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1. 发明公开

CN104246061A 喷墨印花用着色组合物、印花方法以及织物无效
公开(公告)号：CN104246061A
公开(公告)日：2014-12-24
申请号：CN201380021442.8
申请日：2013-03-28
申请人：富士胶片株式会社
发明人：八木一成 , 石绵靖宏 , 法月祐太朗
IPC分类号： D06P1/18 , D06P3/24 , D06P5/30 , B41J2/01 , B41M5/00 , C09B29/46 , C09B67/44
CPC分类号： D06P3/24 , B41J2/01 , B41M5/00 , C09B29/0051 , C09B29/0801 , C09B29/0809 , C09B43/11 , C09D11/00 , C09D11/328 , D06P1/08 , D06P1/18 , D06P3/26 , D06P5/30 , Y10T428/2481
摘要：一种喷墨印花用着色组合物，其含有式(I)所表示的染料以及水[R1为H、卤素、烷基、芳烷基、芳基、杂芳基、烷氧基、或者氰基；R2为H、卤素、氰基、-COOR6、-COR7、-CONR8R9、或者离子性亲水性基；R3为烷基、芳烷基、烯基、炔基、芳基、或者杂芳基；R4及R5分别独立地为H、烷基、环烷基、芳烷基、烯基、炔基、芳基、或者杂芳基；R15为H或者取代基；X为烷基、环烷基、芳烷基、芳基、杂芳基、-COR12、或者-CONR13R14；R6为烷基、芳基、或者杂芳基；R7～R14分别独立地为H、烷基、芳基、或者杂芳基；一分子中的离子性亲水性基数为1～5]。

2. 发明申请

US20190211186A1 DYE, FILLER MADE THEREFROM, COMPOSITIONS INCLUDING THE FILLER, AND METHOD OF DETERMINING DEGREE OF CURE OF SUCH COMPOSITIONS 审中-公开
公开(公告)号：US20190211186A1
公开(公告)日：2019-07-11
申请号：US16356942
申请日：2019-03-18
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： Mark F. Schulz , Michael S. Wendland
IPC分类号： C08K5/47 , C09B29/08 , G01N21/78 , C09B29/033 , C08K9/04 , C08K7/20 , C09C3/08 , C09C1/00 , C09C1/28 , C09C1/02 , C09B69/00
CPC分类号： C08K5/47 , C08K7/20 , C08K9/04 , C09B29/0088 , C09B29/0801 , C09B29/0813 , C09B29/0827 , C09B29/0829 , C09B69/008 , C09C1/00 , C09C1/021 , C09C1/28 , C09C3/08 , G01N21/78
摘要： A compound represented by formula: and a treated filler having the compound on at least a portion of its surface. R is hydrogen or alkyl. X is alkylene, arylalkylene, or alkylarylene, each optionally interrupted by at least one of an ether, thioether, amine, amide, ester, thioester, carbonate, thiocarbonate, carbamate, thiocarbamate, urea, or thiourea, with alkylene optionally interrupted by arylene. W is hydroxyl, a sulfonic acid group, a phosphonic acid group, carboxylic acid group, —NHR1, epoxy, or —Si(Y)x(Z)3-x. Y is alkyl, aryl, arylalkylenyl, or alkylarylenyl. Z is halide, hydroxyl, alkoxy, aryloxy, acyloxy, polyalkyleneoxy, —O— covalently bonded to the surface of the filler, or —O bonded to another silicon atom, and x is 0 or 1. A composition including the treated filler, a method of making the treated filler, and a method of determining the degree of cure of a curable polymeric resin are also disclosed.

3. 发明授权

US09068290B2 Coloring composition for inkjet textile printing, textile printing method, and fabric 有权
标题翻译：喷墨纺织印花着色组合物，纺织印花法和织物
公开(公告)号：US09068290B2
公开(公告)日：2015-06-30
申请号：US14517926
申请日：2014-10-20
申请人： FUJIFILM CORPORATION
发明人： Kazunari Yagi , Yasuhiro Ishiwata , Yutaro Norizuki
IPC分类号： D06P3/24 , B41J2/01 , B41M5/00 , C09D11/00 , C09D11/328 , D06P1/08 , D06P5/30 , D06P3/26 , C09B29/036 , C09B29/08 , C09B43/11 , D06P1/18
CPC分类号： D06P3/24 , B41J2/01 , B41M5/00 , C09B29/0051 , C09B29/0801 , C09B29/0809 , C09B43/11 , C09D11/00 , C09D11/328 , D06P1/08 , D06P1/18 , D06P3/26 , D06P5/30 , Y10T428/2481
摘要： A coloring composition for inkjet textile printing, containing water and a dye represented by Formula (I) [R1 represents H, halogen, alkyl, aralkyl, aryl, heteroaryl, alkoxy, or cyano; R2 represents H, halogen, cyano, —COOR6, —COR7, —CONR8R9, or an ionic hydrophilic group; R3 represents alkyl, aralkyl, alkenyl, alkynyl, aryl, or heteroaryl; each of R4 and R5 independently represents H, alkyl, cycloalkyl, aralkyl, alkenyl, alkynyl, aryl, or heteroaryl; R15 represents H or a substituent; X represents alkyl, cycloalkyl, aralkyl, aryl, heteroaryl, —COR12, or —CONR13R14; R6 represents alkyl, aryl, or heteroaryl; each of R7 to R14 independently represents H, alkyl, aryl, or heteroaryl; and a number of ionic hydrophilic groups in one molecule is from 1 to 5].
摘要翻译：用于喷墨织物印花的着色组合物，含有水和由式（I）表示的染料[R1表示H，卤素，烷基，芳烷基，芳基，杂芳基，烷氧基或氰基; R 2表示H，卤素，氰基，-COOR 6，-COR 7，-CONR 8 R 9或离子性亲水基团; R 3表示烷基，芳烷基，烯基，炔基，芳基或杂芳基; R 4和R 5各自独立地表示H，烷基，环烷基，芳烷基，烯基，炔基，芳基或杂芳基; R 15表示H或取代基; X表示烷基，环烷基，芳烷基，芳基，杂芳基，-COR 12或-CONR 13 R 14; R6表示烷基，芳基或杂芳基; R 7至R 14各自独立地表示H，烷基，芳基或杂芳基; 并且一个分子中的多个离子亲水基团为1〜5]。

4. 发明授权

US06489452B1 Azo dyes, process for making the same, ink-jet printing ink, ink-jet recording method 有权
标题翻译：偶氮染料，制造方法，喷墨印刷油墨，喷墨记录方法
公开(公告)号：US06489452B1
公开(公告)日：2002-12-03
申请号：US09813036
申请日：2001-03-21
申请人： Keiichi Tateishi , Toshiki Fujiwara , Makoto Yamada
发明人： Keiichi Tateishi , Toshiki Fujiwara , Makoto Yamada
IPC分类号： C09B29036
CPC分类号： C09D11/328 , C09B29/0051 , C09B29/0801 , C09B29/0809 , C09B43/11 , C09B43/16
摘要： An azo dye represented by the following general formula (1) and a process for making the azo dye is disclosed. The process comprises a step in which a diazonium salt is formed by the reaction between an aminopyrazole represented by the general formula (3) and an diazotizing agent, a step in which a compound represented by the general formula (5) is formed by the reaction between the diazonium salt and an aromatic coupling agent represented by the general formula (4), and a step in which an azo dye represented by the general formula (6) is formed by the reaction between the compound represented by the general formula (5) and an arylating agent or a heterylating agent in the presence of a base.
摘要翻译：公开了由以下通式（1）表示的偶氮染料和制备偶氮染料的方法。该方法包括通过由通式（3）表示的氨基吡唑与重氮化剂之间的反应形成重氮盐的步骤，其中通过反应形成由通式（5）表示的化合物的步骤在由通式（4）表示的重氮盐和芳族偶联剂之间，通过通式（5）表示的化合物之间的反应形成由通式（6）表示的偶氮染料，和芳基化剂或异构化剂在碱的存在下反应。

5. 发明申请

US20150037546A1 COLORING COMPOSITION FOR INKJET TEXTILE PRINTING, TEXTILE PRINTING METHOD, AND FABRIC 有权
标题翻译：印花纺织印花的印花组合物，纺织印花方法和织物
公开(公告)号：US20150037546A1
公开(公告)日：2015-02-05
申请号：US14517926
申请日：2014-10-20
申请人： FUJIFILM CORPORATION
发明人： Kazunari YAGI , Yasuhiro ISHIWATA , Yutaro NORIZUKI
IPC分类号： D06P3/24 , D06P5/30 , D06P1/08
CPC分类号： D06P3/24 , B41J2/01 , B41M5/00 , C09B29/0051 , C09B29/0801 , C09B29/0809 , C09B43/11 , C09D11/00 , C09D11/328 , D06P1/08 , D06P1/18 , D06P3/26 , D06P5/30 , Y10T428/2481
摘要： A coloring composition for inkjet textile printing, containing water and a dye represented by Formula (I) [R1 represents H, halogen, alkyl, aralkyl, aryl, heteroaryl, alkoxy, or cyano; R2 represents H, halogen, cyano, —COOR6, —COR7, —CONR8R9, or an ionic hydrophilic group; R3 represents alkyl, aralkyl, alkenyl, alkynyl, aryl, or heteroaryl; each of R4 and R5 independently represents H, alkyl, cycloalkyl, aralkyl, alkenyl, alkynyl, aryl, or heteroaryl; R15 represents H or a substituent; X represents alkyl, cycloalkyl, aralkyl, aryl, heteroaryl, —COR12, or —CONR13R14; R6 represents alkyl, aryl, or heteroaryl; each of R7 to R14 independently represents H, alkyl, aryl, or heteroaryl; and a number of ionic hydrophilic groups in one molecule is from 1 to 5].
摘要翻译：用于喷墨织物印花的着色组合物，含有水和由式（I）表示的染料[R1表示H，卤素，烷基，芳烷基，芳基，杂芳基，烷氧基或氰基; R 2表示H，卤素，氰基，-COOR 6，-COR 7，-CONR 8 R 9或离子性亲水基团; R 3表示烷基，芳烷基，烯基，炔基，芳基或杂芳基; R 4和R 5各自独立地表示H，烷基，环烷基，芳烷基，烯基，炔基，芳基或杂芳基; R 15表示H或取代基; X表示烷基，环烷基，芳烷基，芳基，杂芳基，-COR 12或-CONR 13 R 14; R6表示烷基，芳基或杂芳基; R 7至R 14各自独立地表示H，烷基，芳基或杂芳基; 并且一个分子中的多个离子亲水基团为1〜5]。

6. 发明授权

US4243584A Monoazo dyestuffs containing diazo component substituted by disulfimide and trifluoromethyl groups 失效
标题翻译：含有被二硫代酰亚胺和三氟甲基取代的重氮组分的单偶氮染料
公开(公告)号：US4243584A
公开(公告)日：1981-01-06
申请号：US919482
申请日：1978-06-27
申请人： Richard Sommer , Gerhard Wolfrum , Gerhard Buttner
发明人： Richard Sommer , Gerhard Wolfrum , Gerhard Buttner
IPC分类号： C09B29/01 , C09B29/08 , C09B29/36 , C09B29/38 , D06P3/26
CPC分类号： C09B29/0801 , C09B29/08 , C09B29/36
摘要： Monoazo dyestuffs of the formula ##STR1## wherein R.sub.1 represents an aromatic radical, an aliphatic radical with 1-4 C atoms or a dialkylamino radical, in which the alkyl groups contain 1-C atoms, R.sub.2 represents hydrogen, halogen, alkyl with 1-C atoms, alkoxy with 1-4 C atoms or trifluoromethyl, R.sub.3 represents hydrogen, halogen, alkyl with 1-4 C atoms, alkoxy with 1-4 C atoms or trifluoromethyl and K represents the radical of a coupling component K-H of the formulae (II), (III) and (IV) ##STR2## wherein R.sub.4 represents alkyl with 1-4 C atoms or aryl,R.sub.5 represents hydrogen or unsubstituted alkyl with 1-4 C atoms,R.sub.6 represents hydrogen, nitrile, halogen, alkyl with 1-4 C atoms or alkoxy with 1-4 C atoms,R.sub.7 represents hydrogen, alkyl with 1-4 C atoms, aryl, a carboxylic acid ester group or a carboxylic acid amide group,R.sub.8 represents hydrogen, alkyl, cycloalkyl, aryl or the radical of a heterocyclic compound,R.sub.9 represents hydrogen, halogen, alkyl with 1-4 C atoms, alkoxy with 1-4 C atoms or acylamino,R.sub.10 represents hydrogen, halogen, alkyl with 1-4 C atoms, alkoxy with 1-4 C atoms or aryloxy,R.sub.11 represents hydrogen or alkyl,R.sub.12 represents hydrogen or alkyl and m represents 0 or 1,are suitable for the dyeing of synthetic fibre materials, especially those from polyamides. Level yellow, red and ruby shades are obtained with good dyeing yield and fastness.
摘要翻译：其中R 1表示芳族基团，具有1-4个碳原子的脂族基团或二烷基氨基，其中烷基含有1-C原子，R 2表示氢，卤素，具有1- C原子，具有1-4个C原子的烷氧基或三氟甲基，R 3表示氢，卤素，具有1-4个C原子的烷基，具有1-4个C原子的烷氧基或三氟甲基，K表示式（I）的偶合组分KH的基团 II），（III）和（IV）其中R 4表示具有1-4个C原子的烷基或芳基，R 5表示氢或具有1-4个C原子的未取代的烷基，R 6表示氢，腈，卤素，具有1个 -4个C原子或具有1-4个C原子的烷氧基，R7代表氢，具有1-4个C原子的烷基，芳基，羧酸酯基或羧酸酰胺基，R8代表氢，烷基，环烷基，芳基或杂环化合物的基团，R 9表示氢，卤素，具有1-4个C原子的烷基，具有1-4个C原子的烷氧基或a 氨基，R 10表示氢，卤素，具有1-4个C原子的烷基，具有1-4个C原子的烷氧基或芳氧基，R 11表示氢或烷基，R 12表示氢或烷基，m表示0或1，适于染色合成纤维材料，特别是聚酰胺。获得具有良好的染色产率和坚牢度的黄色，红色和红宝石色调。

7. 发明公开

EP3362518A1 SENSOR DYES FOR REAL-TIME SENSING OF METAL IONS IN AQUEOUS ENVIRONMENTS 审中-公开
公开(公告)号：EP3362518A1
公开(公告)日：2018-08-22
申请号：EP16856342.7
申请日：2016-10-14
申请人： The UWM Research Foundation, Inc , Fenski, Tyler G. , Aquametals, LLC
发明人： FENSKE, Tyler, G. , BATHURST, Bruce , SCHWABACHER, Alan , GEISSINGER, Peter , HAGEMANN, Trevor , OEHM, Sarah , HENNING, Paul
IPC分类号： C09B29/036 , C09B29/033 , C09B29/36 , G01N21/78 , G01N31/22 , G01N33/18
CPC分类号： G01N21/78 , C09B29/0003 , C09B29/0014 , C09B29/0801 , C09B29/0811 , C09B29/3621 , C09B29/3665 , C09B29/3673 , C09B33/06 , C09B56/00 , G01N31/22 , G01N33/1813
摘要： Provided herein are dyes for detecting and distinguishing metals in a sample, as well as compositions and methods comprising the same.

8. 发明公开

EP3090025A4 DYE, FILLER MADE THEREFROM, COMPOSITIONS INCLUDING THE FILLER, AND METHOD OF DETERMINING DEGREE OF CURE OF SUCH COMPOSITIONS 审中-公开
标题翻译： FARBSTOFF，FÜLLSTOFFDARAUS，ZUSAMMENSETZUNGEN MIT DWMFÜLLSTOFFUND VERFAHREN ZUR BESTIMMUNG DESHÄTUNGSGRADESDIESER ZUSAMMENSETZUNGEN
公开(公告)号：EP3090025A4
公开(公告)日：2017-08-23
申请号：EP14876676
申请日：2014-12-19
申请人： 3M INNOVATIVE PROPERTIES CO
发明人： SCHULZ MARK F , WENDLAND MICHAEL S
IPC分类号： C09C3/08 , C09B29/045 , C09B29/08
CPC分类号： C08K5/47 , C08K7/20 , C08K9/04 , C09B29/0088 , C09B29/0801 , C09B29/0813 , C09B29/0827 , C09B29/0829 , C09B69/008 , C09C1/00 , C09C1/021 , C09C1/28 , C09C3/08 , G01N21/78
摘要： A compound represented by formula (I): and a treated filler having the compound on at least a portion of its surface. R is hydrogen or alkyl. X is alkylene, arylalkylene, or alkylarylene, each optionally interrupted by at least one of an ether, thioether, amine, amide, ester, thioester, carbonate, thiocarbonate, carbamate, thiocarbamate, urea, or thiourea, with alkylene optionally interrupted by arylene. W is hydroxyl, a sulfonic acid group, a phosphonic acid group, carboxylic acid group, -NHR1, epoxy, or -Si(Y)x(Z)3-x. Y is alkyl, aryl, arylalkylenyl, or alkylarylenyl. Z is halide, hydroxyl, alkoxy, aryloxy, acyloxy, polyalkyleneoxy, -O- covalently bonded to the surface of the filler, or -O bonded to another silicon atom, and x is 0 or 1. A composition including the treated filler, a method of making the treated filler, and a method of determining the degree of cure of a curable polymeric resin are also disclosed.
摘要翻译：由式（I）表示的化合物和在其表面的至少一部分上具有化合物的经处理的填充剂。 R是氢或烷基。 X是亚烷基，芳基亚烷基或烷基亚芳基，其各自任选被醚，硫醚，胺，酰胺，酯，硫酯，碳酸酯，硫代碳酸酯，氨基甲酸酯，硫代氨基甲酸酯，脲或硫脲中的至少一种与亚烷基任选间隔亚芳基插入。 W为羟基，磺酸基，膦酸基，羧酸基，-NHR1，环氧基或-Si（Y）x（Z）3-x。 Y是烷基，芳基，芳基亚烷基或烷基亚芳基。 Z为与填料表面共价键合的-O-，羟基，烷氧基，芳氧基，酰氧基，聚亚烷氧基，-O-或与另一个硅原子键合的-O，x为0或1.包含处理过的填料，制造经处理的填料的方法，以及确定可固化聚合物树脂的固化程度的方法也被公开。

9. 发明申请

US20030040608A1 Azo dyes, process for making the same, ink-jet printing ink, ink-jet recording method 有权
标题翻译：偶氮染料，制造方法，喷墨印刷油墨，喷墨记录方法
公开(公告)号：US20030040608A1
公开(公告)日：2003-02-27
申请号：US10176764
申请日：2002-06-24
发明人： Keiichi Tateishi , Toshiki Fujiwara , Makoto Yamada
IPC分类号： C09B031/047
CPC分类号： C09D11/328 , C09B29/0051 , C09B29/0801 , C09B29/0809 , C09B43/11 , C09B43/16
摘要： An azo dye represented by the following general formulae (10) and (12): 1 (wherein the variables are as defined herein) and a process for making the azo dye is disclosed. The process comprises a step in which a diazonium salt is formed by the reaction between an aminopyrazole represented by the general formula (3) and an diazotizing agent, a step in which a compound represented by the general formula (5) is formed by the reaction between the diazonium salt and an aromatic coupling agent represented by the general formula (4), and a step in which an azo dye represented by the general formula (6) is formed by the reaction between the compound represented by the general formula (5) and an arylating agent or a heterylating agent in the presence of a base.
摘要翻译：由以下通式（10）和（12）表示的偶氮染料（其中变量如本文所定义）和制备偶氮染料的方法。该方法包括通过由通式（3）表示的氨基吡唑与重氮化剂之间的反应形成重氮盐的步骤，其中通过反应形成由通式（5）表示的化合物的步骤在由通式（4）表示的重氮盐和芳族偶联剂之间，通过通式（5）表示的化合物之间的反应形成由通式（6）表示的偶氮染料，和芳基化剂或异构化剂在碱的存在下反应。

10. 发明授权

US4234483A N-(3-Chloro-4-[2,6-dichloro-4-nitrophenyl)azo]-2-methyl phenyl)-.beta.-alanine, methyl ester 失效
标题翻译： N-（3-氯-4- [2,6-二氯-4-硝基苯基）偶氮] -2-甲基苯基）-β-丙氨酸甲酯
公开(公告)号：US4234483A
公开(公告)日：1980-11-18
申请号：US713619
申请日：1976-08-11
申请人： Raouf Botros , Ivan E. Riggle
发明人： Raouf Botros , Ivan E. Riggle
IPC分类号： C09B29/08 , D06P3/04 , D06P3/24 , D06P3/52
CPC分类号： C09B29/0847 , C09B29/0801
摘要： Azo compounds of the formula: ##STR1## are provided where A is a diazotizable aromatic hydrocarbon and X is hydrogen or lower alkyl. The compounds dye synthetic fibers, particularly nylon and polyester, and wool in strong yellow to red hues of outstanding brightness and build-up. The dyeings have excellent fastness properties.
摘要翻译：提供下式的偶氮化合物：其中A是可重氮化的芳族烃，X是氢或低级烷基。化合物染色合成纤维，特别是尼龙和聚酯，以及具有强烈的黄色至红色色调的羊毛，具有出色的亮度和积聚性。染色具有优异的牢度特性。

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