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1. 发明公开

CN103025660A 从生产苏打灰、碳酸氢钠和/或其他衍生物的废料固体中去除杂质无效
公开(公告)号：CN103025660A
公开(公告)日：2013-04-03
申请号：CN201180033567.3
申请日：2011-05-03
申请人：索尔维化学有限公司
发明人： R·O·胡格赫斯 , J·A·莫特 , A·范登多伦 , J·D·菲利普 , D·W·史密斯
IPC分类号： C01D5/16 , C01D7/22 , C01D7/24 , C01D7/28
CPC分类号： C01D5/16 , C01D7/10 , C01D7/12 , C01D7/22 , C01D7/24 , C01D7/28
摘要：一种用于从废料固体中去除杂质，以提供用于生产结晶碳酸钠、碳酸氢盐和/或其他衍生物的工艺的至少一部分合适的结晶器原料的方法。该方法包括：将废料固体接触沥滤液以溶解至少一种杂质和溶解所生成的沥滤残渣。沥滤可包括堆渗透。沥滤液可包括一种结晶器清除液、一种工艺废料流出物、矿井水、或它们的混合物。该方法可以进一步包括在将生成的沥滤残渣溶解以去除另一种杂质期间或之后，添加镁化合物到生成的沥滤残渣。该废料固体优选包括含有这种杂质的一种池固体。该池固体可以从接收一种或多种结晶器清除液和/或一种或多种其他工艺废料流出物的池回收。该池固体可包含碳酸钠、它的任何水合物、碳酸氢钠和/或碳酸氢三钠。要去除的杂质可能包括氯化钠、硫酸钠、硅酸盐、和/或有机物。

2. 发明授权

US6022385A Process for the manufacture of sodium carbonate crystals from minerals or solutions 失效
标题翻译：从矿物或溶液制造碳酸钠晶体的方法
公开(公告)号：US6022385A
公开(公告)日：2000-02-08
申请号：US639611
申请日：1996-04-29
申请人： Ronald W. Bowman
发明人： Ronald W. Bowman
IPC分类号： B01D9/00 , C01D7/12 , C01D7/24 , C01D7/28 , C01D7/40 , C22B26/10 , C01D1/30 , C01D7/14 , B01D9/02
CPC分类号： B01D9/005 , C01D7/126 , C01D7/24 , C01D7/28 , C01D7/40 , C22B26/10
摘要： A method of producing sodium carbonate crystals from a sodium carbonate-containing solution including the steps of passing the sodium carbonate-containing solution to a precipitator, adding methanol to the sodium carbonate-containing solution in the precipitator such that a resultant liquor has methanol in a concentration of between 15% and 70% by volume, precipitating the sodium carbonate crystals from the resultant liquor, washing the precipitated sodium carbonate crystals with an alcohol-containing solution and drying the washed precipitated sodium carbonate crystals. The sodium carbonate-containing solution has a sodium carbonate concentration ranging between 100 g/l to saturation. The methanol is in residence with the sodium carbonate-containing solution for between 10 and 100 minutes. The alcohol-containing solution has an alcohol concentration ranging between 50% and 100%.
摘要翻译：一种从含碳酸钠的溶液中制备碳酸钠晶体的方法，包括以下步骤：将含碳酸钠的溶液通入沉淀器中，向沉淀器中的含碳酸钠的溶液中加入甲醇，使得所得液体中含有甲醇浓度为15体积％至70体积％，从所得液体中沉淀碳酸钠晶体，用含醇溶液洗涤沉淀的碳酸钠晶体，并干燥洗涤的沉淀碳酸钠晶体。含碳酸钠的溶液的碳酸钠浓度范围为100g / l至饱和。甲醇与含碳酸钠的溶液停留10至100分钟。含醇溶液的醇浓度在50％至100％之间。

3. 发明授权

US3498744A Purification of calcined crude trona by monohydrate recrystallization 失效
标题翻译：通过单晶重结晶纯化计算的原油
公开(公告)号：US3498744A
公开(公告)日：1970-03-03
申请号：US3498744D
申请日：1961-09-18
申请人： INTERMOUNTAIN RES & DEV CORP
发明人： FRINT WILLIAM R , WAGGENER RICHARD W
IPC分类号： C01D7/12 , C01D7/28 , C01D7/00 , C01D11/00
CPC分类号： C01D7/28 , C01D7/126

4. 发明申请

US20180044193A1 Process to Recycle and Reuse Trona and Coal Combustion Byproducts in a Coal-Fired Power Plant 审中-公开
公开(公告)号：US20180044193A1
公开(公告)日：2018-02-15
申请号：US15231860
申请日：2016-08-09
申请人： Robert L. Smith
发明人： Robert L. Smith
IPC分类号： C01D7/16 , B03B1/04 , B01J20/34 , C01D7/26 , C09K3/18 , B01J20/04 , B03D1/02 , C01D7/28
CPC分类号： C01D7/16 , B01J20/043 , B01J20/3433 , B01J20/3475 , B03B1/04 , B03B9/04 , B03D1/02 , B03D2203/04 , B03D2203/08 , C01D3/04 , C01D7/18 , C01D7/26 , C01D7/28 , C01F11/18 , C01F11/46 , C01F11/48 , C04B18/08 , Y02W30/92 , C04B20/023
摘要： A process is developed wherein sodium carbonate is reclaimed from Trona-treated fly ash waste stream, and the fly ash rendered suitable for use as a Pozzolan. The process is a closed system wherein all separated aspects of the waste stream are reused by the generating power plant or offered as a commercial product.

5. 发明授权

US3246962A Dissolving lump trona in a descending aqueous film 失效
标题翻译：在下降的水性膜中溶解块状天然碱
公开(公告)号：US3246962A
公开(公告)日：1966-04-19
申请号：US26352563
申请日：1963-03-07
申请人： INTERMOUNTAIN RES & DEV CORP
发明人： STANDISH MILLER WARREN
IPC分类号： C01D7/12 , C01D7/28
CPC分类号： C01D7/12 , C01D7/28

6. 发明公开

EP2566815A1 IMPURITIES REMOVAL FROM WASTE SOLIDS IN THE PRODUCTION OF SODA ASH, SODIUM BICARBONATE AND/OR OTHER DERIVATIVES 有权
标题翻译：固体废物杂质处置钠，碳酸氢钠和/或其他衍生产品生产
公开(公告)号：EP2566815A1
公开(公告)日：2013-03-13
申请号：EP11725613.1
申请日：2011-05-03
申请人： Solvay Chemicals, Inc.
发明人： HUGHES, Ronald, O. , MOTE, Jessica A. , VANDENDOREN, Alain , PHILLIP, James D. , SMITH, David W.
IPC分类号： C01D5/16 , C01D7/22 , C01D7/24 , C01D7/28
CPC分类号： C01D5/16 , C01D7/10 , C01D7/12 , C01D7/22 , C01D7/24 , C01D7/28
摘要： A method for removing impurities from a waste solid to provide at least a portion of a suitable crystallizer feed to a process for making crystalline sodium carbonate, bicarbonate, and/or other derivatives. The method comprises: contacting the waste solid with a leach solution to dissolve at least one impurity and dissolving the resulting leached residue. Leaching may include heap percolation. The leach solution may comprise a crystallizer purge liquor, a process waste effluent, a mine water, or mixtures thereof. The method may further comprise adding a magnesium compound to the resulting leached residue during or after its dissolution to remove another impurity. The waste solid preferably comprises a pond solid containing such impurities. The pond solid may be recovered from a pond receiving crystallizer purge liquor(s) and/or other process waste effluent(s). The pond solid may contain sodium carbonate, any hydrate thereof, sodium bicarbonate, and/or sodium sesquicarbonate. The impurities to be removed may comprise sodium chloride, sodium sulfate, silicates, and/or organics.

7. 发明申请

WO1997041271A1 CRYSTALLIZATION OF SODIUM CARBONATES USING ALCOHOLS 审中-公开
标题翻译：使用醇的碳酸钙的结晶
公开(公告)号：WO1997041271A1
公开(公告)日：1997-11-06
申请号：PCT/US1997006429
申请日：1997-04-17
申请人： BOWMAN, Ronald, W.
发明人： BOWMAN, Ronald, W.
IPC分类号： C22B26/10
CPC分类号： B01D9/005 , B01D9/0059 , C01D7/126 , C01D7/24 , C01D7/28 , C01D7/40 , C22B26/10
摘要： A method of producing sodium carbonate crystals (34) from a sodium carbonate-containing solution (14) including the steps of passing the sodium carbonate solution (14) to a precipitator (12), adding methanol (16) to the sodium carbonate solution (14) in the precipitator (12) such that a resultant liquor has methanol in a concentration of between 15 % and 70 % by volume, precipitating the sodium carbonate from the resultant liquor (18), washing (20) the precipitated sodium carbonate crystals with an alcohol-containing solution (22) and drying the washed precipitated sodium carbonate crystals. The sodium carbonate-containing solution (14) has a sodium carbonate concentration ranging from 100g/l to saturation. The methanol is in residence with the sodium carbonate containing solution for between 10 and 100 minutes. The alcohol-containing solution (16) has an alcohol concentration ranging between 50 % and 100 %.
摘要翻译：一种从含碳酸钠溶液（14）制备碳酸钠晶体（34）的方法，包括将碳酸钠溶液（14）通入沉淀器（12）的步骤，将甲醇（16）加入到碳酸钠溶液 14），使得所得液体具有浓度为15体积％至70体积％的甲醇，从所得液体（18）中沉淀碳酸钠，用沉淀的碳酸钠晶体洗涤（20）沉淀的碳酸钠晶体，含醇溶液（22）并干燥洗涤过的沉淀碳酸钠晶体。含碳酸钠的溶液（14）的碳酸钠浓度为100g / l至饱和。甲醇与含碳酸钠的溶液停留10至100分钟。含醇溶液（16）的醇浓度为50％至100％。

8. 发明申请

WO1995032040A1 PROCESS FOR THE MANUFACTURE OF SODIUM CARBONATE, SODIUM BICARBONATE AND/OR SESQUICARBONATE 审中-公开
标题翻译：碳酸钙，二硼酸钠和/或硫代碳酸钠的制备方法
公开(公告)号：WO1995032040A1
公开(公告)日：1995-11-30
申请号：PCT/US1995006533
申请日：1995-05-16
申请人： BOWMAN, Ronald, W.
IPC分类号： B01D09/02
CPC分类号： C22B26/10 , B01D9/005 , B01D9/0059 , C01D7/126 , C01D7/24 , C01D7/28 , C01D7/40 , Y02P10/234
摘要： A method of producing sodium carbonate from trona including the steps of passing a solution containing trona (14) to a precipitator (17), adding alcohol (16) to the solution in the precipitator so as to precipitate carbonate from the solution, washing (20) the precipitated carbonate with an alcohol-containing solution (22) and drying the washed precipitated carbonate. The solution containing trona has a concentration of trona ranging between 50 grams per litre to saturation at 200 DEG F at one atmosphere. The alcohol is methanol which is added at a concentration ranging from 10 to 90 volume percent. The alcohol is vacuum filtered from the precipitated carbonate prior to the step of washing. The precipitated carbonate is washed with methanol in a concentration of between 50 and 100 volume percent. The washed precipitated carbonate is dried by heating to a temperature of no less than 120 DEG F. The alcohol in this process is recycled through a distillation system (30, 38).
摘要翻译：一种从天然碱生产碳酸钠的方法，包括将含有天竺葵（14）的溶液通入沉淀器（17）的步骤，向沉淀器中的溶液中加入酒精（16），以从溶液中沉淀出碳酸盐，洗涤（20 ）沉淀的碳酸酯与含醇溶液（22），并干燥洗涤过的沉淀碳酸盐。含有天然碱的溶液的浓度范围在50克/升至200°F在一个大气压下饱和。醇是以10至90体积％的浓度加入的甲醇。在洗涤步骤之前，将醇从沉淀的碳酸盐中真空过滤。沉淀的碳酸盐用浓度为50-100体积％的甲醇洗涤。经洗涤的沉淀碳酸盐通过加热至不低于120°F的温度来干燥。该方法中的醇通过蒸馏系统再循环（30,38）。

9. 发明授权

US08771622B2 Impurities removal from waste solids in the production of soda ash, sodium bicarbonate and/or other derivatives 有权
标题翻译：在苏打灰，碳酸氢钠和/或其他衍生物的生产中从废物固体中除去杂质
公开(公告)号：US08771622B2
公开(公告)日：2014-07-08
申请号：US13099501
申请日：2011-05-03
申请人： Ronald O. Hughes , Jessica A. Mote , Alain Vandendoren , James D. Phillip , David W. Smith
发明人： Ronald O. Hughes , Jessica A. Mote , Alain Vandendoren , James D. Phillip , David W. Smith
IPC分类号： C01D1/32 , C01D3/16
CPC分类号： C01D5/16 , C01D7/10 , C01D7/12 , C01D7/22 , C01D7/24 , C01D7/28
摘要： A method for removing impurities from a waste solid to provide at least a portion of a suitable crystallizer feed to a process for making crystalline sodium carbonate, bicarbonate, and/or other derivatives. The method comprises: contacting the waste solid with a leach solution to dissolve at least one impurity and dissolving the resulting leached residue. Leaching may include heap percolation. The leach solution may comprise a crystallizer purge liquor, a process waste effluent, a mine water, or mixtures thereof. The method may further comprise adding a magnesium compound to the resulting leached residue during or after its dissolution to remove another impurity. The waste solid preferably comprises a pond solid containing such impurities. The pond solid may be recovered from a pond receiving crystallizer purge liquor(s) and/or other process waste effluent(s). The pond solid may contain sodium carbonate, any hydrate thereof, sodium bicarbonate, and/or sodium sesquicarbonate. The impurities to be removed may comprise sodium chloride, sodium sulfate, silicates, and/or organics.
摘要翻译：从废弃固体中除去杂质的方法，以提供至少一部分合适的结晶器进料，以制备结晶碳酸钠，碳酸氢盐和/或其它衍生物的方法。该方法包括：使废弃物与浸出溶液接触以溶解至少一种杂质并溶解所产生的浸出残渣。浸出可能包括堆渗。浸出溶液可以包括结晶器清洗液，工艺废物流出物，矿井水或其混合物。该方法可以进一步包括在其溶解期间或之后向所产生的浸出残渣中加入镁化合物以除去另一种杂质。废固体优选包含含有这种杂质的池塘固体。池塘固体可以从接收结晶器清洗液和/或其它工艺废物流出物的池中回收。池塘固体可以含有碳酸钠，其任何水合物，碳酸氢钠和/或倍半碳酸钠。待除去的杂质可包括氯化钠，硫酸钠，硅酸盐和/或有机物。

10. 发明申请

US20110274599A1 Impurities removal from waste solids in the production of soda ash, sodium bicarbonate and/or other derivatives 有权
标题翻译：在苏打灰，碳酸氢钠和/或其他衍生物的生产中从废物固体中除去杂质
公开(公告)号：US20110274599A1
公开(公告)日：2011-11-10
申请号：US13099501
申请日：2011-05-03
申请人： Ronald O. HUGHES , Jessica A. MOTE , Alain VANDENDOREN , James D. PHILLIP , David W. SMITH
发明人： Ronald O. HUGHES , Jessica A. MOTE , Alain VANDENDOREN , James D. PHILLIP , David W. SMITH
IPC分类号： C01D7/00 , C01D7/24 , C01D5/14
CPC分类号： C01D5/16 , C01D7/10 , C01D7/12 , C01D7/22 , C01D7/24 , C01D7/28
摘要： A method for removing impurities from a waste solid to provide at least a portion of a suitable crystallizer feed to a process for making crystalline sodium carbonate, bicarbonate, and/or other derivatives. The method comprises: contacting the waste solid with a leach solution to dissolve at least one impurity and dissolving the resulting leached residue. Leaching may include heap percolation. The leach solution may comprise a crystallizer purge liquor, a process waste effluent, a mine water, or mixtures thereof. The method may further comprise adding a magnesium compound to the resulting leached residue during or after its dissolution to remove another impurity. The waste solid preferably comprises a pond solid containing such impurities. The pond solid may be recovered from a pond receiving crystallizer purge liquor(s) and/or other process waste effluent(s). The pond solid may contain sodium carbonate, any hydrate thereof, sodium bicarbonate, and/or sodium sesquicarbonate. The impurities to be removed may comprise sodium chloride, sodium sulfate, silicates, and/or organics.
摘要翻译：从废弃固体中除去杂质的方法，以提供至少一部分合适的结晶器进料，以制备结晶碳酸钠，碳酸氢盐和/或其它衍生物的方法。该方法包括：使废弃物与浸出溶液接触以溶解至少一种杂质并溶解所产生的浸出残渣。浸出可能包括堆渗。浸出溶液可以包括结晶器清洗液，工艺废物流出物，矿井水或其混合物。该方法可以进一步包括在其溶解期间或之后向所产生的浸出残渣中加入镁化合物以除去另一种杂质。废固体优选包含含有这种杂质的池塘固体。池塘固体可以从接收结晶器清洗液和/或其它工艺废物流出物的池中回收。池塘固体可以含有碳酸钠，其任何水合物，碳酸氢钠和/或倍半碳酸钠。待除去的杂质可包括氯化钠，硫酸钠，硅酸盐和/或有机物。

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