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1. 发明申请

WO2013039260A2 METHOD FOR PURIFYING CHLORINATED HYDROCARBON 审中-公开
标题翻译：纯化氯化烃的方法
公开(公告)号：WO2013039260A2
公开(公告)日：2013-03-21
申请号：PCT/JP2012074131
申请日：2012-09-13
申请人： DAIKIN IND LTD , CHAKI TAKEHIRO , TAKAHASHI KAZUHIRO , YOSHIMI HITOSHI , TANAKA YOSHINORI , IWANAGA YUUSUKE
发明人： CHAKI TAKEHIRO , TAKAHASHI KAZUHIRO , YOSHIMI HITOSHI , TANAKA YOSHINORI , IWANAGA YUUSUKE
IPC分类号： C07C17/38
CPC分类号： C07C17/383 , C07C17/206 , C07C17/25 , C07C17/38 , Y02P20/582 , C07C19/10 , C07C21/18 , C07C19/01
摘要： The present invention provides a method for purifying chlorinated hydrocarbon(s), comprising cooling a mixture containing hydrogen fluoride and at least one chlorinated hydrocarbon selected from the group consisting of 2-chloro-3,3,3-trifluoropropene, 2,3-dichloro-3,3-difluoropropene, 1,2,3-trichloro-1,1-difluoropropane, and 1,1,1,2,3-pentachloropropane to cause liquid-liquid separation of the mixture into an upper liquid phase having a high hydrogen fluoride concentration and a lower liquid phase having a high chlorinated hydrocarbon concentration, and a method for purifying a chlorinated hydrocarbon, comprising subjecting the lower liquid phase obtained by the liquid-liquid separation to a distillation operation. According to the present invention, a chlorinated hydrocarbon can be purified by separating and removing hydrogen fluoride from a chlorinated hydrocarbon-hydrogen fluoride mixture under simple and economically advantageous conditions.
摘要翻译：本发明提供了一种纯化氯化烃的方法，该方法包括冷却含有氟化氢和至少一种选自2-氯-3,3,3-三氟丙烯，2,3-二氯 -3,3-二氟丙烯，1,2,3-三氯-1,1-二氟丙烷和1,1,1,2,3-五氯丙烷，以引起混合物的液 - 液分离成具有高氟化氢浓度以及氯代烃浓度高的下层液相的氯化烃精制方法，以及将通过液液分离得到的下层液相进行蒸馏操作的方法。根据本发明，可以通过在简单和经济上有利的条件下从氯化烃 - 氟化氢混合物中分离和除去氟化氢来纯化氯化烃。

2. 发明申请

WO2010050373A3 PROCESS FOR PREPARING 2,3,3,3-TETRAFLUOROPROPENE 审中-公开
标题翻译：制备2,3,3,3-四氯丙烯的方法
公开(公告)号：WO2010050373A3
公开(公告)日：2010-11-25
申请号：PCT/JP2009067971
申请日：2009-10-13
申请人： DAIKIN IND LTD , NOSE MASATOSHI , TAKAHASHI KAZUHIRO , KOMATSU YUZO , SUGIYAMA AKINARI , SHIBANUMA TAKASHI
发明人： NOSE MASATOSHI , TAKAHASHI KAZUHIRO , KOMATSU YUZO , SUGIYAMA AKINARI , SHIBANUMA TAKASHI
IPC分类号： C07C17/087 , C07C17/25 , C07C17/383 , C07C21/18
CPC分类号： C07C17/25 , C07C17/087 , C07C17/383 , C07C21/18 , Y02P20/582 , C07C21/22
摘要： The present invention provides a process for preparing 2,3,3,3-tetrafluoropropene comprising the steps of: (a) reacting 3,3,3-trifluoropropyne with hydrogen fluoride while heating to obtain a product containing 2,3,3,3-tetrafluoropropene; (b) separating the product obtained in Step (a) into Component A containing 2,3,3,3-tetrafluoropropene and 3,3,3-trifluoropropyne, and Component B containing 1,3,3,3-tetrafluoropropene; (c) separating 2,3,3,3-tetrafluoropropene and 3,3,3-trifluoropropyne contained in Component A obtained in Step (b) into each compound; (d) conducting a dehydrofluorination reaction by heating Component B obtained in Step (b) in the presence of a catalyst; (e) separating the product obtained in Step (d) into Component C containing 2,3,3,3-tetrafluoropropene and 3,3,3-trifluoropropyne, and Component D containing 1,3,3,3-tetrafluoropropene; (f) separating 2,3,3,3-tetrafluoropropene and 3,3,3-trifluoropropyne contained in Component C obtained in Step (e) into each compound; and (g) conducting a dehydrofluorination reaction by heating Component D obtained in Step (e) in the presence of a catalyst. The present invention provides an effective and industrially applicable process for preparing 2,3,3,3-tetrafluoropropene.
摘要翻译：本发明提供一种制备2,3,3,3-四氟丙烯的方法，包括以下步骤：（a）在加热的同时使3,3,3-三氟丙炔与氟化氢反应，得到含有2,3,3,3-四氟丙烯的产物 -tetrafluoropropene; （b）将步骤（a）中获得的产物分离成含有2,3,3,3-四氟丙烯和3,3,3-三氟丙炔的组分A，以及含有1,3,3,3-四氟丙烯的组分B; （c）将步骤（b）中获得的组分A中所含的2,3,3,3-四氟丙烯和3,3,3-三氟丙炔分离成各化合物; （d）通过加热步骤（b）中获得的组分B在催化剂存在下进行脱氟化氢反应; （e）将步骤（d）中获得的产物分离成含有2,3,3,3-四氟丙烯和3,3,3-三氟丙炔的组分C，以及含有1,3,3,3-四氟丙烯的组分D; （f）将步骤（e）中获得的组分C中所含的2,3,3,3-四氟丙烯和3,3,3-三氟丙炔分离成各化合物; 和（g）通过加热在步骤（e）中获得的组分D在催化剂存在下进行脱氟化氢反应。本发明提供了制备2,3,3,3-四氟丙烯的有效和工业上适用的方法。

3. 发明申请

WO2010024366A2 AZEOTROPIC OR AZEOTROPE-LIKE COMPOSITION AND PROCESS FOR PRODUCING 2,3,3,3-TETRAFLUOROPROPENE 审中-公开
标题翻译：共沸或类共沸组合物及生产2,3,3,3-四氟丙烯的方法
公开(公告)号：WO2010024366A2
公开(公告)日：2010-03-04
申请号：PCT/JP2009065023
申请日：2009-08-21
申请人： DAIKIN IND LTD , TAKAHASHI KAZUHIRO
发明人： TAKAHASHI KAZUHIRO
IPC分类号： C07C17/383 , C07C21/18
CPC分类号： C09K5/10 , C07C17/383 , C07C21/18 , C09K2205/24 , C09K2205/32 , C09K2205/40
摘要： The present invention provides a process for producing 2,3,3,3-tetrafluoropropene, comprising distilling a mixture of water and 2,3,3,3-tetrafluoropropene to separate the mixture into a first stream and a second stream, the first stream containing 2,3,3,3-tetrafluoropropene with a water content higher than the original mixture, and the second stream containing 2,3,3,3-tetrafluoropropene with a water content lower than the original mixture; and obtaining 2,3,3,3-tetrafluoropropene with a reduced water content from the second stream. The process of the invention can efficiently remove water from 2,3,3,3-tetrafluoropropene (HFO-1234yf).
摘要翻译：本发明提供了生产2,3,3,3-四氟丙烯的方法，包括蒸馏水和2,3,3,3-四氟丙烯的混合物以将混合物分离成第一物流和第二物流，第一物流含水量高于原始混合物的2,3,3,3-四氟丙烯和含水量低于原始混合物的第二流体含2,3,3,3-四氟丙烯; 并从第二物流获得具有降低的水含量的2,3,3,3-四氟丙烯。本发明的方法可以有效地从2,3,3,3-四氟丙烯（HFO-1234yf）中除去水。

4. 发明申请

WO2009064022A3 PROCESS FOR PRODUCING ( Z) - AND (E) -1, 1, 1, 2, 3-PENTAFLUOROPROPENE 审中-公开
标题翻译：（Z） - 和（E）-1,1,2,3-三氟苯酚的制备方法
公开(公告)号：WO2009064022A3
公开(公告)日：2009-07-09
申请号：PCT/JP2008071063
申请日：2008-11-13
申请人： DAIKIN IND LTD , TAKAHASHI KAZUHIRO
发明人： TAKAHASHI KAZUHIRO
IPC分类号： C07C17/358 , C07C17/383 , C07C21/18
CPC分类号： C07C17/358 , C07B2200/09 , C07C17/25 , C07C17/383 , C07C21/18
摘要： A mixture comprising a Z-isomer and an E-isomer of 1,1,1,2,3-pentafluoropropene (HFC-1225ye) is distilled to separate it into a first stream composed substantially of either one of the Z-isomer and the E-isomer, and a second stream comprising the Z-isomer and the E-isomer; and the second stream is subjected to an isomerization reaction to obtain a third stream having an increased ratio of the one isomer therein from that in the second stream; and then the third stream is reused as at least a part of the above mixture as a raw material. The order of the isomerization reaction and the distillation may be reversed. Thus, either one of the Z-isomer and E-isomer can be efficiently produced.
摘要翻译：将包含1,1,1,2,3-五氟丙烯（HFC-1225ye）的Z-异构体和E-异构体的混合物蒸馏，将其分离成基本上由Z-异构体和 E-异构体和包含Z-异构体和E-异构体的第二物流; 使第二物流进行异构化反应，得到与第二物流中的一种异构体的比率增加的第三物流; 然后将第三流作为原料的上述混合物的至少一部分再利用。异构化反应和蒸馏的顺序可以颠倒。因此，可以有效地制备Z-异构体和E-异构体之一。

5. 发明公开

EP2223906A4 METHOD FOR PRODUCING FLUORINE-CONTAINING OLEFIN 有权
标题翻译：用于生产含氟烯烃
公开(公告)号：EP2223906A4
公开(公告)日：2011-02-09
申请号：EP08852480
申请日：2008-11-11
申请人： DAIKIN IND LTD
发明人： TAKAHASHI KAZUHIRO , NOSE MASATOSHI , CHAKI TAKEHIRO
IPC分类号： C07C17/25 , C07B61/00 , C07C21/18
CPC分类号： C07B39/00 , C07C17/25 , C07C21/18

6. 发明公开

EP1110936A4 PROCESS FOR PRODUCING FLUOROETHANE 有权
标题翻译：用于生产氟
公开(公告)号：EP1110936A4
公开(公告)日：2003-07-16
申请号：EP99929890
申请日：1999-07-16
申请人： DAIKIN IND LTD
发明人： TAKAHASHI KAZUHIRO , KONO SATORU , SHIBANUMA TAKASHI
IPC分类号： B01J27/12 , B01J27/132 , C07B61/00 , C07C17/087 , C07C17/20 , C07C17/21 , C07C19/08 , C07C19/12
CPC分类号： C07C17/206 , B01J27/132 , C07C17/21 , C07C19/08
摘要： A process for producing fluoroethanes consisting mainly of 1,1,1,2-pentafluoroethane by fluorinating at least one member selected from the group consisting of tetrachloroethylene, 2,2-dichloro-1,1,1-trifluoroethane, and 2-chloro-1,1,1,2-tetrafluoroethane with hydrogen fluoride with the aid of chromium oxyfluoride having a fluorine content of 30 wt.% or higher. The process can be carried out while minimizing the generation of CFC's.

7. 发明公开

EP1024124A4 PROCESS FOR THE PREPARATION OF 1,1,1,2,2-PENTAFLUOROETHANE 有权
标题翻译：用于生产1,1,1,2,2-五氟乙烷
公开(公告)号：EP1024124A4
公开(公告)日：2001-03-28
申请号：EP98945624
申请日：1998-10-06
申请人： DAIKIN IND LTD
发明人： KONO SATORU , SHIBANUMA TAKASHI , KANEMURA TAKASHI , YOSHIMURA TOSHIKAZU , TAKAHASHI KAZUHIRO
IPC分类号： B01J27/132 , C07B61/00 , C07C17/20 , C07C19/08 , B01J23/26 , B01J27/12 , B01J37/26
CPC分类号： B01J27/132 , C07C17/206 , Y02P20/582 , C07C19/08
摘要： A process for the preparation of 1,1,1,2,2-pentafluoroethane by fluorinating a halohydro-carbonaceous feedstock containing 2-chloro-1,1,1,2-tetrafluoroethane with hydrogen fluoride in a gas phase, characterized in that: (i) a chromium fluoride oxide obtained by fluorinating a chromium oxide represented by the composition formula: CrOm (wherein 1.5

8. 发明公开

EP3170804A4 METHOD FOR PRODUCING CHLOROPROPENE AND METHOD FOR PRODUCING 2,3,3,3-TETRAFLUOROPROPENE 审中-公开
公开(公告)号：EP3170804A4
公开(公告)日：2018-03-14
申请号：EP15821671
申请日：2015-06-16
申请人： DAIKIN IND LTD
发明人： TAKAKUWA TATSUYA , TAKAHASHI KAZUHIRO , KARUBE DAISUKE , CHAKI TAKEHIRO , KISHIMOTO MASAYUKI , KOMATSU YUZO
IPC分类号： C07C17/20 , C01B7/19 , C07C17/25 , C07C17/383 , C07C21/18
CPC分类号： C07C17/25 , B01D3/143 , B01J23/26 , C01B7/195 , C01B7/196 , C07C17/206 , C07C17/383 , Y02P20/582 , C07C21/18
摘要： This invention provides a method for stably producing 2,3,3,3-tetrafluoropropene for a long period of time wherein unreacted materials are reused after distillation without liquid-liquid separation to suppress catalyst deactivation. The method for producing 2,3,3,3-tetrafluoropropene comprises the step of reacting 1233xf or like chloropropene with hydrogen fluoride in the presence of a catalyst, the step of subjecting the reaction mixture obtained in the above step to distillation to separate the mixture into a first stream comprising 2,3,3,3-tetrafluoropropene as a main component and a second stream comprising unreacted hydrogen fluoride and organic matter containing unreacted chloropropene as main components, and the step of recycling the second stream to the above reaction, the distillation being performed under conditions in which the unreacted hydrogen fluoride and the organic matter containing the unreacted chloropropene do not undergo liquid-liquid separation at a portion of a distillation column from which the second stream is withdrawn.

9. 发明公开

EP3040326A4 HALO-OLEFIN COMPOSITION 审中-公开
标题翻译： HALOOLEFINZUSAMMENSETZUNG
公开(公告)号：EP3040326A4
公开(公告)日：2017-07-05
申请号：EP15760361
申请日：2015-08-10
申请人： DAIKIN IND LTD
发明人： TAKAHASHI KAZUHIRO , TSUCHIYA TATSUMI , YAMADA YASUFU
IPC分类号： C09K5/04 , C07C21/18 , C10M171/00
CPC分类号： C09K5/045 , A62D1/0035 , B01F17/0035 , C09K3/00 , C09K3/30 , C09K2205/126 , C09K2205/22 , C09K2205/40 , C10M171/008 , C10M2209/1033 , C10N2220/302 , C10N2230/66 , C11D7/30
摘要： The present invention provides a highly stable haloolefin-based composition that inhibits decomposition or oxidization. The haloolefin-based composition comprising (a) a haloolefin; (b) at least one compound selected from the group consisting of HFO-1234ze, HFC-254eb, HFO-1243zf, HFC-245eb, HFC-245fa, HFC-245cb, HFC-236ea, HFC-236fa, HFO-1225ye, 3,3,3-trifluoropropine, HFC-23, HFC-32, HFC-125, HFC-143a, HFC-134a, FC-1216, HCFO-1233xf, HCFO-1233zd, HCFO-1232xf, HCFO-1223xd, and chloromethane; and (c) water.
摘要翻译：本发明提供抑制分解或氧化的高度稳定的基于卤烯烃的组合物。所述基于卤烯烃的组合物包含（a）卤烯烃; （b）至少一种选自HFO-1234ze，HFC-254eb，HFO-1243zf，HFC-245eb，HFC-245fa，HFC-245cb，HFC-236ea，HFC-236fa，HFO-1225ye，3 ，HFC-23，HFC-32，HFC-125，HFC-143a，HFC-134a，FC-1216，HCFO-1233xf，HCFO-1233zd，HCFO-1232xf，HCFO-1223xd和氯甲烷; 和（c）水。

10. 发明公开

EP3020695A4 METHOD FOR PRODUCING 2,3,3,3-TETRAFLUOROPROPENE 审中-公开
标题翻译： VERFAHREN ZUR HERSTELLUNG VON 2,3,3,3-TETRAFLUORPROPEN
公开(公告)号：EP3020695A4
公开(公告)日：2017-03-15
申请号：EP14823042
申请日：2014-07-08
申请人： DAIKIN IND LTD
发明人： CHAKI TAKEHIRO , TAKAHASHI KAZUHIRO , TAKAKUWA TATSUYA
IPC分类号： C07C17/20 , C07C17/25 , C07C21/18
CPC分类号： C07C17/087 , C07C17/202 , C07C17/206 , C07C17/25 , C07C17/383 , Y02P20/582 , C07C21/18 , C07C19/10
摘要： This invention provides a method for producing 2,3,3,3-tetrafluoropropene or 2-chloro-1,1,1,2-tetrafluoropropane, which is a precursor of 2,3,3,3-tetrafluoropropene, in two or three reaction steps, using at least one chlorine-containing compound selected from the group consisting of 1,1,1,2,3-pentachloropropane, 2,3-dichloro-1,1,1-trifluoropropane, and 1,1,2,3-tetrachloropropene as a starting material, the reaction products of at least two of the steps being supplied to the same distillation apparatus to subject the products to a separation operation simultaneously. With this method, 2,3,3,3-tetrafluoropropene or 2-chloro-1,1,1,2-tetrafluoropropane, which is a precursor of 2,3,3,3-tetrafluoropropene, can be efficiently produced with reduced energy and equipment costs in an economically advantageous manner.
摘要翻译：本发明提供一种2,3,3,3-四氟丙烯的前体2,3,3,3-四氟丙烯或2-氯-1,1,1,2-四氟丙烷的制造方法，其特征在于，反应步骤，使用至少一种选自1,1,1,2,3-五氯丙烷，2,3-二氯-1,1,1-三氟丙烷和1,1,2-三氯丙烷的含氯化合物， 3-四氯丙烯作为起始原料，将至少两个步骤的反应产物提供给同一蒸馏装置，以使产物同时进行分离操作。利用该方法，能够以降低的能量有效地生产作为2,3,3,3-四氟丙烯的前体的2,3,3,3-四氟丙烯或2-氯-1,1,1,2-四氟丙烷以及经济上有利的设备成本。

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