02-17
- 公开(公告)号:CN104030363A 公开(公告)日:2014-09-10
- 发明人: 胡军 , 胡熙健 , 陈爱民 , 汪晶
- 申请人: 瑞安市浙工大技术转移中心
- 申请人地址: 浙江省温州市瑞安市万松路141号科技大楼北首三楼
- 专利权人: 瑞安市浙工大技术转移中心
- 当前专利权人: 瑞安市浙工大技术转移中心
- 当前专利权人地址: 浙江省温州市瑞安市万松路141号科技大楼北首三楼
- 代理机构: 杭州天正专利事务所有限公司
- 代理人: 黄美娟; 王晓普
- 主分类号: C01G49/08
- IPC分类号: C01G49/08 ; B82Y30/00
The invention relates to a preparing method of ferroferric oxide nanometer particles with good dispersibility. The ferroferric oxide nanometer particles are prepared by steps of: adding ferric chloride and ferrous sulfate having the same molar as the ferric chloride into deionized water under the protection of an inert gas, so that the molar volume concentration of the ferrous sulfate containing ferrous iron and the molar volume concentration of the ferric chloride containing ferric iron are both maintained between 0.01-0.1 mol/L; adding a [BMIN]BF4 ionic liquid in place of a traditional surfactant; mixing uniformly; adding dropwise a sodium hydroxide solution adopted as a precipitator at 70 DEG C to precipitate to obtain a reaction product; washing alternatively with deionized water and absolute ethyl alcohol; centrifuging; and drying under vacuum. Raw materials used in the method are easily available, low in cost and short in preparation period. The obtained ferroferric oxide nanometer particles can be used as high-performance catalysts, magnetic materials and electrode materials.
公开/授权文献:
- CN104030363B 一种四氧化三铁纳米粒子的制备方法 公开/授权日:2016-05-25