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    • 1. 发明授权
    • Process for the reclamation of spent alkanolamine solution
    • 废链烷醇胺溶液回收方法
    • US06245128B1
    • 2001-06-12
    • US09333196
    • 1999-06-15
    • Joseph T. George, Jr.
    • Joseph T. George, Jr.
    • B01D5314
    • B01D53/526B01D53/1425B01J41/05B01J49/57
    • A process for the reclamation of spent aqueous alkanolamine solutions by contacting a spent aqueous alkanolamine solution with a strong base ion exchange resin for time sufficient to sorb from the aqueous alkanolamine solution at least a portion of the accumulated ions and after a high concentration of ions accumulate on the resin, regenerating the strong base ion exchange resin by: a) purging the resin with water or nitrogen, b) contacting the strong base ion exchange resin with a sodium chloride solution for a time sufficient to remove the ions, c) purging the resin to remove the sodium chloride solution, d) contacting the resin with an alkali metal hydroxide solution, preferably sodium hydroxide, for a time sufficient to convert the resin to a substantially hydroxide form; and e) purging the resin, wherein the ion sorption capacity of the resin is maintained at a substantially constant value.
    • 通过使废水性链烷醇胺溶液与强碱性离子交换树脂接触的时间足以从链烷醇胺溶液中吸收至少一部分积聚的离子并且在高浓度的离子积聚之后使废水性链烷醇胺溶液回收的方法 在树脂上,通过以下步骤再生强碱离子交换树脂:a)用水或氮吹扫树脂,b)使强碱离子交换树脂与氯化钠溶液接触足够时间以除去离子,c) 树脂以除去氯化钠溶液,d)使树脂与碱金属氢氧化物溶液(优选氢氧化钠)接触一段足以将树脂转化为基本氢氧化物形式的时间; 以及e)清洗树脂,其中树脂的离子吸附容量保持在基本恒定的值。