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11. 发明授权

US07790319B2 Method for making electrode active material 有权
标题翻译：电极活性物质的制造方法
公开(公告)号：US07790319B2
公开(公告)日：2010-09-07
申请号：US11379754
申请日：2006-04-21
申请人： Titus Faulkner
发明人： Titus Faulkner
IPC分类号： H01M4/58 , C01B25/26
CPC分类号： C01B25/45 , B01J27/198 , C01G31/006 , C01P2002/72 , C01P2006/40 , H01M4/136 , H01M4/5825 , H01M10/052
摘要： The present invention is directed to a method for making electrode active materials represented by the general formula: Aa(VO)bXO4, wherein: (a) A is an alkali metal or mixture of alkali metals, and 0
摘要翻译：本发明涉及一种制备由以下通式表示的电极活性材料的方法：Aa（VO）bXO4，其中：（a）A是碱金属或碱金属的混合物，0

12. 发明授权

US5766800A Highly homogeneous spinel Li.sub.1+X Mn.sub.2-X O.sub.4+Y intercalation compounds and method for preparing same 失效
标题翻译：高均相尖晶石Li1 + XMn2-XO4 + Y插层化合物及其制备方法
公开(公告)号：US5766800A
公开(公告)日：1998-06-16
申请号：US867160
申请日：1997-06-02
申请人： Vesselin Manev , Titus Faulkner
发明人： Vesselin Manev , Titus Faulkner
IPC分类号： C01B31/02 , C01G45/00 , H01M4/131 , H01M4/50 , H01M4/505 , H01M10/052 , H01M10/36 , C01G45/12
CPC分类号： H01M4/505 , C01G45/1242 , H01M4/131 , C01P2002/32 , C01P2002/72 , C01P2002/74 , C01P2006/12 , C01P2006/40 , H01M10/052
摘要： A novel method of preparing a spinel Li.sub.1+X Mn.sub.2-X O.sub.4+Y intercalation compound with low lattice distortion and a highly ordered and homogeneous structure for 4 V secondary lithium and lithium ion cells is provided. The method of preparing the spinel Li.sub.1+X Mn.sub.2-X O.sub.4+Y intercalation compound comprises providing a spinel Li.sub.1+X Mn.sub.2-X O.sub.4 intercalation compound having a lithium to manganese mole ratio of between about 1.02:2 and 1.1:2 and firing the spinel at different temperature ranges with corresponding gas flow rates to form the spinel Li.sub.1+X Mn.sub.2-X O.sub.4+Y intercalation compounds. The spinel Li.sub.1+X Mn.sub.2-X O.sub.4+Y intercalation compounds have a mean X value of between about 0.01 and 0.05, a mean Y value of between about -0.02 and 0.04 and a full width at half maximum of the x-ray diffraction peaks at a diffraction angle 2.theta. of planes (400) and (440) using CuK.alpha..sub.1 rays of between about 0.08.degree. and 0.13.degree.. The spinel Li.sub.1+X Mn.sub.2-X O.sub.4+Y intercalation compounds may be used in the positive electrodes of secondary lithium and lithium ion cells to provide cells having high specific capacities and long cycling lives.
摘要翻译：提供了一种制备具有低晶格畸变的尖晶石Li1 + XMn2-XO4 + Y插层化合物和用于4 V二次锂和锂离子电池的高度有序和均匀结构的新方法。制备尖晶石Li1 + XMn2-XO4 + Y插层化合物的方法包括提供锂/锰摩尔比在约1.02:2至1.1:2之间的尖晶石Li1 + XMn2-XO4插层化合物，并在不同温度下烧制尖晶石范围与相应的气体流速形成尖晶石Li1 + XMn2-XO4 + Y插层化合物。尖晶石Li1 + XMn2-XO4 + Y插入化合物的平均X值在约0.01和0.05之间，平均Y值在约-0.02和0.04之间，并且x射线衍射峰的全宽度在使用约0.08和0.13之间的CuKα1射线的平面（400）和（440）的衍射角2θ。尖晶石Li1 + XMn2-XO4 + Y插层化合物可用于二次锂离子电池和锂离子电池的正电极，以提供具有高比容量和长循环寿命的电池。

13. 发明申请

US20100303701A1 Method For Making Electrode Active Materials 失效
标题翻译：制作电极活性材料的方法
公开(公告)号：US20100303701A1
公开(公告)日：2010-12-02
申请号：US12845869
申请日：2010-07-29
申请人： Titus Faulkner
发明人： Titus Faulkner
IPC分类号： C01B25/45
CPC分类号： C01B25/45 , B01J27/198 , C01G31/006 , C01P2002/72 , C01P2006/40 , H01M4/136 , H01M4/5825 , H01M10/052
摘要： The present invention is directed to a method for making electrode active materials represented by the general formula: Aa(VO)bXO4, wherein: (a) A is an alkali metal or mixture of alkali metals, and 0
摘要翻译：本发明涉及一种制备由以下通式表示的电极活性材料的方法：Aa（VO）bXO4，其中：（a）A是碱金属或碱金属的混合物，0

14. 发明申请

US20100266474A1 Method of Making Active Materials for Use in Secondary Electrochemical Cells 审中-公开
标题翻译：制备活性材料用于二次电化学电池的方法
公开(公告)号：US20100266474A1
公开(公告)日：2010-10-21
申请号：US12752652
申请日：2010-04-01
申请人： Titus Faulkner , Jon Parke
发明人： Titus Faulkner , Jon Parke
IPC分类号： C01B25/30
CPC分类号： C01B25/37 , H01M4/5825 , H01M10/0525
摘要： The present invention provides for the preparation of an “optimized” lithium vanadium phosphate material. The materials are synthesized under conditions that avoid exposure to reducing gases, such as hydrogen, at high temperatures and thus materials of high performance are produced. The lithium vanadium phosphate materials so produced find use in producing electrodes for electrochemical cells.
摘要翻译：本发明提供了制备“优化”的磷酸钒锂材料。这些材料在避免在高温下避免暴露于诸如氢的还原气体的条件下合成，因此产生高性能的材料。所生产的磷酸钒锂材料用于生产电化学电池的电极。

15. 发明授权

US06423294B1 Lithium manganese oxide spinel compound and method of preparing same 有权
公开(公告)号：US06423294B1
公开(公告)日：2002-07-23
申请号：US09842459
申请日：2001-04-26
申请人： Vesselin Manev , Titus Faulkner , D. Wayne Barnette
发明人： Vesselin Manev , Titus Faulkner , D. Wayne Barnette
IPC分类号： C01G4502
摘要： The present invention includes lithium manganese oxide spinel compounds having a low porosity, a high tap density and a high pellet density, and methods of preparing these compounds. In particular, the method comprises preparing a lithium manganese oxide with a spinel structure and having the formula: wherein: Li 1 + X ⁢ Mn 2 - Y ⁢ M m 1 1 ⁢ M m 2 2 ⁢ … ⁢ ⁢ M m k k ⁢ O 4 + Z M1, M2, . . . Mk are cations different than lithium or manganese selected from the group consisting of alkaline earth metals, transition metals, B, Al, Si, Ga and Ge; X, Y, m1, m2, . . . mk, each have a value between 0 and 0.2; Z has a value between −0.1 and 0.2; and X, Y, m1, M2. . . mk are selected to satisfy the equation: Y=X+m1+m2+. . . +mk.

16. 发明授权

US08318353B2 Method for making electrode active materials 失效
标题翻译：电极活性物质的制造方法
公开(公告)号：US08318353B2
公开(公告)日：2012-11-27
申请号：US12845869
申请日：2010-07-29
申请人： Titus Faulkner
发明人： Titus Faulkner
IPC分类号： H01M4/58 , C01B25/26
CPC分类号： C01B25/45 , B01J27/198 , C01G31/006 , C01P2002/72 , C01P2006/40 , H01M4/136 , H01M4/5825 , H01M10/052
摘要： The present invention is directed to a method for making electrode active materials represented by the general formula: Aa(VO)bXO4, wherein: (a) A is an alkali metal or mixture of alkali metals, and 0
摘要翻译：本发明涉及一种制备由以下通式表示的电极活性材料的方法：Aa（VO）bXO4，其中：（a）A是碱金属或碱金属的混合物，0

17. 发明申请

US20090068080A1 Method of Making Active Materials For Use in Secondary Electrochemical Cells 审中-公开
标题翻译：制备用于二次电化学电池的活性材料的方法
公开(公告)号：US20090068080A1
公开(公告)日：2009-03-12
申请号：US11850792
申请日：2007-09-06
申请人： Titus Faulkner
发明人： Titus Faulkner
IPC分类号： C01B25/30
CPC分类号： C01B25/45 , H01M4/5825 , H01M10/0525
摘要： The present invention provides for the two step preparation of lithium vanadium phosphate by pre-treatment of a mixture of precursor materials via high pressure at relatively low temperatures in water (hydrothermal pretreatment) and then calcining such hydrothermally pretreated precursors at relatively high temperatures for a period of time sufficient to produce lithium vanadium phosphate. The lithium vanadium phosphate so produced finds use in producing electrodes for electrochemical cells.
摘要翻译：本发明提供了通过在较低温度（水热预处理）中通过高压在高温下预处理前体材料的混合物，然后在相对较高的温度下煅烧这种水热预处理的前体一段时间来提供两步制备磷酸钒锂的时间足以产生磷酸钒锂。所生产的锂钒磷酸盐可用于生产电化学电池的电极。

18. 发明申请

US20070248520A1 METHOD FOR MAKING ELECTRODE ACTIVE MATERIAL 有权
标题翻译：制备电极活性材料的方法
公开(公告)号：US20070248520A1
公开(公告)日：2007-10-25
申请号：US11379754
申请日：2006-04-21
申请人： Titus Faulkner
发明人： Titus Faulkner
IPC分类号： C01B25/26
CPC分类号： C01B25/45 , B01J27/198 , C01G31/006 , C01P2002/72 , C01P2006/40 , H01M4/136 , H01M4/5825 , H01M10/052
摘要： The present invention is directed to a method for making electrode active materials represented by the general formula: Aa(VO)bXO4, wherein: (a) A is an alkali metal or mixture of alkali metals, and 0
摘要翻译：本发明涉及一种制备由以下通式表示的电极活性材料的方法：<？in-line-formula description =“In-line Formulas”end =“lead”？> A （VO）在线公式描述=“在线公式”end =“tail”？>其中：（a）A 碱金属或碱金属的混合物，0

19. 发明授权

US06517803B2 Highly crystalline Mn2O3 or Mn3O4 manganese oxides 失效
标题翻译：高结晶的Mn2O3或Mn3O4锰氧化物
公开(公告)号：US06517803B2
公开(公告)日：2003-02-11
申请号：US09842968
申请日：2001-04-26
申请人： Vesselin Manev , Titus Faulkner , D. Wayne Barnette
发明人： Vesselin Manev , Titus Faulkner , D. Wayne Barnette
IPC分类号： C01G4502
CPC分类号： H01M4/505 , C01G45/02 , C01G45/1242 , C01G53/54 , C01P2002/32 , C01P2002/52 , C01P2002/54 , C01P2004/03 , C01P2006/10 , C01P2006/11 , C01P2006/12 , C01P2006/14 , C01P2006/40
摘要： The present invention includes lithium manganese oxide spinel compounds having a low porosity, a high tap density and a high pellet density, and methods of preparing these compounds. In particular, the method comprises preparing a lithium manganese oxide with a spinel structure and having the formula: wherein: Li1+XMn2−YMm11Mm22 . . . MmkkO4+Z M1, M2, . . . Mk are cations different than lithium or manganese selected from the group consisting of alkaline earth metals, transition metals, B, Al, Si, Ga and Ge; X, Y, m1, m2, . . . , mk, each have a value between 0 and 0.2; Z has a value between −0.1 and 0.2; and X, Y, m1, m2, . . . mk are selected to satisfy the equation: Y=X+m1+m2+ . . . +mk.
摘要翻译：本发明包括具有低孔隙率，高振实密度和高颗粒密度的锂锰氧化物尖晶石化合物以及这些化合物的制备方法。特别地，该方法包括制备具有尖晶石结构的锂锰氧化物并具有下式：其中：M1，M2，...。。。 Mk是选自碱土金属，过渡金属，B，Al，Si，Ga和Ge中的锂或锰的阳离子; X，Y，m1，m2。。。，mk各自具有介于0和0.2之间的值; Z具有介于-0.1和0.2之间的值; 和X，Y，m1，m2。。。 mk被选择以满足等式：

20. 发明授权

US06267943B1 Lithium manganese oxide spinel compound and method of preparing same 失效
标题翻译：锂锰氧化物尖晶石化合物及其制备方法
公开(公告)号：US06267943B1
公开(公告)日：2001-07-31
申请号：US09418352
申请日：1999-10-14
申请人： Vesselin Manev , Titus Faulkner , D. Wayne Barnette
发明人： Vesselin Manev , Titus Faulkner , D. Wayne Barnette
IPC分类号： C01G4502
CPC分类号： H01M4/505 , C01G45/02 , C01G45/1242 , C01G53/54 , C01P2002/32 , C01P2002/52 , C01P2002/54 , C01P2004/03 , C01P2006/10 , C01P2006/11 , C01P2006/12 , C01P2006/14 , C01P2006/40
摘要： The present invention includes lithium manganese oxide spinel compounds having a low porosity, a high tap density and a high pellet density, and methods of preparing these compounds. In particular, the method comprises preparing a lithium manganese oxide with a spinel structure and having the formula: wherein: Li1+XMn2−YM1m1M2m2 . . . MkmkO4+Z M1, M2, . . . Mk are cations different than lithium or manganese selected from the group consisting of alkaline earth metals, transition metals, B, Al, Si, Ga and Ge; X, Y, m1, m2, . . . , mk, each have a value between 0 and 0.2; Z has a value between −0.1 and 0.2; and X, Y, m1, m2, . . . mk are selected to satisfy the equation: Y=X+m1+m2+ . . . +mk.
摘要翻译：本发明包括具有低孔隙率，高振实密度和高颗粒密度的锂锰氧化物尖晶石化合物，以及这些化合物的制备方法。特别地，该方法包括制备具有尖晶石结构的锂锰氧化物并具有下式：其中：M1，M2，...。。。 Mk是选自碱土金属，过渡金属，B，Al，Si，Ga和Ge中的锂或锰的阳离子; X，Y，m1，m2。。。，mk各自具有介于0和0.2之间的值; Z具有介于-0.1和0.2之间的值; 和X，Y，m1，m2。。。 mk被选择以满足等式：

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