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21. 发明申请

US20150239741A1 Production of graphene materials in a cavitating fluid 有权
标题翻译：在气蚀液中生产石墨烯材料
公开(公告)号：US20150239741A1
公开(公告)日：2015-08-27
申请号：US13999397
申请日：2014-02-21
申请人： David Joseph Burton , Bor Z. Jang , Aruna Zhamu
发明人： David Joseph Burton , Bor Z. Jang , Aruna Zhamu
IPC分类号： C01B31/04 , C08G65/48 , C07B41/02 , C07B43/04 , C07B43/08 , C07B41/04 , C08G63/91 , C08F120/32 , C07D301/02 , C07B41/08
CPC分类号： C01B31/0469 , C01B32/19 , C01B32/23 , C07D301/02 , C08G65/321 , C08L71/02
摘要： The invention provides a method of producing a graphene material from a starting graphitic material. In an embodiment, the method comprises: (a) dispersing the starting graphitic material in a liquid medium to form a graphite suspension; and (b) introducing the graphite suspension into a hydrodynamic cavitation reactor that generates and collapses cavitation or bubbles in the liquid medium to exfoliate and separate graphene planes from the starting graphitic material for producing the graphene material. The process is fast (minutes as opposed to hours or days of conventional processes), environmentally benign, and highly scalable. The reactor can concurrently perform the functions of graphene production, chemical functionalization, dispersion, and mixing with a polymer to make a composite.
摘要翻译：本发明提供从起始石墨材料生产石墨烯材料的方法。在一个实施方案中，该方法包括：（a）将起始石墨材料分散在液体介质中以形成石墨悬浮液; 和（b）将石墨悬浮液引入到流体动力空化反应器中，该反应器在液体介质中产生和塌陷空化或气泡，以将石墨烯平面与用于生产石墨烯材料的起始石墨材料分离和分离。这个过程是快速的（分钟，而不是常规过程的几天或几天），环境友好和高度可扩展。反应器可以同时执行石墨烯生产，化学官能化，分散和与聚合物混合以制备复合材料的功能。

22. 发明授权

US09112210B2 Rechargeable lithium cell having a phthalocyanine-based high-capacity cathode 有权
标题翻译：具有酞菁类高容量阴极的可充电锂电池
公开(公告)号：US09112210B2
公开(公告)日：2015-08-18
申请号：US13506778
申请日：2012-05-17
申请人： Guorong Chen , Yanbo Wang , Aruna Zhamu , Bor Z. Jang
发明人： Guorong Chen , Yanbo Wang , Aruna Zhamu , Bor Z. Jang
IPC分类号： H01M10/0525 , H01M4/133 , B82Y30/00 , H01M4/60 , H01M10/052 , H01M4/36 , H01M4/587
CPC分类号： H01M4/133 , B82Y30/00 , H01M4/364 , H01M4/587 , H01M4/60 , H01M10/052 , Y02E60/122
摘要： A rechargeable lithium cell comprising: (a) an anode; (b) a cathode comprising a hybrid cathode active material composed of a graphene material and a phthalocyanine compound, wherein the graphene material is in an amount of from 0.1% to 99% by weight based on the total weight of the graphene material and the phthalocyanine compound combined; and (c) a porous separator disposed between the anode and the cathode and electrolyte in ionic contact with the anode and the cathode. This secondary cell exhibits a long cycle life and the best cathode specific capacity and best cell-level specific energy of all rechargeable lithium-ion cells ever reported.
摘要翻译：一种可再充电锂电池，包括：（a）阳极; （b）包含由石墨烯材料和酞菁化合物组成的混合阴极活性材料的阴极，其中石墨烯材料的量为基于石墨烯材料和酞菁的总重量的0.1重量％至99重量％复合组合和（c）设置在阳极和阴极之间的多孔隔离体和与阳极和阴极离子接触的电解质。该二次电池显示出所有可再充电锂离子电池的循环寿命长以及最佳阴极比容量和最佳电池级比能。

23. 发明授权

US09029019B2 Carbon anode compositions for lithium ion batteries 有权
公开(公告)号：US09029019B2
公开(公告)日：2015-05-12
申请号：US11893398
申请日：2007-08-17
申请人： Bor Z. Jang , Aruna Zhamu , Jinjun Shi , Jiusheng Guo
发明人： Bor Z. Jang , Aruna Zhamu , Jinjun Shi , Jiusheng Guo
IPC分类号： H01M4/587 , H01M4/131 , H01G11/50 , H01M10/0525 , H01M4/62
CPC分类号： H01M4/587 , H01G11/50 , H01M4/131 , H01M4/621 , H01M4/624 , H01M4/625 , H01M10/0525 , Y02E60/122 , Y02E60/13
摘要： A lithium secondary battery comprising a positive electrode, a negative electrode comprising a carbonaceous material which is capable of absorbing and desorbing lithium ions, and a non-aqueous electrolyte disposed between the negative electrode and the positive electrode. The carbonaceous material comprises a graphite crystal structure having an interplanar spacing d002 of at least 0.400 nm (preferably at least 0.55 nm) as determined from a (002) reflection peak in powder X-ray diffraction. This larger interplanar spacing implies a larger interstitial space between two graphene planes to accommodate a greater amount of lithium. The battery exhibits an exceptional specific capacity, excellent reversible capacity, and long cycle life.

24. 发明授权

US08947854B2 Spacer-modified graphene electrode for supercapacitor 有权
标题翻译：用于超级电容器的间隔改性石墨烯电极
公开(公告)号：US08947854B2
公开(公告)日：2015-02-03
申请号：US13573844
申请日：2012-10-09
申请人： Aruna Zhamu , Zhenning Yu , Chen-guang Liu , Bor Z. Jang
发明人： Aruna Zhamu , Zhenning Yu , Chen-guang Liu , Bor Z. Jang
IPC分类号： H01G9/00 , H01G11/36 , B82Y30/00
CPC分类号： H01G11/36 , B82Y30/00 , B82Y40/00 , H01G11/32 , Y02E60/13 , Y02T10/7022 , Y10S977/734 , Y10S977/932 , Y10S977/948
摘要： A spacer-modified nano graphene platelet electrode, comprising: (a) multiple nano graphene platelets or sheets having an average thickness smaller than 10 nm; and (b) discrete, non-metallic nano-scaled particles that are disposed between two graphene platelets or sheets to serve as a spacer. In such a spacer-modified graphene electrode, large amounts of electrolyte-accessible pores are formed, enabling the formation of large amounts of electric double layer charges in a supercapacitor, which exhibits an exceptionally high specific capacitance.
摘要翻译：一种间隔物改性的纳米石墨烯片晶电极，包括：（a）平均厚度小于10nm的多个纳米石墨烯片晶或片; 和（b）分散的非金属纳米级粒子，其设置在两个石墨烯片晶片之间以用作间隔物。在这种间隔物改性的石墨烯电极中，形成大量的电解质可接近的孔，使得能够在超级电容器中形成大量的双电层电荷，这表现出特别高的比电容。

25. 发明申请

US20140363746A1 Lithium secondary batteries containing non-flammable quasi-solid electrolyte 有权
标题翻译：锂二次电池含有不易燃的准固体电解质
公开(公告)号：US20140363746A1
公开(公告)日：2014-12-11
申请号：US13986814
申请日：2013-06-10
申请人： Hui He , Bor Z. Jang , Yanbo Wang , Aruna Zhamu
发明人： Hui He , Bor Z. Jang , Yanbo Wang , Aruna Zhamu
IPC分类号： H01M10/056 , H01M10/052
CPC分类号： H01M10/052 , H01M4/136 , H01M4/5825 , H01M10/0525 , H01M10/0568 , H01M10/0569 , H01M12/08 , H01M2004/028 , H01M2300/0028 , Y02E60/122 , Y02E60/128 , Y02T10/7011
摘要： A rechargeable lithium cell comprising a cathode having a cathode active material, an anode having an anode active material, a porous separator electronically separating the anode and the cathode, a non-flammable quasi-solid electrolyte in contact with the cathode and the anode, wherein the electrolyte contains a lithium salt dissolved in a first organic liquid solvent with a concentration sufficiently high so that the electrolyte exhibits a vapor pressure less than 0.01 kPa when measured at 20° C., a flash point at least 20 degrees Celsius higher than the flash point of the first organic liquid solvent alone, a flash point higher than 150° C., or no flash point. This battery cell is non-flammable and safe, has a long cycle life, high capacity, and high energy density.
摘要翻译：一种可再充电锂电池，包括具有阴极活性材料的阴极，具有阳极活性材料的阳极，电子分离阳极和阴极的多孔隔板，与阴极和阳极接触的不可燃的准固体电解质，其中电解质含有溶解在浓度足够高的第一有机液体溶剂中的锂盐，使得当在20℃下测量时，电解质的蒸汽压力低于0.01kPa，闪点高于闪光灯的至少20摄氏度第一有机液体溶剂点，闪点高于150℃，或无闪点。该电池不易燃，安全，循环寿命长，容量大，能量密度高。

26. 发明授权

US08865040B2 Highly conductive composites for fuel cell flow field plates and bipolar plates 有权
标题翻译：用于燃料电池流场板和双极板的高导电复合材料
公开(公告)号：US08865040B2
公开(公告)日：2014-10-21
申请号：US13021041
申请日：2011-02-04
申请人： Bor Z. Jang , Aruna Zhamu , Lulu Song
发明人： Bor Z. Jang , Aruna Zhamu , Lulu Song
IPC分类号： C04B35/00 , H01M8/02 , C08J5/04 , H01B1/24
CPC分类号： H01M8/0221 , C08J5/04 , H01B1/24 , H01M8/0213 , H01M8/0226 , H01M8/0228 , Y02E60/50 , Y02P70/56
摘要： This invention provides a fuel cell flow field plate or bipolar plate having flow channels on faces of the plate, comprising an electrically conductive polymer composite. The composite is composed of (A) at least 50% by weight of a conductive filler, comprising at least 5% by weight reinforcement fibers, expanded graphite platelets, graphitic nano-fibers, and/or carbon nano-tubes; (B) polymer matrix material at 1 to 49.9% by weight; and (C) a polymer binder at 0.1 to 10% by weight; wherein the sum of the conductive filler weight %, polymer matrix weight % and polymer binder weight % equals 100% and the bulk electrical conductivity of the flow field or bipolar plate is at least 100 S/cm. The invention also provides a continuous process for cost-effective mass production of the conductive composite-based flow field or bipolar plate.
摘要翻译：本发明提供了一种在板的表面上具有流动通道的燃料电池流场板或双极板，包括导电聚合物复合材料。复合材料由（A）至少50重量％的导电填料构成，包括至少5重量％的增强纤维，膨胀石墨片，石墨纳米纤维和/或碳纳米管; （B）1〜49.9重量％的聚合物基质材料; 和（C）0.1至10重量％的聚合物粘合剂; 其中导电填料重量％，聚合物基质重量％和聚合物粘合剂重量％的总和等于100％，并且流场或双极板的体电导率至少为100S / cm。本发明还提供了一种用于成本有效地批量生产基于导电复合材料的流场或双极板的连续方法。

27. 发明申请

US20140308449A1 Process for producing continuous graphitic fibers from living graphene molecules 有权
标题翻译：从活性石墨烯分子生产连续石墨纤维的方法
公开(公告)号：US20140308449A1
公开(公告)日：2014-10-16
申请号：US13986208
申请日：2013-04-15
申请人： Aruna Zhamu , Bor Z Jang
发明人： Aruna Zhamu , Bor Z Jang
IPC分类号： C01B31/04
CPC分类号： C01B31/04 , C01B32/20 , D01D1/02 , D01D5/04 , D01D10/02 , D01F9/12
摘要： A process for producing a continuous graphitic fiber, comprising: (a) preparing a graphene oxide gel having living graphene oxide molecules or functionalized graphene chains dissolved in a fluid medium; (b) depositing at least a continuous filament of graphene oxide gel onto a supporting substrate under a condition of stress-induced molecular alignment of living graphene oxide molecules along a filament axis direction; (c) removing the fluid medium to form a continuous graphene oxide fiber, having an inter-plane spacing d002 of 0.4 nm to 1.2 nm and an oxygen content no less than 5% by weight; and (d) heat treating the continuous graphene oxide fiber to form the continuous graphitic fiber at a temperature higher than 100° C. (preferably >600° C.) to an extent that an inter-plane spacing d002 is decreased to a value of 0.3354-0.4 nm and the oxygen content is decreased to less than 5% by weight.
摘要翻译：一种生产连续石墨纤维的方法，包括：（a）制备具有溶解在流体介质中的活性氧化石墨烯分子或官能化石墨烯链的石墨烯氧化物凝胶; （b）在活性石墨烯氧化物分子沿着长丝轴线方向的应力诱导分子取向的条件下，将至少一层氧化石墨烯凝胶的连续长丝沉积到支撑基底上; （c）除去流体介质以形成连续的石墨烯氧化纤维，其平面间距d002为0.4nm至1.2nm，氧含量不低于5wt％; 和（d）在高于100℃（优选> 600℃）的温度下对连续的石墨烯氧化纤维进行热处理以形成连续的石墨纤维，使得平面间距d002降低到 0.3354-0.4nm，氧含量降低到小于5重量％。

28. 发明授权

US08765302B2 Graphene-enabled vanadium oxide cathode and lithium cells containing same 有权
标题翻译：含有石墨烯的钒氧化物阴极和含有相同的锂电池
公开(公告)号：US08765302B2
公开(公告)日：2014-07-01
申请号：US13134782
申请日：2011-06-17
申请人： Guorong Chen , Aruna Zhamu , Bor Z. Jang , Zhenning Yu
发明人： Guorong Chen , Aruna Zhamu , Bor Z. Jang , Zhenning Yu
IPC分类号： H01M4/13 , H01M10/052 , H01M4/587 , C01G31/02 , H01M4/485 , H01M4/58 , H01M4/36 , B82Y30/00 , H01M4/76 , H01M4/62 , H01M4/48 , C01G31/00 , H01M4/02
CPC分类号： H01M10/052 , B82Y30/00 , C01G31/00 , C01G31/02 , C01P2004/03 , C01P2004/17 , C01P2004/24 , C01P2004/61 , C01P2004/64 , C01P2006/40 , H01M4/362 , H01M4/483 , H01M4/485 , H01M4/5825 , H01M4/587 , H01M4/625 , H01M4/76 , H01M2004/028 , Y02E60/122
摘要： A nano graphene-enabled vanadium oxide composite composition for use as a lithium battery cathode active material, wherein the composite composition is formed of one or a plurality of graphene, graphene oxide, or graphene fluoride sheets or platelets and a plurality of nano-particles, nano-rods, nano-wires, nano-sheets, and/or nano-belts of a vanadium oxide with a size smaller than 100 nm (preferably smaller than 20 nm, further preferably smaller than 10 nm, and most preferably smaller than 5 nm), and wherein the graphene, graphene oxide, or graphene fluoride (having a thickness
摘要翻译：一种用作锂电池正极活性材料的纳米石墨烯氧化钒复合材料组合物，其中该复合组合物由一个或多个石墨烯，氧化石墨烯或氟化石墨烯薄片或片状微粒和多个纳米颗粒形成，尺寸小于100nm（优选小于20nm，进一步优选小于10nm，最优选小于5nm）的氧化钒的纳米棒，纳米线，纳米片和/或纳米带），并且其中所述石墨烯，氧化石墨烯或氟化石墨烯（厚度<20nm，优选<10nm，进一步优选<5nm，最优选单层或小于5层）的量为基于石墨烯，氧化石墨烯或氟化石墨烯和氧化钒的总重量，为0.01重量％至50重量％（优选<10重量％）。这种电极材料表现出前所未有的优异的比容量，容量保持率和速率能力特性的组合。

29. 发明授权

US08753539B2 Environmentally benign graphite intercalation compound composition for exfoliated graphite, flexible graphite, and nano-scaled graphene platelets 有权
标题翻译：用于剥离石墨，柔性石墨和纳米级石墨烯血小板的环保良性石墨插层化合物组合物
公开(公告)号：US08753539B2
公开(公告)日：2014-06-17
申请号：US11881390
申请日：2007-07-27
申请人： Aruna Zhamu , Bor Z. Jang
发明人： Aruna Zhamu , Bor Z. Jang
IPC分类号： C01B31/04
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/15 , C01B32/19 , C01B32/22 , C01B32/225 , C01B2204/04
摘要： A carboxylic-intercalated graphite compound composition for the production of exfoliated graphite, flexible graphite, or nano-scaled graphene platelets. The composition comprises a layered graphite with interlayer spaces or interstices and a carboxylic acid residing in at least one of the interstices, wherein the composition is prepared by a chemical oxidation reaction which uses a combination of a carboxylic acid and hydrogen peroxide as an intercalate source. Alternatively, the composition may be prepared by an electrochemical reaction, which uses a carboxylic acid as both an electrolyte and an intercalate source. Exfoliation of the invented composition does not release undesirable chemical contaminants into air or drainage.
摘要翻译：用于生产剥离石墨，柔性石墨或纳米级石墨烯血小板的羧基插层石墨化合物组合物。所述组合物包含具有层间空间或空隙的层状石墨和位于至少一个间隙中的羧酸，其中所述组合物通过化学氧化反应制备，所述化学氧化反应使用羧酸和过氧化氢的组合作为插层源。或者，组合物可以通过电化学反应制备，其使用羧酸作为电解质和插层源。本发明组合物的剥落不会将不期望的化学污染物排放到空气或排水中。

30. 发明申请

US20140127488A1 Graphene oxide-coated graphitic foil and processes for producing same 有权
标题翻译：石墨烯氧化物被覆石墨箔及其制造方法
公开(公告)号：US20140127488A1
公开(公告)日：2014-05-08
申请号：US13694161
申请日：2012-11-02
申请人： Aruna Zhamu , Mingchao Wang , Wei Xiong , Bor Z. Jang
发明人： Aruna Zhamu , Mingchao Wang , Wei Xiong , Bor Z. Jang
IPC分类号： H01B1/04
CPC分类号： H01B1/04 , B82Y30/00 , B82Y40/00 , C01B32/192 , C01B32/198 , C01B32/20 , C01B32/23 , C01P2006/10 , C01P2006/40 , C01P2006/90 , Y10S977/734 , Y10S977/742 , Y10S977/89 , Y10T428/24975 , Y10T428/30
摘要： A graphene oxide-coated graphitic foil, composed of a graphitic substrate or core layer having two opposed primary surfaces and at least a graphene oxide coating layer deposited on at least one of the two primary surfaces, wherein the graphitic substrate layer has a thickness preferably from 0.34 nm to 1 mm, and the graphene oxide coating layer has a thickness preferably from 0.5 nm to 1 mm and an oxygen content of 0.01%-40% by weight based on the total graphene oxide weight. The graphitic substrate layer may be preferably selected from flexible graphite foil, graphene film, graphene paper, graphite particle paper, carbon-carbon composite film, carbon nano-fiber paper, or carbon nano-tube paper. This graphene oxide-coated laminate exhibits a combination of exceptional thermal conductivity, electrical conductivity, mechanical strength, surface smoothness, surface hardness, and scratch resistance unmatched by any thin-film material of comparable thickness range.
摘要翻译：一种石墨烯氧化物涂覆石墨箔，由石墨基底或具有两个相对的主表面的核心层和至少沉积在两个主表面中的至少一个上的氧化石墨烯涂层组成，其中石墨基底层的厚度优选为 0.34nm至1mm，并且氧化石墨烯氧化物涂层的厚度优选为0.5nm至1mm，氧含量为基于氧化石墨烯总重量的0.01％-40重量％。石墨基材层可优选选自柔性石墨箔，石墨烯膜，石墨烯纸，石墨颗粒纸，碳 - 碳复合膜，碳纳米纤维纸或碳纳米管纸。该氧化石墨烯氧化物涂层的层压材料显示了由具有相当厚度范围的任何薄膜材料而具有优异的导热性，导电性，机械强度，表面光滑度，表面硬度和耐划伤性的组合。

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