
基本信息:
- 专利标题: 聚乙二醇1500双丙烯酸酯的制备方法
- 专利标题(英):Method for preparing polyethylene glycol 1500 diacrylate
- 申请号:CN201510577800.4 申请日:2015-09-11
- 公开(公告)号:CN106519207A 公开(公告)日:2017-03-22
- 发明人: 徐博刚
- 申请人: 天津市化学试剂研究所有限公司
- 申请人地址: 天津市东丽区金钟河大街徐庄子
- 专利权人: 天津市化学试剂研究所有限公司
- 当前专利权人: 天津市化学试剂研究所有限公司
- 当前专利权人地址: 天津市东丽区金钟河大街徐庄子
- 代理机构: 天津盛理知识产权代理有限公司
- 代理人: 赵瑶瑶
- 主分类号: C08G65/332
- IPC分类号: C08G65/332 ; C08G65/30 ; C07C69/54 ; C07C67/08
The invention relates to a method for preparing polyethylene glycol 1500 diacrylate. The method comprises the steps: (1) carrying out an esterification reaction: adding polyethylene glycol 1500, acrylic acid, a solvent, i.e., toluene, a catalyst, i.e., para-toluenesulfonic acid and a polymerization inhibitor, i.e., p-hydroxyanisole into a reactor, heating the system until the system is subjected to refluxing with stirring, separating water produced from a reaction through an oil-water separator, continuing to carry out stirring for 2 hours after no water is produced, stopping heating, and stopping stirring, wherein the mole ratio of polyethylene glycol 1500 to acrylic acid is 1: (1.1 to 1.2); (2) carrying out water washing; and (3) carrying out depressurized desolventizing, thereby obtaining the finished product. According to the method disclosed by the invention, expensive special equipment is not required to be employed during production, the production cost can be reduced, and the market competitiveness of enterprises is improved, so that the product can be more extensively popularized and applied on the market.
IPC结构图谱:
C | 化学;冶金 |
--C08 | 有机高分子化合物;其制备或化学加工;以其为基料的组合物 |
----C08G | 用碳—碳不饱和键以外的反应得到的高分子化合物 |
------C08G65/00 | 由在高分子主链中形成醚键的反应得到的高分子化合物 |
--------C08G65/02 | .由环醚用杂环开环的反应 |
----------C08G65/32 | ..化学后处理改性的聚合物 |
------------C08G65/321 | ...用无机化合物 |
--------------C08G65/331 | ....含氧 |
----------------C08G65/332 | .....含羧基,或其卤化物或酯 |