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91. 发明授权

US08124708B2 Polyolefin powder 有权
标题翻译：聚烯烃粉末
公开(公告)号：US08124708B2
公开(公告)日：2012-02-28
申请号：US12227705
申请日：2007-05-18
申请人： Thomas F. Ameye , Andre Frederich , Dominique Jan
发明人： Thomas F. Ameye , Andre Frederich , Dominique Jan
IPC分类号： C08F10/00 , C08F10/02 , C08F210/02 , F16L9/12
CPC分类号： C08F10/02 , C08F110/02 , C08F210/16 , Y10T428/2982 , C08F4/6555 , C08F2500/12 , C08F2500/07 , C08F2500/24 , C08F2/001 , C08F210/14 , C08F2500/05 , C08F210/08
摘要： Uncompounded polyolefin powder which is multimodal and has a particle size distribution such that D95 is less than 355 μm, D5 is at least 60 μm, and (D90−D10)/D50 is less than 1.2, where D95, D90, D50 and D10 are defined such that 95 wt %, 90 wt %, 50 wt % and 10 wt % of the polymer particles have a diameter of less than D95, D90, D50 and D10 respectively.
摘要翻译：未复合聚烯烃粉末为多峰，粒径分布为D95小于355μm，D5为至少60μm，（D90-D10）/ D50小于1.2，其中D95，D90，D50和D10为定义为聚合物颗粒的95重量％，90重量％，50重量％和10重量％分别具有小于D95，D90，D50和D10的直径。

92. 发明申请

US20120035047A1 CATALYST AND PROCESS FOR OBTAINING CATALYST OF HIGH ACTIVITY 有权
标题翻译：用于获得高活性催化剂的催化剂和方法
公开(公告)号：US20120035047A1
公开(公告)日：2012-02-09
申请号：US13260058
申请日：2010-03-10
申请人： Noemi Tatizawa , Jaime Correia Da Silva , Danielle De Carvalho Pinto Freitas , Katia Simone Zanco Palma , Richard Faraco Amorim , Leandro Dos Santos Silveira
发明人： Noemi Tatizawa , Jaime Correia Da Silva , Danielle De Carvalho Pinto Freitas , Katia Simone Zanco Palma , Richard Faraco Amorim , Leandro Dos Santos Silveira
IPC分类号： C08F4/646
CPC分类号： C08F10/00 , B01J21/04 , B01J23/02 , B01J37/035 , C08F110/02 , C08F110/06 , C08F210/16 , C08F4/025 , C08F4/6543 , C08F4/6555 , C08F4/022 , C08F2500/12 , C08F2500/24 , C08F210/08
摘要： The present invention relates to a process for obtaining a catalyst of high activity based on a mixture of supports, more specifically, the mixture of supports being Al2O3 plus MgCl2, intended for the production of polyolefins. The catalyst of the present invention involves the use of a spherical support based on special alumina that serves as a porous matrix, which is impregnated, by precipitation, with magnesium chloride by dissolving the latter in ethers and/or alcohols.
摘要翻译：本发明涉及一种基于载体的混合物获得高活性的催化剂的方法，更具体地说，用于生产聚烯烃的Al 2 O 3加MgCl 2的载体混合物。本发明的催化剂包括使用基于特殊氧化铝的球形载体，其作为多孔基质，其通过沉淀而被氯化镁浸渍在醚和/或醇中而被浸渍。

93. 发明申请

US20100160154A1 Magnesium Chloroakolate-Based Catalyst Precursors 失效
标题翻译：氯化钒酸镁催化剂前体
公开(公告)号：US20100160154A1
公开(公告)日：2010-06-24
申请号：US12308623
申请日：2007-06-01
申请人： Giampiero Morini , Antonio Cristofori , Benedetta Gaddi , Dario Liguori , Joachim T. M. Pater , Gianni Vitale
发明人： Giampiero Morini , Antonio Cristofori , Benedetta Gaddi , Dario Liguori , Joachim T. M. Pater , Gianni Vitale
IPC分类号： C08F4/64 , C08F4/643
CPC分类号： C08F10/00 , C08F110/02 , C08F110/06 , C08F210/16 , C08F4/6548 , C08F4/6555 , C08F4/651 , C08F2500/18 , C08F2500/12 , C08F210/06 , C08F210/08
摘要： Catalyst precursors comprising Mg, Cl, Ti, and OR groups that are in molar ratios defined by the formula MgClnTip(OR)(2-n)+4p in which n is from 0.3 to less than 1.7, p is lower than 0.6, the molar ratio (OR)/Cl is lower than 4 and R is C1-C15 hydrocarbon groups. The said precursor, just upon activation with organo-Al compounds, are able to advantageously polymerize ethylene and alpha olefins, and that upon reaction with halogenating compounds generate in high yields catalyst components with high polymerization activity particularly in the polymerization of propylene also in combination with 1,3-diethers.
摘要翻译：包含Mg，Cl，Ti和OR基团的催化剂前体，其摩尔比由式MgClnTip（OR）（2-n）+ 4p定义，其中n为0.3至小于1.7，p低于0.6，摩尔比（OR）/ Cl低于4，R为C1-C15烃基。所述前体刚好在有机铝化合物活化后能够有利地聚合乙烯和α-烯烃，并且当与卤化化合物反应时，产生高产率的催化剂组分，具有高聚合活性，特别是在丙烯的聚合中也与 1,3-二醚。

94. 发明授权

US07683003B2 Method for identifying Ziegler-Natta cocatalysts 有权
标题翻译：识别齐格勒 - 纳塔助催化剂的方法
公开(公告)号：US07683003B2
公开(公告)日：2010-03-23
申请号：US11596335
申请日：2005-05-13
申请人： Richard E. Campbell, Jr. , Sylvie Desjardins , Phillip D. Hustad , Duane R. Romer
发明人： Richard E. Campbell, Jr. , Sylvie Desjardins , Phillip D. Hustad , Duane R. Romer
IPC分类号： C08F4/64 , C08F4/642 , C08F4/646
CPC分类号： B01J31/0272 , B01J19/0046 , B01J27/138 , B01J31/0212 , B01J31/128 , B01J31/143 , B01J31/26 , B01J2219/00283 , B01J2219/00286 , B01J2219/00308 , B01J2219/00315 , B01J2219/00322 , B01J2219/00353 , B01J2219/00369 , B01J2219/00423 , B01J2219/00477 , B01J2219/00495 , B01J2219/00585 , B01J2219/00689 , B01J2219/00691 , B01J2219/00704 , B01J2219/00707 , B01J2219/00736 , B01J2219/00738 , B01J2219/00747 , C08F210/16 , C08F4/6555 , C08F210/14 , C08F2500/12
摘要： A method for identifying a catalyst composition for use in the heterogeneous Ziegler-Natta addition polymerization of an olefin monomer, said catalyst composition comprising a procatalyst comprising a magnesium and titanium containing procatalyst and a cocatalyst said method comprising: a) providing a library comprising at least one procatalyst compound, b) forming a catalyst composition library by contacting the member of said procatalyst library with one or more cocatalysts and contacting the resulting mixture with an olefin monomer under olefin polymerization conditions thereby causing the polymerization reaction to take place, c) measuring at least one variable of interest during the polymerization, and d) selecting the catalyst composition of interest by reference to said measured variable.
摘要翻译：一种用于鉴定用于烯烃单体的异质齐格勒 - 纳塔加成聚合的催化剂组合物的方法，所述催化剂组合物包含含有镁和钛的前催化剂的前催化剂和助催化剂，所述方法包括：a）提供至少包含一种主催化剂化合物，b）通过使所述前催化剂文库的成员与一种或多种助催化剂接触而形成催化剂组合物文库，并在烯烃聚合条件下使所得混合物与烯烃单体接触，从而引起聚合反应，c）在聚合过程中至少一个感兴趣的变量，以及d）通过参考所述测量的变量来选择感兴趣的催化剂组合物。

95. 发明授权

US07659223B2 Process for preparing an olefin polymerization catalyst component with improved high temperature activity 有权
标题翻译：制备具有改善的高温活性的烯烃聚合催化剂组分的方法
公开(公告)号：US07659223B2
公开(公告)日：2010-02-09
申请号：US10529812
申请日：2003-09-30
申请人： Timo Leinonen , Peter Denifl , Holger Pöhler
发明人： Timo Leinonen , Peter Denifl , Holger Pöhler
IPC分类号： B01J37/08
CPC分类号： C08F110/06 , C08F4/651 , C08F4/6555 , C08F2500/12
摘要： The invention refers to a process for preparing a Group 2 metal/transition metal olefin polymerization catalyst component in particulate form having an improved high temperature activity and the use thereof in a process for polymerizing olefins.
摘要翻译：本发明涉及一种制备具有改善的高温活性的颗粒形式的第2族金属/过渡金属烯烃聚合催化剂组分的方法及其在烯烃聚合方法中的用途。

96. 发明授权

US07649061B2 Process for preparing a poly-1-olefin in the presence of a Ziegler catalyst 有权
标题翻译：在齐格勒催化剂存在下制备聚-1-烯烃的方法
公开(公告)号：US07649061B2
公开(公告)日：2010-01-19
申请号：US11658808
申请日：2005-07-27
申请人： Friedhelm Gundert
发明人： Friedhelm Gundert
IPC分类号： C08F4/42
CPC分类号： C08F10/00 , C08F110/02 , C08F4/6548 , C08F4/6555 , C08F2500/12 , C08F2500/17 , C08F2500/18 , C08F2500/24
摘要： The invention relates to a process for preparing a poly-1-olefin by polymerization of a 1-olefin of the formula R4CH═CH2, where R4 is hydrogen or an alkyl radical having from 1 to 10 carbon atoms, in suspension, in solution or in the gas phase, at a temperature of from 20 to 200° C. and a pressure of from 0.5 to 50 bar, in the presence of a catalyst which comprises the reaction product of a magnesium alkoxide with a transition metal compound (=component a) and an organometallic compound (=component b) and whose component a has been prepared in a manner having the feature that a magnesium alkoxide powder having a mean particle size, expressed as the d50, in the range from 100 to 1000 μm is firstly processed by dry milling in a mill under inert conditions to produce magnesium alkoxide powder having a mean particle size, expressed as the d50, of less than 15 μm, then suspended in an inert hydrocarbon in which the magnesium alkoxide is insoluble, and is reacted immediately without further pretreatment with a transition metal compound of titanium, zirconium, vanadium or chromium.
摘要翻译：本发明涉及通过聚合式R 4 CH-CH 2的1-烯烃（其中R 4是氢或具有1至10个碳原子的烷基，在悬浮液中，在溶液中或溶液中）聚合制备聚-1-烯烃的方法，在气相中，在20〜200℃的温度和0.5〜50巴的压力下，在含有烷氧基镁与过渡金属化合物的反应产物（=组分a ）和有机金属化合物（=成分b），其成分a以具有以d50表示的平均粒径的烷氧基镁粉末在100〜1000μm的范围内的方式制备，首先被处理通过在惰性条件下在研磨机中干研磨以产生平均粒度（d50表示）小于15μm的烷氧基镁粉末，然后悬浮在惰性烃中，其中烷氧化镁不溶，并且立即反应而没有愤怒用钛，锆，钒或铬的过渡金属化合物预处理。

97. 发明授权

US07601783B2 Method of controlling olefin polymerization 失效
标题翻译：控制烯烃聚合的方法
公开(公告)号：US07601783B2
公开(公告)日：2009-10-13
申请号：US11099328
申请日：2005-04-05
申请人： Mark B. Davis , James Daniel Madden
发明人： Mark B. Davis , James Daniel Madden
IPC分类号： C08L23/00 , C08L23/04
CPC分类号： C08F10/00 , C08F10/02 , C08F110/02 , C08F210/16 , C08F4/6555 , C08F2/38 , C08F2500/01 , C08F2500/02 , C08F2500/05 , C08F2500/12 , C08F210/14
摘要： A method of making polyolefin with a target melt flow index and melt flow rate is disclosed. The method polymerizes one or more olefinic monomers in a single reactor containing a bicomponent catalyst system. The catalyst system includes a first catalyst component and a second catalyst component each characterized by a catalyst productivity and a chain-transfer-agent response. The single reactor has a chain-transfer-agent concentration and a temperature. The productivity of the second catalyst component is substantially different temperature dependent than that of the first catalyst component. The chain-transfer-agent response of the second catalyst component is substantially different sensitive than that of the first catalyst component. The temperature of the reactor is adjusted so that the melt flow ratio approaches the target value. The chain transfer agent concentration in the reactor is adjusted so that the melt index approaches the target value.
摘要翻译：公开了制备具有目标熔体流动指数和熔体流动速率的聚烯烃的方法。该方法在含有双组分催化剂体系的单个反应器中聚合一种或多种烯属单体。催化剂体系包括第一催化剂组分和第二催化剂组分，每个催化剂组分的特征在于催化剂生产率和链转移剂反应。单个反应器具有链转移剂浓度和温度。第二催化剂组分的生产率与第一催化剂组分的生产率基本上不同。第二催化剂组分的链转移剂反应与第一催化剂组分的反应基本不同。调整反应器的温度使得熔体流动比接近目标值。调节反应器中的链转移剂浓度，使得熔体指数接近目标值。

98. 发明授权

US07504464B2 Process for control of polymer fines in a gas-phase polymerization 失效
标题翻译：在气相聚合中控制聚合物细粉的方法
公开(公告)号：US07504464B2
公开(公告)日：2009-03-17
申请号：US10553689
申请日：2004-04-07
申请人： Stephanie M. Whited , Michael D. Turner , Michael A. Kinnan , Robert J. Jorgensen
发明人： Stephanie M. Whited , Michael D. Turner , Michael A. Kinnan , Robert J. Jorgensen
IPC分类号： C08F4/642
CPC分类号： C08F10/00 , C08F210/16 , C08F4/6555 , C08F2/34 , C08F2/001 , C08F210/14 , C08F2500/12
摘要： A gas phase polymerization process comprising: (1) preparing a solution of a catalyst precursor comprising a mixture of magnesium and titanium compounds, an electron donor and a solvent; (2) adding a filler to the solution from step (1) to form a slurry; (3) spray drying the slurry from step (2) at a temperature of 100 to 140° C. to form a spray dried precursor, (4) slurring the spray dried precursor from step (3) in mineral oil, (5) partially or fully pre-activating the catalyst precursor by contacting the slurry of (4) with one or more Lewis Acids, and (6) transferring the partially or fully activated precursor from step (5) into a gas phase reactor in which an olefin polymerization reaction is in progress.
摘要翻译：一种气相聚合方法，包括：（1）制备包含镁和钛化合物，电子给体和溶剂的混合物的催化剂前体溶液; （2）向来自步骤（1）的溶液中加入填料以形成浆料; （3）在100〜140℃的温度下对来自步骤（2）的浆料进行喷雾干燥以形成喷雾干燥的前体，（4）将来自步骤（3）的喷雾干燥的前体在矿物油中sl浆，（5）部分或通过使（4）的浆料与一种或多种路易斯酸接触来完全预活化催化剂前体，和（6）将来自步骤（5）的部分或完全活化的前体转移到气相反应器中，其中烯烃聚合反应正在进行中

99. 发明申请

US20080194781A1 Process for Preparing Catalyst Components for the Olefin Polymerization 失效
标题翻译：制备烯烃聚合催化剂组分的方法
公开(公告)号：US20080194781A1
公开(公告)日：2008-08-14
申请号：US11629274
申请日：2005-06-01
申请人： Paolo Vincenzi , Rosa Spoto
发明人： Paolo Vincenzi , Rosa Spoto
IPC分类号： C08F4/44 , C07C31/30 , B32B5/16
CPC分类号： C08F10/00 , C08F110/02 , Y10T428/2982 , C08F4/6543 , C08F4/6567 , C08F4/6555 , C08F2500/12 , C08F2500/24 , C08F2500/18
摘要： Process for the preparation of a solid catalyst component for the polymerization of olefins, the process comprising the steps of:—continuously contacting solid particles of a MgCl2.mROH adduct, wherein 0.5
摘要翻译：用于制备用于烯烃聚合的固体催化剂组分的方法，所述方法包括以下步骤： - 连续接触MgCl 2··MOH加成物的固体颗粒，其中0.5

100. 发明授权

US07354981B2 Polyethylene catalyst and a process for preparing the same 有权
标题翻译：聚乙烯催化剂及其制备方法
公开(公告)号：US07354981B2
公开(公告)日：2008-04-08
申请号：US11003236
申请日：2004-12-03
申请人： Mingwei Xiao , Shijiong Yu , Xiaofeng Ye
发明人： Mingwei Xiao , Shijiong Yu , Xiaofeng Ye
IPC分类号： C08F110/02
CPC分类号： B01J31/0211 , B01J31/068 , B01J31/122 , B01J31/128 , B01J31/143 , B01J2231/122 , B01J2531/22 , B01J2531/31 , B01J2531/46 , C08F10/00 , C08F110/02 , C08F4/6555 , C08F2500/18 , C08F2500/12
摘要： The present invention discloses a polyethylene catalyst and a process for preparing the same, said catalyst being composed of a main component of catalyst and a cocatalyst, wherein the main component of catalyst is prepared by reacting: (1) a magnesium-alcohol complex, (2) an alkyl aluminum compound having a formula R3nAlCl3-n supported on silica, and (3) a titanium compound having a formula Ti(OR2)mCl4-m, and the cocatalyst is an organic aluminum compound. The catalyst of the present invention has advantages including high polymerization activity, less difference between the polymerization activities at low hydrogen level condition and at high hydrogen level condition, stable polymerization reaction, good particle morphology of catalyst, and less fine powder of polymer product.
摘要翻译：本发明公开了一种聚乙烯催化剂及其制备方法，所述催化剂由催化剂的主要成分和助催化剂组成，其中催化剂的主要成分是通过使（1）镁 - 醇络合物，（ 2）负载在二氧化硅上的具有式R 3 3 AlCl 3-n N的烷基铝化合物，和（3）具有式Ti（OR 2）3 Cl 4-m，助催化剂是有机铝化合物。本发明的催化剂具有聚合活性高，氢气低条件下的聚合活性与高氢水平条件下的差异小，聚合反应稳定，催化剂粒子形态好，聚合物产品细微粉末等优点。

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