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    • 8. 发明申请
    • NANOCOMPOSITES CONTAINING SILICA NANOPARTICLES AND DISPERSANT, COMPOSITES, ARTICLES, AND METHODS OF MAKING SAME
    • 含有二氧化硅纳米颗粒和分散剂的纳米复合材料,复合材料,制品及其制备方法
    • US20160200898A1
    • 2016-07-14
    • US14911058
    • 2014-08-12
    • 3M INNOVATIVE PROPERTIES COMPANY
    • Peter D. CondoJeremy O. SwansonJames E. ThorsonKristin L. Thunhorst
    • C08K9/04
    • A nanocomposite is provided including silica nanoparticles and a dispersant dispersed in a curable resin or a curing agent, where the nanocomposite contains less than 2% by weight solvent. The silica nanoparticles include nonspherical silica nanoparticles and/or spherical pyrogenic silica nanoparticles. A composite is also provided including from about 4 to 70 weight percent of silica nanoparticles, and a dispersant, dispersed in a cured resin, and a filler embedded in the cured resin. Optionally, the composite further contains a curing agent. Further, a method of preparing a nanoparticle-containing curable resin system is provided including mixing from 10 to 70 weight percent of aggregated silica nanoparticles with a curable resin and a dispersant to form a mixture. The mixture contains less than 2% by weight solvent. The method also includes milling the mixture in an immersion mill containing milling media to form a milled resin system including silica nanoparticles dispersed in the curable resin.
    • 提供纳米复合材料,其包括分散在可固化树脂或固化剂中的二氧化硅纳米颗粒和分散剂,其中纳米复合材料含有小于2重量%的溶剂。 二氧化硅纳米颗粒包括非球形二氧化硅纳米颗粒和/或球形致热二氧化硅纳米颗粒。 还提供了包含约4-70重量%的二氧化硅纳米颗粒和分散在固化树脂中的分散剂和嵌入固化树脂中的填料的复合材料。 任选地,复合物还含有固化剂。 此外,提供了制备含纳米颗粒的可固化树脂体系的方法,包括将10至70重量%的聚集二氧化硅纳米颗粒与可固化树脂和分散剂混合以形成混合物。 该混合物含有小于2重量%的溶剂。 该方法还包括在含有研磨介质的浸轧机中研磨混合物以形成包含分散在可固化树脂中的二氧化硅纳米颗粒的研磨树脂体系。