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1. 发明授权

US06331282B1 Manganese oxyiodides and their method of preparation and use in energy storage 失效
标题翻译：锰氧碘化物及其在能量储存中的制备和使用方法
公开(公告)号：US06331282B1
公开(公告)日：2001-12-18
申请号：US09189446
申请日：1998-11-10
申请人： Arumugam Manthiram , Jaekook Kim
发明人： Arumugam Manthiram , Jaekook Kim
IPC分类号： C01G4512
CPC分类号： C01G45/1221 , C01P2002/52 , C01P2002/72 , C01P2006/40 , C01P2006/80
摘要： A method for synthesizing a manganese oxyiodide, including the steps of reducing sodium permanganate by lithium iodide at ambient temperature to obtain the manganese oxyiodide, and annealing the manganese oxyiodide at an elevated temperature. Such a manganese oxyiodide may be used for energy conversion and storage, particularly for battery and supercapacitor applications.
摘要翻译：一种合成锰氧化锰的方法，包括以下步骤：在环境温度下用碘化锂还原高锰酸钠，得到锰氧化锰，并在升高的温度下退火锰氧化物。这种锰氧碘化物可用于能量转换和储存，特别是用于电池和超级电容器应用。

2. 发明授权

US06183718B2 Method of making stabilized electrochemical cell active material of lithium manganese oxide 有权
标题翻译：制备锂锰氧化物稳定的电化学电池活性材料的方法
公开(公告)号：US06183718B2
公开(公告)日：2001-02-06
申请号：US09307355
申请日：1999-05-07
申请人： Jeremy Barker , M. Yazid Saidi , Chariclea A. Scordilis-Kelley
发明人： Jeremy Barker , M. Yazid Saidi , Chariclea A. Scordilis-Kelley
IPC分类号： C01G4512
CPC分类号： H01M4/131 , C01G45/1221 , C01G45/1242 , C01P2002/32 , C01P2002/77 , C01P2004/51 , C01P2004/60 , C01P2006/40 , H01M4/1391 , H01M4/505 , H01M4/62 , H01M10/0525 , H01M10/0567
摘要： A method for forming the composition stabilized against capacity degradation comprises particles of spinel lithium manganese oxide (LMO) enriched with lithium by a decomposition product of lithium carbonate forming a part of each said particle and characterized by a reduced surface area and increased capacity expressed in milliamp hours per gram as compared to non-enriched spinel.
摘要翻译：形成稳定防止容量降解的组合物的方法包括通过碳酸锂的分解产物富集锂的尖晶石锂锰氧化物（LMO），其形成每个所述颗粒的一部分，其特征在于表面积减小并且以毫安表示的增加的容量小时/克，与非富集尖晶石相比。

3. 发明授权

US06821498B2 Oxygen ion conducting materials 失效
标题翻译：氧离子导电材料
公开(公告)号：US06821498B2
公开(公告)日：2004-11-23
申请号：US10327502
申请日：2002-12-20
申请人： John Vaughey , Michael Krumpelt , Xiaoping Wang , J. David Carter
发明人： John Vaughey , Michael Krumpelt , Xiaoping Wang , J. David Carter
IPC分类号： C01G4512
CPC分类号： H01M4/8621 , B01J23/002 , B01J23/10 , B01J23/34 , B01J2523/00 , C01G45/1264 , C01P2002/34 , C01P2002/52 , C01P2002/54 , C01P2002/77 , C01P2006/40 , H01M4/8652 , H01M4/9016 , B01J2523/24 , B01J2523/32 , B01J2523/3706 , B01J2523/72
摘要： An oxygen ion conducting ceramic oxide that has applications in industry including fuel cells, oxygen pumps, oxygen sensors, and separation membranes. The material is based on the idea that substituting a dopant into the host perovskite lattice of (La,Sr)MnO3 that prefers a coordination number lower than 6 will induce oxygen ion vacancies to form in the lattice. Because the oxygen ion conductivity of (La,Sr)MnO3 is low over a very large temperature range, the material exhibits a high overpotential when used. The inclusion of oxygen vacancies into the lattice by doping the material has been found to maintain the desirable properties of (La,Sr)MnO3, while significantly decreasing the experimentally observed overpotential.
摘要翻译：氧离子传导陶瓷氧化物，在工业中应用，包括燃料电池，氧气泵，氧传感器和分离膜。该材料基于以下思想：将掺杂剂置换为优选配位数低于6的（La，Sr）MnO 3的主体钙钛矿晶格将诱导在晶格中形成氧离子空位。由于（La，Sr）MnO 3的氧离子电导率在非常大的温度范围内较低，所以当使用时材料表现出高的超电势。已经发现通过掺杂材料将氧空位包含在晶格中已被发现保持了（La，Sr）MnO 3的所需性质，同时显着降低了实验观察到的超电势。

4. 发明授权

US06348182B1 Process for producing lithium manganese oxide with spinel structure 失效
标题翻译：尖晶石结构生产锰酸锂的工艺
公开(公告)号：US06348182B1
公开(公告)日：2002-02-19
申请号：US08883272
申请日：1997-06-26
申请人： Qi Lu , Gohei Yoshida , Kazuhiko Hirao , Yukinori Honjo
发明人： Qi Lu , Gohei Yoshida , Kazuhiko Hirao , Yukinori Honjo
IPC分类号： C01G4512
CPC分类号： H01M4/505 , C01G45/1242 , C01P2002/32 , C01P2002/72 , C01P2004/03 , C01P2006/40
摘要： A process for producing a lithium manganese oxide with a spinel structure for use as a cathode material of an organic electrolyte lithium ion secondary battery, which comprises: mixing at least one lithium compound selected from the group consisting of lithium hydroxide and lithium carbonate with manganese dioxide in a solvent consisting essentially of water or an aliphatic lower alcohol having from 1 to 3 carbon atoms or a mixture thereof, optionally in the presence of at least one organic acid selected from the group consisting of formic acid and acetic acid; allowing the resultant mixture to form a gel-like mixture; and drying the gel-like mixture as required; and calcining the resulting product.
摘要翻译：一种用作有机电解质锂离子二次电池的阴极材料的尖晶石结构的锂锰氧化物的制造方法，其特征在于，将至少一种选自氢氧化锂和碳酸锂的锂化合物与二氧化锰在基本上由水或具有1至3个碳原子的脂族低级醇或其混合物组成的溶剂中，任选在至少一种选自甲酸和乙酸的有机酸存在下进行; 使所得混合物形成凝胶状混合物; 并根据需要干燥凝胶状混合物; 并煅烧所得产物。

5. 发明授权

US06296830B1 Layered structure manganese dioxide for cathode material in lithium rechargeable cell and process for producing the same 失效
标题翻译：锂二次电池用阴极材料的分层结构二氧化锰及其制造方法
公开(公告)号：US06296830B1
公开(公告)日：2001-10-02
申请号：US09236325
申请日：1999-01-25
申请人： Seung-Mo Oh , Sa-Heum Kim , Wan Mook Im
发明人： Seung-Mo Oh , Sa-Heum Kim , Wan Mook Im
IPC分类号： C01G4512
CPC分类号： C01G45/02 , C01G45/1221 , C01P2002/20 , C01P2002/54 , C01P2002/72 , C01P2002/76 , C01P2002/78 , C01P2006/40 , H01M4/505
摘要： A layered structure manganese dioxide (MnO2) of which oxide lattices are in the pattern of pseudo-hexagonal close packing ( . . . AABB . . . ) and has hexagonal P63/mmc space group or orthorhombic Cmcm space group. The present invention also provides a process for producing said layered structure manganese dioxide (MnO2) which comprises heat treating a mixture of an alkali metal compound and a manganese compound at a high temperature. During the process, bismuth compounds or lead compounds may be added in order to stabilize the layered crystal structure of MnO2, or lithium compounds may be added in order to improve the reversibility of charge and discharge. The layered structure MnO2 is suitable for use as a cathode material in lithium rechargeable cells, since it does not transform into a spinel phase during charge and discharge cycling, thus having an excellent charging and discharging reversibility.
摘要翻译：氧化物晶格呈伪六方密堆积图案（AABB ...）并具有六边形P63 / mmc空间群或正交Cmcm空间群的层状结构二氧化锰（MnO 2）。本发明还提供了一种制备所述层状结构二氧化锰（MnO 2）的方法，其包括在高温下热处理碱金属化合物和锰化合物的混合物。在此过程中，为了稳定MnO2的层状晶体结构，可以加入铋化合物或铅化合物，也可以添加锂化合物，以提高充放电的可逆性。层状结构MnO 2适合用作锂可再充电电池中的阴极材料，因为它在充电和放电循环期间不会转变为尖晶石相，因此具有优异的充电和放电可逆性。

6. 发明授权

US06607706B1 Composite metal oxide particles 有权
公开(公告)号：US06607706B1
公开(公告)日：2003-08-19
申请号：US09188768
申请日：1998-11-09
申请人： Sujeet Kumar , Hariklia Dris Reitz , Xiangxin Bi
发明人： Sujeet Kumar , Hariklia Dris Reitz , Xiangxin Bi
IPC分类号： C01G4512
CPC分类号： H01M4/525 , B82Y30/00 , C01G45/02 , C01G45/1221 , C01G45/1242 , C01G45/1292 , C01P2002/02 , C01P2002/72 , C01P2002/77 , C01P2004/04 , C01P2004/51 , C01P2004/52 , C01P2004/62 , C01P2004/64 , C01P2004/80 , C01P2006/40 , H01M4/131 , H01M4/485 , H01M4/50
摘要： A powder of lithiated manganese oxide has an average particle diameter preferably less than about 250 nm. The particles have a high degree of uniformity and preferably a very narrow particle size distribution. The lithiated manganese oxide can be produce by the reaction of an aerosol where the aerosol comprises both a first metal (lithium) precursor and a second metal (manganese) precursor. Preferably, the reaction involves laser pyrolysis where the reaction is driven by heat absorbed from an intense laser beam.

7. 发明授权

US06551571B2 Cobalt-coated lithium manganese complex oxide and preparation process thereof 失效
标题翻译：钴包覆的锂锰复合氧化物及其制备方法
公开(公告)号：US06551571B2
公开(公告)日：2003-04-22
申请号：US10166409
申请日：2002-06-11
申请人： Shoichi Fujino , Hiroshi Takahama , Mitsuaki Hatatani , Norimiki Sugiyama , Hideaki Sadamura
发明人： Shoichi Fujino , Hiroshi Takahama , Mitsuaki Hatatani , Norimiki Sugiyama , Hideaki Sadamura
IPC分类号： C01G4512
CPC分类号： H01M4/505 , C01G45/02 , C01P2002/32 , C01P2002/72 , C01P2004/04 , C01P2004/51 , C01P2004/61 , C01P2004/62 , C01P2004/80 , C01P2006/12 , C01P2006/40 , H01M4/0497 , H01M4/1391 , H01M4/50 , H01M4/502 , H01M4/62 , H01M10/4235
摘要： A cobalt-coated lithium manganese complex oxide is disclosed. This provides a particularly high discharge capacity which is useful for the improvement of cycle characteristics of a secondary battery as an active material of a positive electrode for a secondary battery with a nonaqueous electrolyte.
摘要翻译：公开了一种钴包覆的锂锰复合氧化物。这提供了特别高的放电容量，其可用于改善作为用于具有非水电解质的二次电池的正极的活性材料的二次电池的循环特性。

8. 发明授权

US06325988B1 Process for preparing spinel type lithium manganese composite oxide and cathode active material for rechargeable battery 有权
标题翻译：制备可再充电电池的尖晶石型锂锰复合氧化物和阴极活性材料的方法
公开(公告)号：US06325988B1
公开(公告)日：2001-12-04
申请号：US09403548
申请日：1999-10-25
申请人： Hidetoshi Inoue , Kazuhiko Kikuya , Hitoshi Machimura , Yukio Matsubara
发明人： Hidetoshi Inoue , Kazuhiko Kikuya , Hitoshi Machimura , Yukio Matsubara
IPC分类号： C01G4512
摘要： A process for preparing a spinel lithium manganese complex oxide having the general formula LixMn2−yAlyO4 (wherein 0.9≦x≦1.1, and 0.002≦y≦0.5) the process comprising the steps of reacting a manganese complex hydroxide represented by the general formula (IIa) Mn2+(1−a)Al3+a(OH)[2+a−nz](An−)2·mH2O (wherein An− is an anion having a valence n, 0.001≦a≦0.25, 0.03
摘要翻译：一种制备具有通式LixMn2-yAlyO4（其中0.9 <= x <= 1.1，和0.002 <= y <= 0.5）的尖晶石锂锰复合氧化物的方法，该方法包括以下步骤：使由通式（IIa）Mn2 +（1-a）Al3 + a（OH）[2 + a-nz]（An-）2mH2O（其中An-为正数n，0.001 <= a <= 0.25 ，0.03

9. 发明授权

US06207129B1 Lithiated manganese oxide 失效
标题翻译：锂化锰
公开(公告)号：US06207129B1
公开(公告)日：2001-03-27
申请号：US09312033
申请日：1999-05-14
申请人： Akshaya Kumar Padhi , Chithambarathanu Pillai
发明人： Akshaya Kumar Padhi , Chithambarathanu Pillai
IPC分类号： C01G4512
CPC分类号： H01M4/505 , C01G45/1242 , C01P2002/32 , C01P2002/72 , C01P2004/51 , C01P2004/60 , C01P2004/61 , C01P2006/40 , H01M4/131 , H01M4/1391
摘要： The invention is a process which provides a high purity lithiated manganese oxide (Li1+xMn2−yO4) from chemically made MnO2. The lithiated manganese oxide has an especially effective utility for use as a cathodic material in rechargeable batteries. The process of the invention includes blending a lithium compound with a chemically made manganese dioxide to form a manganese dioxide/lithium compound blend. The lithium compound in the blend is at least about one mole of lithium for every mole of manganese dioxide. The manganese dioxide and lithium compound in the blend undergo an ion exchange reaction to provide an ion replaced product where lithium ions have replaced sodium and potassium ions in the MnO2 to form an ion replaced product. Thereafter, the ion replaced product is heated or calcined to provide the lithiated manganese oxide.
摘要翻译：本发明是从化学制造的MnO 2提供高纯度锂化锰氧化物（Li1 + xMn2-yO4）的方法。锂二氧化锰在可再充电电池中用作阴极材料具有特别有效的用途。本发明的方法包括将锂化合物与化学制备的二氧化锰混合以形成二氧化锰/锂化合物共混物。混合物中的锂化合物对于每摩尔二氧化锰为至少约1摩尔的锂。共混物中的二氧化锰和锂化合物经历离子交换反应以提供离子替代产物，其中锂离子已经在MnO 2中取代了钠和钾离子以形成离子替代产物。此后，将离子置换产物加热或煅烧以提供锂化氧化锰。

10. 发明授权

US06521202B1 Oxygen ion conducting materials 失效
标题翻译：氧离子导电材料
公开(公告)号：US06521202B1
公开(公告)日：2003-02-18
申请号：US09344859
申请日：1999-06-28
申请人： John Vaughey , Michael Krumpelt , Xiaoping Wang , J. David Carter
发明人： John Vaughey , Michael Krumpelt , Xiaoping Wang , J. David Carter
IPC分类号： C01G4512
CPC分类号： H01M4/8621 , B01J23/002 , B01J23/10 , B01J23/34 , B01J2523/00 , C01G45/1264 , C01P2002/34 , C01P2002/52 , C01P2002/54 , C01P2002/77 , C01P2006/40 , H01M4/8652 , H01M4/9016 , B01J2523/24 , B01J2523/32 , B01J2523/3706 , B01J2523/72
摘要： An oxygen ion conducting ceramic oxide that has applications in industry including fuel cells, oxygen pumps, oxygen sensors, and separation membranes. The material is based on the idea that substituting a dopant into the host perovskite lattice of (La,Sr)MnO3 that prefers a coordination number lower than 6 will induce oxygen ion vacancies to form in the lattice. Because the oxygen ion conductivity of (La,Sr)MnO3 is low over a very large temperature range, the material exhibits a high overpotential when used. The inclusion of oxygen vacancies into the lattice by doping the material has been found to maintain the desirable properties of (La,Sr)MnO3, while significantly decreasing the experimentally observed overpotential.
摘要翻译：氧离子传导陶瓷氧化物，在工业中应用，包括燃料电池，氧气泵，氧传感器和分离膜。该材料基于以下思想：将掺杂剂置换为优选配位数低于6的（La，Sr）MnO 3的主体钙钛矿晶格将诱导在晶格中形成氧离子空位。由于（La，Sr）MnO 3的氧离子电导率在非常大的温度范围内较低，所以当使用时材料表现出高的超电势。已经发现通过掺杂材料将氧空位包含在晶格中已被发现保持了（La，Sr）MnO 3的所需性质，同时显着降低了实验观察到的超电势。

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