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1. 发明申请

US20080119678A1 Olefin metathesis catalysts and related methods 有权
标题翻译：烯烃复分解催化剂及相关方法
公开(公告)号：US20080119678A1
公开(公告)日：2008-05-22
申请号：US11603951
申请日：2006-11-22
申请人： Adam S. Hock , Richard R. Schrock
发明人： Adam S. Hock , Richard R. Schrock
IPC分类号： B01J31/00 , C07C2/00
CPC分类号： B01J31/2295 , B01J31/122 , B01J31/1805 , B01J31/181 , B01J31/2234 , B01J31/2265 , B01J31/2291 , B01J2231/482 , B01J2231/54 , B01J2231/543 , B01J2531/64 , B01J2531/66 , C07C6/04 , C07C2531/22
摘要： The present invention provides methods for the synthesis of catalysts and precursors thereof. Methods of the invention may comprise combining a catalyst precursor and at least one ligand to generate a catalytically active species, often under mild conditions and in high yields. In some cases, a wide variety of catalysts may be synthesized from a single catalyst precursor. Methods of the invention may also include the preparation of catalysts which, under reaction conditions known in the art, may have been difficult or impossible to prepare and/or isolate due to, for example, steric crowding at the metal center. The present invention also provides catalyst compositions, and precursors thereof, which may be useful in various chemical reactions including olefin metathesis. In some cases, methods of the invention may reduce the number of synthetic and purification steps required to produce catalysts and/or other reaction products, as well as reducing time, cost, and waste production.
摘要翻译：本发明提供合成催化剂及其前体的方法。本发明的方法可以包括将催化剂前体和至少一种配体结合以产生催化活性物质，通常在温和条件下和高产率下。在一些情况下，可以从单一催化剂前体合成多种催化剂。本发明的方法还可以包括催化剂的制备，其在本领域已知的反应条件下可能由于例如在金属中心的空间拥挤而难以或不可能制备和/或分离。本发明还提供催化剂组合物及其前体，其可用于包括烯烃复分解的各种化学反应。在一些情况下，本发明的方法可以减少制备催化剂和/或其它反应产物所需的合成和纯化步骤的数量，以及减少时间，成本和废物的产生。

2. 发明申请

US20110237815A1 OLEFIN METATHESIS CATALYSTS AND RELATED METHODS 有权
标题翻译： OLEFIN METATHESIS催化剂及相关方法
公开(公告)号：US20110237815A1
公开(公告)日：2011-09-29
申请号：US13033472
申请日：2011-02-23
申请人： Adam S. Hock , Richard R. Schrock
发明人： Adam S. Hock , Richard R. Schrock
IPC分类号： C07F11/00
CPC分类号： B01J31/2295 , B01J31/122 , B01J31/1805 , B01J31/181 , B01J31/2234 , B01J31/2265 , B01J31/2291 , B01J2231/482 , B01J2231/54 , B01J2231/543 , B01J2531/64 , B01J2531/66 , C07C6/04 , C07C2531/22
摘要： The present invention provides methods for the synthesis of catalysts and precursors thereof. Methods of the invention may comprise combining a catalyst precursor and at least one ligand to generate a catalytically active species, often under mild conditions and in high yields. In some cases, a wide variety of catalysts may be synthesized from a single catalyst precursor. Methods of the invention may also include the preparation of catalysts which, under reaction conditions known in the art, may have been difficult or impossible to prepare and/or isolate due to, for example, steric crowding at the metal center. The present invention also provides catalyst compositions, and precursors thereof, which may be useful in various chemical reactions including olefin metathesis. In some cases, methods of the invention may reduce the number of synthetic and purification steps required to produce catalysts and/or other reaction products, as well as reducing time, cost, and waste production.
摘要翻译：本发明提供合成催化剂及其前体的方法。本发明的方法可以包括将催化剂前体和至少一种配体结合以产生催化活性物质，通常在温和条件下和高产率下。在一些情况下，可以从单一催化剂前体合成多种催化剂。本发明的方法还可以包括催化剂的制备，其在本领域已知的反应条件下可能由于例如在金属中心的空间拥挤而难以或不可能制备和/或分离。本发明还提供催化剂组合物及其前体，其可用于包括烯烃复分解的各种化学反应。在一些情况下，本发明的方法可以减少制备催化剂和/或其它反应产物所需的合成和纯化步骤的数量，以及减少时间，成本和废物的产生。

3. 发明授权

US08350073B2 Olefin metathesis catalysts and related methods 有权
标题翻译：烯烃复分解催化剂及相关方法
公开(公告)号：US08350073B2
公开(公告)日：2013-01-08
申请号：US13033472
申请日：2011-02-23
申请人： Adam S. Hock , Richard R. Schrock
发明人： Adam S. Hock , Richard R. Schrock
IPC分类号： C07F11/00
CPC分类号： B01J31/2295 , B01J31/122 , B01J31/1805 , B01J31/181 , B01J31/2234 , B01J31/2265 , B01J31/2291 , B01J2231/482 , B01J2231/54 , B01J2231/543 , B01J2531/64 , B01J2531/66 , C07C6/04 , C07C2531/22
摘要： The present invention provides methods for the synthesis of catalysts and precursors thereof. Methods of the invention may comprise combining a catalyst precursor and at least one ligand to generate a catalytically active species, often under mild conditions and in high yields. In some cases, a wide variety of catalysts may be synthesized from a single catalyst precursor. Methods of the invention may also include the preparation of catalysts which, under reaction conditions known in the art, may have been difficult or impossible to prepare and/or isolate due to, for example, steric crowding at the metal center. The present invention also provides catalyst compositions, and precursors thereof, which may be useful in various chemical reactions including olefin metathesis. In some cases, methods of the invention may reduce the number of synthetic and purification steps required to produce catalysts and/or other reaction products, as well as reducing time, cost, and waste production.
摘要翻译：本发明提供合成催化剂及其前体的方法。本发明的方法可以包括将催化剂前体和至少一种配体结合以产生催化活性物质，通常在温和条件下和高产率下。在一些情况下，可以从单一催化剂前体合成多种催化剂。本发明的方法还可以包括催化剂的制备，其在本领域已知的反应条件下可能由于例如在金属中心的空间拥挤而难以或不可能制备和/或分离。本发明还提供催化剂组合物及其前体，其可用于包括烯烃复分解的各种化学反应。在一些情况下，本发明的方法可以减少制备催化剂和/或其它反应产物所需的合成和纯化步骤的数量，以及减少时间，成本和废物的产生。

4. 发明授权

US07932397B2 Olefin metathesis catalysts and related methods 有权
标题翻译：烯烃复分解催化剂及相关方法
公开(公告)号：US07932397B2
公开(公告)日：2011-04-26
申请号：US11603951
申请日：2006-11-22
申请人： Adam S. Hock , Richard R. Schrock
发明人： Adam S. Hock , Richard R. Schrock
IPC分类号： C07F11/00 , B01J31/00
CPC分类号： B01J31/2295 , B01J31/122 , B01J31/1805 , B01J31/181 , B01J31/2234 , B01J31/2265 , B01J31/2291 , B01J2231/482 , B01J2231/54 , B01J2231/543 , B01J2531/64 , B01J2531/66 , C07C6/04 , C07C2531/22
摘要： The present invention provides methods for the synthesis of catalysts and precursors thereof. Methods of the invention may comprise combining a catalyst precursor and at least one ligand to generate a catalytically active species, often under mild conditions and in high yields. In some cases, a wide variety of catalysts may be synthesized from a single catalyst precursor. Methods of the invention may also include the preparation of catalysts which, under reaction conditions known in the art, may have been difficult or impossible to prepare and/or isolate due to, for example, steric crowding at the metal center. The present invention also provides catalyst compositions, and precursors thereof, which may be useful in various chemical reactions including olefin metathesis. In some cases, methods of the invention may reduce the number of synthetic and purification steps required to produce catalysts and/or other reaction products, as well as reducing time, cost, and waste production.
摘要翻译：本发明提供合成催化剂及其前体的方法。本发明的方法可以包括将催化剂前体和至少一种配体结合以产生催化活性物质，通常在温和条件下和高产率下。在一些情况下，可以从单一催化剂前体合成多种催化剂。本发明的方法还可以包括催化剂的制备，其在本领域已知的反应条件下可能由于例如在金属中心的空间拥挤而难以或不可能制备和/或分离。本发明还提供催化剂组合物及其前体，其可用于包括烯烃复分解的各种化学反应。在一些情况下，本发明的方法可以减少制备催化剂和/或其它反应产物所需的合成和纯化步骤的数量，以及减少时间，成本和废物的产生。

5. 发明授权

US08796483B2 Cyclic metal amides and vapor deposition using them 有权
标题翻译：使用它们的环状金属酰胺和气相沉积
公开(公告)号：US08796483B2
公开(公告)日：2014-08-05
申请号：US13077241
申请日：2011-03-31
申请人： Roy G. Gordon , Adam S. Hock , Jaeyeong Heo , Prasert Sinsermsuksakul
发明人： Roy G. Gordon , Adam S. Hock , Jaeyeong Heo , Prasert Sinsermsuksakul
IPC分类号： C07F7/22 , C07F7/24 , C23C16/00
CPC分类号： C07F7/003 , C23C16/18 , C23C16/305 , C23C16/407 , C23C16/45553
摘要： Novel cyclic amides containing tin or lead are disclosed. These cyclic amides can be used for atomic layer deposition or chemical vapor deposition of tin or lead as well as their oxides, sulfides, selenides, nitrides, phosphides, carbides, silicides or borides or other compounds. Tin(IV) oxide, SnO2, films were deposited by reaction of a cyclic tin amide vapor and H2O2 or NO2 as oxygen sources. The films have high purity, smoothness, transparency, electrical conductivity, density, and uniform thickness even inside very narrow holes or trenches. Deposition temperatures are low enough for thermally sensitive substrates such as plastics. Suitable applications of these films include displays, light-emitting diodes, solar cells and gas sensors. Doping SnO2 with aluminum was used to reduce its conductivity, making material suitable as the active semiconductor layer in electron multipliers or transparent transistors. Deposition using the same tin precursor and H2S deposited tin monosulfide, SnS, a material suitable for solar cells.
摘要翻译：公开了含有锡或铅的新型环状酰胺。这些环状酰胺可用于锡或铅及其氧化物，硫化物，硒化物，氮化物，磷化物，碳化物，硅化物或硼化物或其它化合物的原子层沉积或化学气相沉积。通过环状锡酰胺蒸气和H 2 O 2或NO 2作为氧源反应沉积氧化锡（IV），SnO 2。即使在非常狭窄的孔或沟槽内，这些膜也具有高纯度，平滑度，透明度，导电性，密度和均匀的厚度。沉积温度对于热敏基材如塑料来说足够低。这些膜的合适应用包括显示器，发光二极管，太阳能电池和气体传感器。使用铝掺杂SnO2以降低其导电性，使得材料适合作为电子倍增器或透明晶体管中的有源半导体层。沉积使用相同的锡前体和H2S沉积锡一硫化物，SnS，适合太阳能电池的材料。

6. 发明申请

US20120027937A1 Cyclic Metal Amides and Vapor Deposition Using Them 有权
标题翻译：使用它们的循环金属酰胺和气相沉积
公开(公告)号：US20120027937A1
公开(公告)日：2012-02-02
申请号：US13077241
申请日：2011-03-31
申请人： Roy G. Gordon , Adam S. Hock , Jaeyeong Heo , Prasert Sinsermsuksakul
发明人： Roy G. Gordon , Adam S. Hock , Jaeyeong Heo , Prasert Sinsermsuksakul
IPC分类号： B05D1/38 , C07F7/22 , C07F5/02 , C07F9/02 , C07F7/02 , B05D3/10 , C07F7/24
CPC分类号： C07F7/003 , C23C16/18 , C23C16/305 , C23C16/407 , C23C16/45553
摘要： Novel cyclic amides containing tin or lead are disclosed. These cyclic amides can be used for atomic layer deposition or chemical vapor deposition of tin or lead as well as their oxides, sulfides, selenides, nitrides, phosphides, carbides, silicides or borides or other compounds. Tin(IV) oxide, SnO2, films were deposited by reaction of a cyclic tin amide vapor and H2O2 or NO2 as oxygen sources. The films have high purity, smoothness, transparency, electrical conductivity, density, and uniform thickness even inside very narrow holes or trenches. Deposition temperatures are low enough for thermally sensitive substrates such as plastics. Suitable applications of these films include displays, light-emitting diodes, solar cells and gas sensors. Doping SnO2 with aluminum was used to reduce its conductivity, making material suitable as the active semiconductor layer in electron multipliers or transparent transistors. Deposition using the same tin precursor and H2S deposited tin monosulfide, SnS, a material suitable for solar cells.
摘要翻译：公开了含有锡或铅的新型环状酰胺。这些环状酰胺可用于锡或铅及其氧化物，硫化物，硒化物，氮化物，磷化物，碳化物，硅化物或硼化物或其它化合物的原子层沉积或化学气相沉积。通过环状锡酰胺蒸气和H 2 O 2或NO 2作为氧源反应沉积氧化锡（IV），SnO 2。即使在非常狭窄的孔或沟槽内，这些膜也具有高纯度，平滑度，透明度，导电性，密度和均匀的厚度。沉积温度对于热敏基材如塑料来说足够低。这些膜的合适应用包括显示器，发光二极管，太阳能电池和气体传感器。使用铝掺杂SnO2以降低其导电性，使得材料适合作为电子倍增器或透明晶体管中的有源半导体层。沉积使用相同的锡前体和H2S沉积锡一硫化物，SnS，适合太阳能电池的材料。

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