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1. 发明授权

US06395431B1 Electrolytes having improved stability comprising an N,N-dialkylamide additive 有权
标题翻译：具有改进稳定性的电解质包括N，N-二烷基酰胺添加剂
公开(公告)号：US06395431B1
公开(公告)日：2002-05-28
申请号：US09182392
申请日：1998-10-28
申请人： Feng Gao , Jeremy Barker , Hang Shi , Tracy Kelley , Chariclea Scordilis-Kelley
发明人： Feng Gao , Jeremy Barker , Hang Shi , Tracy Kelley , Chariclea Scordilis-Kelley
IPC分类号： H01M616
CPC分类号： H01M10/0525 , H01M10/0567 , H01M10/0569 , H01M2300/0025
摘要： The invention provides an electrochemical cell having an electrolyte which comprises a solute, a solvent, and an additive. The additive is a dialkylamide. The dialkylamide lessens the extent of decomposition of the solute, which is a lithium salt. The ionic species of the lithium salt are thereby preserved. The additive also prevents damage to active material by absorbing excess charge energy below the breakdown potential of the active material.
摘要翻译：本发明提供一种具有电解质的电化学电池，其包含溶质，溶剂和添加剂。添加剂是二烷基酰胺。二烷基酰胺减少作为锂盐的溶质的分解程度。从而保留锂盐的离子种类。该添加剂还通过吸收低于活性材料的击穿电位的过量的电荷能量来防止对活性材料的损害。

2. 发明授权

US5846673A Additive to stabilize electrochemical cell 失效
标题翻译：添加剂稳定电化学电池
公开(公告)号：US5846673A
公开(公告)日：1998-12-08
申请号：US762079
申请日：1996-12-09
申请人： M. Yazid Saidi , Feng Gao , Jeremy Barker , Chariclea Scordilis-Kelley
发明人： M. Yazid Saidi , Feng Gao , Jeremy Barker , Chariclea Scordilis-Kelley
IPC分类号： H01M4/131 , H01M4/133 , H01M4/50 , H01M4/505 , H01M4/62 , H01M10/0525 , H01M10/0567 , H01M10/36 , H01M10/40
CPC分类号： H01M10/0567 , H01M4/131 , H01M4/133 , H01M4/62 , H01M10/0525 , H01M4/505 , Y10T29/49108
摘要： The present invention provides a novel composition and method for preventing decomposition of one or more electrochemical cell components comprising an electrode having an active material, and an electrolyte. The method of the invention, for the first time, effectively overcomes problems which arise between the interaction of cell components and contaminate water retained in a cell. Such contaminate water reacts with the electrolyte which comprises a salt of lithium in a solvent. Solubilizing of the salt in solution with attendant interaction between the salt and water causes formation of hydrogen-containing acids. The method of the invention effectively blocks decomposition of a lithium metal oxide cathode active material, and particularly lithium manganese oxide (LMO, nominally LiMn.sub.2 O.sub.4). Such decomposition is prevented by including in the cell a basic compound which forms an electron donor species in the electrolyte solution; and by neutralizing at least a portion of the acid by reacting the donor species with the hydrogen-containing acids thereby preventing decomposition of the lithium manganese oxide by the acid. The preservation of the lithium manganese oxide prevents degradation of other cell components by other mechanism. The basic compound is desirably an organic base, preferably a butylamine.
摘要翻译：本发明提供一种用于防止一种或多种电化学电池元件分解的新型组合物和方法，所述电化学电池组件包括具有活性材料的电极和电解质。本发明的方法第一次有效地克服了细胞成分的相互作用和污染细胞中残留的水之间产生的问题。这种污染水与包含锂在溶剂中的盐的电解质反应。溶解盐中的盐与盐和水之间伴随的相互作用引起含氢酸的形成。本发明的方法有效地阻止锂金属氧化物正极活性物质，特别是锰酸锂（LMO，名义上是LiMn 2 O 4）的分解。通过在电解液中包含在电解质溶液中形成电子供体物质的碱性化合物来防止这种分解; 并且通过使供体物质与含氢酸反应从而中和酸的至少一部分，从而防止酸分解锰酸锂。锂锰氧化物的保存通过其他机理防止其他电池组分的降解。碱性化合物优选为有机碱，优选为丁胺。

3. 发明授权

US5869207A Stabilized electrochemical cell 失效
标题翻译：稳定电化学电池
公开(公告)号：US5869207A
公开(公告)日：1999-02-09
申请号：US762081
申请日：1996-12-09
申请人： M. Yazid Saidi , Chariclea Scordilis-Kelley , Jeremy Barker
发明人： M. Yazid Saidi , Chariclea Scordilis-Kelley , Jeremy Barker
IPC分类号： C01G45/00 , H01M4/50 , H01M4/505 , H01M4/62 , H01M10/0525 , H01M10/0567 , H01M10/36
CPC分类号： H01M4/505 , C01G45/1221 , C01G45/1242 , H01M10/0567 , H01M4/62 , C01P2006/40 , H01M10/0525
摘要： The present invention provides a novel composition and method for preventing decomposition of one or more electrochemical cell components comprising an electrode having an active material, and an electrolyte. The method of the invention, for the first time, effectively overcomes problems which arise between the interaction of cell components and contaminate water retained in a cell. Such contaminate water reacts with the electrolyte which comprises a salt of lithium in a solvent. Solubilizing of the salt in solution with attendant interaction between the salt and water causes formation of hydrogen-containing acids. The method of the invention effectively blocks decomposition of a lithium metal oxide cathode active material, and particularly lithium manganese oxide (LMO, nominally LiMn.sub.2 O.sub.4). Such decomposition is prevented by including in the cell a basic compound which forms an electron donor species in the electrolyte solution; and by neutralizing at least a portion of the acid by reacting the donor species with the hydrogen-containing acids thereby preventing decomposition of the lithium manganese oxide by the acid. The preservation of the lithium manganese oxide prevents degradation of other cell components by other mechanism.
摘要翻译：本发明提供一种用于防止一种或多种电化学电池元件分解的新型组合物和方法，所述电化学电池组件包括具有活性材料的电极和电解质。本发明的方法第一次有效地克服了细胞成分的相互作用和污染细胞中残留的水之间产生的问题。这种污染水与包含锂在溶剂中的盐的电解质反应。溶解盐中的盐与盐和水之间伴随的相互作用引起含氢酸的形成。本发明的方法有效地阻止锂金属氧化物正极活性物质，特别是锰酸锂（LMO，名义上是LiMn 2 O 4）的分解。通过在电解液中包含在电解质溶液中形成电子供体物质的碱性化合物来防止这种分解; 并且通过使供体物质与含氢酸反应从而中和酸的至少一部分，从而防止酸分解锰酸锂。锂锰氧化物的保存通过其他机理防止其他电池组分的降解。

4. 发明申请

US20060194112A1 Electrodes Comprising Mixed Active Particles 有权
标题翻译：包含混合活性颗粒的电极
公开(公告)号：US20060194112A1
公开(公告)日：2006-08-31
申请号：US11381602
申请日：2006-05-04
申请人： Jeremy Barker , M. Saidi , Tracy Kelley
发明人： Jeremy Barker , M. Saidi , Tracy Kelley
IPC分类号： H01M4/58 , H01M4/50 , H01M4/52 , H01M4/48
CPC分类号： H01M4/525 , H01M4/13 , H01M4/364 , H01M4/505 , H01M4/582 , H01M4/5825 , H01M10/0525
摘要： Electrode active materials comprising two or more groups of particles having differing chemical compositions, wherein each group of particles comprises a material selected from: (a) materials of the formula A1aM1b(XY4)cZd; and (b) materials of the formula A2eM2fOg; and wherein (i) A1, A2, and A3 are Li, Na, or K; (ii) M1 and M3 comprise a transition metal; (iv) XY4 a phosphate or similar moiety; and (v) Z is OH, or halogen.
摘要翻译：包含两组或更多组具有不同化学组成的颗粒的电极活性材料，其中每组颗粒包含选自以下的材料：（a）式A的材料（XY 4）C 1 C 1 H 2 O 2（X 4）和（b）式A的物质 >; 并且其中（i）A 1，A 2和A 3是Li，Na或K; （ii）M 1和M 3 3包含过渡金属; （iv）磷酸酯或类似部分的XY 4; 和（v）Z是OH或卤素。

5. 发明授权

US07771628B2 Electrodes comprising mixed active particles 有权
标题翻译：包含混合活性颗粒的电极
公开(公告)号：US07771628B2
公开(公告)日：2010-08-10
申请号：US11381602
申请日：2006-05-04
申请人： Jeremy Barker , M. Yazid Saidi , Tracy Kelley
发明人： Jeremy Barker , M. Yazid Saidi , Tracy Kelley
IPC分类号： H01B1/08 , H01M4/58
CPC分类号： H01M4/525 , H01M4/13 , H01M4/364 , H01M4/505 , H01M4/582 , H01M4/5825 , H01M10/0525
摘要： Electrode active materials comprising two or more groups of particles having differing chemical compositions, wherein each group of particles comprises a material selected from: (a) materials of the formula A1 aM1 b(XY4)cZd; and (b) materials of the formula A2eM2fOg; and (c) materials of the formula A3hMniO4; wherein (i) A1, A2, and A3 are Li, Na, or K; (ii) M1and M3 comprise a transition metal; (iv) XY4 a phosphate or similar moiety; and (v) Z is OH, or halogen.
摘要翻译：包含两组或更多组具有不同化学组成的颗粒的电极活性材料，其中每组颗粒包括选自以下的材料：（a）式A1aM1b（XY4）cZd的材料; 和（b）式A2eM2fOg的材料; 和（c）式为A3hMniO4的材料; 其中（i）A1，A2和A3是Li，Na或K; （ii）M1和M3包含过渡金属; （iv）XY4磷酸酯或类似部分; 和（v）Z是OH或卤素。

6. 发明授权

US5700298A Carbon anode for lithium ion electrochemical cell 失效
标题翻译：锂阳极用于锂离子电化学电池
公开(公告)号：US5700298A
公开(公告)日：1997-12-23
申请号：US616826
申请日：1996-03-15
申请人： Hang Shi , Jeremy Barker , Rene Koksbang
发明人： Hang Shi , Jeremy Barker , Rene Koksbang
IPC分类号： C01B31/00 , H01M4/02 , H01M4/1393 , H01M4/58 , H01M4/587 , H01M10/0525 , H01M10/36 , H01M6/00 , C01B31/04 , C25B11/12 , H01M4/62
CPC分类号： H01M10/0525 , C01B31/0415 , H01M4/587 , H01M2004/021 , H01M4/1393 , Y02P70/54 , Y10T29/49108
摘要： Increasing the percentage of the 3R phase present in graphite reduces the first capacity loss of anodes employing the so modified graphite. Conversion of 2H phase graphite to 3R phase graphite can be achieved by grinding graphite. Non-aqueous solid electrochemical cells with improved performance can be fabricated by employing intercalation based carbon anodes comprising graphite with high percentage of 3R. When employed in an electrochemical cell, the first cycle capacity loss of only about 10%.
摘要翻译：增加存在于石墨中的3R相的百分比降低了使用这种改性石墨的阳极的第一容量损失。 2H相石墨转化为3R相石墨可以通过研磨石墨来实现。具有改进性能的非水固体电化学电池可以通过采用包含高比例的3R的石墨的基于嵌入的碳阳极来制造。当用于电化学电池时，第一次循环容量损失仅为10％左右。

7. 发明授权

US6015639A Thermally stable, highly conductive salt 失效
标题翻译：热稳定，高导电性盐
公开(公告)号：US6015639A
公开(公告)日：2000-01-18
申请号：US16608
申请日：1998-01-30
申请人： Feng Gao , Jeremy Barker , Peikang Liu
发明人： Feng Gao , Jeremy Barker , Peikang Liu
IPC分类号： H01B1/12 , H01M10/0525 , H01M10/0568 , H01M6/18
CPC分类号： H01M10/0568 , H01B1/122 , H01M10/0525
摘要： The invention provides a new family of compounds and a method of making the compounds. The new compounds are useful as ion conductive salts, and particularly useful as salts for batteries. The compounds of the invention are prepared from three principal reagents, bis (trifluoromethanesufonyl) methane (CF.sub.3 SO.sub.2).sub.2 CH.sub.2 ; benzoyl chloride; and pyridine which facilitates reaction and then is removed. A precursor sodium salt (CF.sub.3 SO.sub.2).sub.2 CHNa is first prepared. Then, equimolar amounts of the precursor sodium salt and pyridine are dissolved in anhydrous acetonitrile. A stoichiometric amount of the selected substitute benzoyl chloride is then added drop by drop. After addition of Li.sub.3 PO.sub.4, there is pyridine release and formation of the product of the aforesaid two reagents. In the benzene ring, R.sub.1, R.sub.2, R.sub.3, R.sub.4, and R.sub.5 are each identical or different and are each independently selected from hydrogen and an electron withdrawing substituent.
摘要翻译：本发明提供一种新的化合物族和一种制备该化合物的方法。新化合物可用作离子导电盐，并且特别用作电池的盐。本发明的化合物由三种主要试剂，二（三氟甲磺酰基）甲烷（CF 3 SO 2）2 CH 2; 苯甲酰氯; 和吡啶，这有助于反应然后被除去。首先制备前体钠盐（CF 3 SO 2）2 CHNa。然后将等摩尔量的前体钠盐和吡啶溶于无水乙腈中。然后逐滴加入化学计量的所选择的替代苯甲酰氯。添加Li3PO4后，存在吡啶释放并形成上述两种试剂的产物。在苯环中，R 1，R 2，R 3，R 4和R 5各自相同或不同，各自独立地选自氢和吸电子取代基。

8. 发明授权

US5922494A Stabilized electrolyte for electrochemical cells and batteries 失效
标题翻译：用于电化学电池和电池的稳定电解质
公开(公告)号：US5922494A
公开(公告)日：1999-07-13
申请号：US843203
申请日：1997-04-14
申请人： Jeremy Barker , Feng Gao
发明人： Jeremy Barker , Feng Gao
IPC分类号： H01M2/16 , H01M10/052 , H01M10/0525 , H01M10/0565 , H01M10/0569 , H01M10/40
CPC分类号： H01M10/0569 , H01M10/052 , H01M10/0565 , H01M10/0525 , H01M2/1613 , H01M2/1653
摘要： An electrochemical cell comprising a first electrode; a counter-electrode which forms an electrochemical couple with the first electrode; and an electrolyte comprising a solvent and a solute. The solvent comprises a dialkyl carbonate of the formula R'OCOOR" where each of R' and R' represents an alkyl, and having at least one of R' and R" selected from the group consisting of non-linear, branched alkyls where R' and R" are preferably different from one another.
摘要翻译：一种电化学电池，包括第一电极; 与第一电极形成电化学耦合的对电极; 以及包含溶剂和溶质的电解质。溶剂包括式R'OCOOR“的二烷基碳酸酯，其中R'和R'各自表示烷基，并且具有选自非直链，支链烷基的R'和R”中的至少一个其中R'和R“优选彼此不同。

9. 发明授权

US5780182A Propylene carbonate based electrolyte for lithium ion electrochemical cell 失效
标题翻译：用于锂离子电化学电池的碳酸亚丙酯基电解质
公开(公告)号：US5780182A
公开(公告)日：1998-07-14
申请号：US742398
申请日：1996-11-04
申请人： Jeremy Barker , Feng Gao
发明人： Jeremy Barker , Feng Gao
IPC分类号： H01M4/58 , H01M10/40
CPC分类号： H01M10/0569 , H01M10/052 , H01M10/0565 , H01M4/587 , Y10T29/49108
摘要： Non-aqueous solid electrochemical cells with improved performance can be fabricated by employing intercalation based carbon anodes comprising graphite, coke, or mixtures thereof, and an electrolyte having an electrolyte solvent formed of propylene carbonate and 4,5-dichloroethylene carbonate. The cells are particularly suited for low temperature applications.
摘要翻译：具有改进性能的非水固体电化学电池可以通过使用包含石墨，焦炭或其混合物的基于嵌入的碳阳极和具有由碳酸丙烯酯和4,5-二氯乙烯碳酸酯形成的电解质溶剂的电解质来制造。这些电池特别适用于低温应用。

10. 发明授权

US5972055A Binary solvent method for battery 失效
标题翻译：电池二元溶剂法
公开(公告)号：US5972055A
公开(公告)日：1999-10-26
申请号：US680421
申请日：1996-07-15
申请人： Feng Gao , Jeremy Barker , Porter H. Mitchell , Jeffrey Swoyer , Arnie Stux
发明人： Feng Gao , Jeremy Barker , Porter H. Mitchell , Jeffrey Swoyer , Arnie Stux
IPC分类号： H01M6/16 , H01M6/18 , H01M10/052 , H01M10/0565 , H01M10/38
CPC分类号： H01M10/052 , H01M10/0565 , H01M6/164 , H01M6/188 , Y10T29/49115
摘要： The subject invention discloses a novel method of providing a binary electrolyte-solvent solution in a solid battery system. A first component of this binary electrolyte solvent system is provided by a material which acts as a plasticizer in the formation of a solid polymeric matrix (separator), composite cathode and/or composite anode, and which also acts as an electrolyte solvent in the completed electrochemical cell. The second component of the binary electrolyte solvent system is an electrolyte solvent, which generally carries the electrolyte salt into the electrolytic cell precursor. The first and second components of the binary electrolyte solvent system mix within the electrolytic cell, dispersing the electrolyte salt throughout the binary electrolyte solvent system. The addition of the electrolyte salt to the electrolytic cell precursor acts to activate the cell precursor, and to form a functional electrolytic cell or battery system.
摘要翻译：本发明公开了一种在固体电池系统中提供二元电解质溶剂溶液的新方法。这种二元电解质溶剂体系的第一个组分由一种在形成固体聚合物基质（分离器），复合阴极和/或复合阳极中作为增塑剂的材料提供，并且还可以在完成后的电解质溶剂电化学电池。二元电解质溶剂系统的第二组分是电解质溶剂，其通常将电解质盐携带到电解槽前体中。二元电解质溶剂系统的第一和第二组分在电解池内混合，将电解质盐分散在整个二元电解质溶剂系统中。将电解质盐添加到电解槽前体中起作用以活化细胞前体，并形成功能性电解池或电池系统。

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