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41. 发明授权

US5310851A Spin-labelled thickeners 失效
标题翻译：自旋标记的增稠剂
公开(公告)号：US5310851A
公开(公告)日：1994-05-10
申请号：US13887
申请日：1993-02-04
申请人： Willie Lau
发明人： Willie Lau
IPC分类号： C08G18/10 , C08G18/48 , C08G18/00 , C08G18/28 , C08G18/77 , C08G18/81
CPC分类号： C08G18/4833 , C08G18/10
摘要： A hydrophobically-modified thickener having at least one hydrophilic portion and at least two terminal hydrophobic portions wherein at least one of the hydrophobic portions contains a stable free radical and its preparation are disclosed. The presence of the stable free radical permits analysis by spin-labelling analytical techniques, such as, for example, electron spin resonance.
摘要翻译：具有至少一个亲水部分和至少两个末端疏水部分的疏水改性增稠剂，其中至少一个疏水部分含有稳定的自由基，并且其制备被公开。稳定自由基的存在允许通过自旋标记分析技术进行分析，例如电子自旋共振。

42. 发明授权

US08304462B2 Process for making polymer composites having thermoplastic properties 失效
标题翻译：制备具有热塑性的聚合物复合材料的方法
公开(公告)号：US08304462B2
公开(公告)日：2012-11-06
申请号：US12655287
申请日：2009-12-28
申请人： Willie Lau , Rachel Z. Pytel , Joseph M. Rokowski
发明人： Willie Lau , Rachel Z. Pytel , Joseph M. Rokowski
IPC分类号： C08J11/04
CPC分类号： C08F6/22 , C08C1/14 , C08F220/06 , C08F220/14 , C08F220/18 , C08F2220/1825 , C08F2220/1883 , C08J11/04 , C08J2300/30 , C08J2319/00 , C08J2321/00 , C08L19/003 , C08L31/04 , C08L33/06 , C08L33/12 , C08L33/20 , C08L35/06 , C08L101/02 , Y02P20/143 , Y02W30/70 , Y10T428/24355 , Y10T428/24364 , Y10T428/2438 , Y10T428/24405 , C08L2666/04
摘要： The present invention provides methods of making composite materials comprising combining particles of crosslinked rubber with one or more aqueous polymer dispersion of a suspension polymer to form a mixture in aqueous dispersion, and, optionally, subjecting the aqueous dispersion mixture to solid state shear pulverization to form materials that can be processed as thermoplastics at crosslinked rubber concentrations of from 10 to as high as 95 wt. %, based on the total solids of the material. The method may further comprise kneading and/or compression molding the pulverized product to form useful articles, such as roofing membranes and shoe soles.
摘要翻译：本发明提供制备复合材料的方法，其包括将交联橡胶的颗粒与一种或多种悬浮聚合物的聚合物水分散体结合以在水分散体中形成混合物，以及任选地使水分散体混合物进行固态剪切粉碎以形成可在10至高达95wt。交联橡胶浓度下加工成热塑性塑料的材料。％，基于材料的总固体。该方法还可以包括捏合和/或压缩模制粉碎产品以形成有用的制品，例如屋顶膜和鞋底。

43. 发明申请

US20120164385A1 POLYMER RUBBER COMPOSITE SHINGLES WITH HIGH SOLAR REFLECTANCE 有权
标题翻译：聚合物橡胶复合材料具有高的太阳能反射性
公开(公告)号：US20120164385A1
公开(公告)日：2012-06-28
申请号：US13333320
申请日：2011-12-21
申请人： Harry R. HEULINGS , Willie LAU , Joseph M. ROKOWSKI
发明人： Harry R. HEULINGS , Willie LAU , Joseph M. ROKOWSKI
IPC分类号： E04D1/22 , B32B5/16
CPC分类号： E04D1/20 , C08J3/2053 , C08J7/042 , C08J2300/22 , C08J2317/00 , C08K3/22 , C08K5/092 , C08K2201/019 , C08L17/00 , C08L19/003 , C08L25/00 , C08L33/08 , Y02A30/255 , Y02B80/34 , Y10T428/2438
摘要： The present invention provides shaped articles comprising one or more composite layer of (i) a vulcanizate encapsulated in a colored or uncolored thermoplastic polymer matrix containing one or more passivating agent, and (ii) a reflective material chosen from colored fluidizable particles of a thermoplastic reflective colorant encapsulated vulcanizate, roofing granules, thermoplastic encapsulated roofing granules, the colored thermoplastic polymer matrix, and combinations thereof. The articles can be laminates of colored or reflective layers on uncolored or other layers, or one or more colored layer having colored fluidizable particles are dispersed within the surface of the uppermost composite layer or having either the colored fluidizable particles or the granules are dispersed on the surface of the composite layer or are adhered thereto with a thermoplastic resin. Roofing shingles are provided.
摘要翻译：本发明提供了一种成形制品，其包含一种或多种复合层，所述复合层包含（i）包封在含有一种或多种钝化剂的有色或未着色的热塑性聚合物基质中的硫化胶，和（ii）选自热塑性反射的有色可流化颗粒的反射材料着色剂包封的硫化橡胶，屋顶颗粒，热塑性包封屋顶颗粒，着色热塑性聚合物基质及其组合。制品可以是未着色或其它层上的有色或反射层的层压体，或者具有可着色的可流化颗粒的一个或多个着色层分散在最上层复合层的表面内，或者将着色的可流化颗粒或颗粒分散在复合层的表面或者用热塑性树脂粘附在其上。提供屋顶木瓦。

44. 发明申请

US20100112344A1 Blocking and stain resistant surface treated articles and methods for making 有权
标题翻译：防粘和防污的表面处理制品及其制造方法
公开(公告)号：US20100112344A1
公开(公告)日：2010-05-06
申请号：US12589587
申请日：2009-10-26
申请人： Bonnie E. Baker , Arnold S. Brownell , Nancy P. Buford , Willie Lau , Joseph J. Spanier
发明人： Bonnie E. Baker , Arnold S. Brownell , Nancy P. Buford , Willie Lau , Joseph J. Spanier
IPC分类号： B32B27/30 , B32B27/06 , C08J7/04 , B05D7/00
CPC分类号： C09D143/02 , Y10T428/273 , Y10T428/31855 , Y10T428/31895
摘要： The present invention provides surface treated articles comprising a recoatable surface treatment of an acrylic or vinyl polymer that does not change the appearance of the treated surface, and which imparts blocking resistance and/or stain and dirt pickup resistance to the treated surface. The one or more acrylic or vinyl polymer has a number average molecular weight of from 1,000 to 100,000, a glass transition temperature of −10° C. or higher, preferably, 30° C. or higher, and comprises the polymerization product of one or more non-ionic monomer, such as methyl methacrylate, with up to 47 wt. % of an ethylenically unsaturated acid monomer and, preferably, is non-migrating under use conditions. When dry, the surface treatments may form a layer of domains of polymer distributed all over the treated surface, rather than a film. Treated articles include coating or painted articles and elastomer films exhibiting blocking and stain resistance, and uncoated wood, glass, metal or plastic articles and laminates, such as countertops, exhibiting stain and dirt pickup resistance.
摘要翻译：本发明提供了表面处理制品，其包括丙烯酸或乙烯基聚合物的可重复表面处理，其不会改变经处理的表面的外观，并且赋予对经处理的表面的抗粘连性和/或污渍和污垢拾取抗性。一种或多种丙烯酸或乙烯基聚合物的数均分子量为1,000至100,000，玻璃化转变温度为-10℃或更高，优选为30℃或更高，并且包含一种或多种聚合产物更多的非离子单体，如甲基丙烯酸甲酯，高达47wt。％的烯键式不饱和酸单体，并且优选在使用条件下不迁移。当干燥时，表面处理可以形成分布在整个处理过的表面上的聚合物的一层，而不是膜。被处理的制品包括涂层或涂漆制品以及显示阻挡和防污性的弹性体膜，以及未涂覆的木材，玻璃，金属或塑料制品以及层压板，例如台面，具有防污染和抗污性。

45. 发明申请

US20100016456A1 Process for making polymer composites having thermoplastic properties 失效
标题翻译：制备具有热塑性的聚合物复合材料的方法
公开(公告)号：US20100016456A1
公开(公告)日：2010-01-21
申请号：US12459975
申请日：2009-07-10
申请人： Carlos A. Cruz , Willie Lau , Joseph M. Rokowski , Qi Wang
发明人： Carlos A. Cruz , Willie Lau , Joseph M. Rokowski , Qi Wang
IPC分类号： C08J11/04
CPC分类号： C08J3/16 , C08F6/22 , C08J2300/30 , C08J2319/00 , C08J2321/00 , C08L19/003 , C08L33/12 , C08L101/02 , Y10T428/24355 , Y10T428/24364 , Y10T428/2438 , Y10T428/24405 , C08L2666/04
摘要： The present invention provides methods of making composite materials comprising combining particles of crosslinked rubber with coagulated aqueous polymer dispersions to form a mixture in aqueous dispersion, and subjecting the aqueous dispersion mixture to solid state shear pulverization to form materials that can be processed as thermoplastics at crosslinked rubber concentrations of from 10 to as high as 95 wt. %, based on the total solids of the material. The method may further comprise kneading the pulverized product to form useful articles, such as roofing membranes and shoe soles.
摘要翻译：本发明提供制备复合材料的方法，其包括将交联橡胶的颗粒与凝固的聚合物水分散体混合以在水分散体中形成混合物，并将水性分散体混合物进行固态剪切粉碎以形成可作为交联的热塑性塑料加工的材料橡胶浓度为10至高达95wt。％，基于材料的总固体。该方法还可以包括捏合粉碎产品以形成有用的制品，例如屋顶膜和鞋底。

46. 发明授权

US07416739B2 Composition and process for retaining active ingredients 有权
标题翻译：保留活性成分的组成和工艺
公开(公告)号：US07416739B2
公开(公告)日：2008-08-26
申请号：US10179776
申请日：2002-06-25
申请人： Steven M. Baxter , Willie Lau , Berislav Markovic , Mark E. Rerek , Curtis Schwartz , Thomas R. Tepe , Elliott Zucker
发明人： Steven M. Baxter , Willie Lau , Berislav Markovic , Mark E. Rerek , Curtis Schwartz , Thomas R. Tepe , Elliott Zucker
IPC分类号： A61K9/14
CPC分类号： A61K8/345 , A61K8/8152 , A61Q17/04
摘要： A composition for retaining active ingredients in personal care compositions is described based on one or more polymers having a network structure in an oil phase in amounts from 0.01 to 10% by weight based on the total weight of the composition in the oil phase, the polymers including at least one associative agent, the composition further including at least one active component. The oil phase viscosity of each composition is at least 10 poise under a shear stress up to 1000 dynes/cm2.
摘要翻译：基于一种或多种在油相中具有网状结构的聚合物，基于油相中组合物的总重量为0.01〜10重量％，聚合物中的聚合物包括至少一种缔合剂，所述组合物还包含至少一种活性组分。每种组合物的油相粘度在高达1000达因/厘米2的剪切应力下至少为10泊。

47. 发明申请

US20070128260A1 Aqueous polymer dispersions for stabilizing actives 审中-公开
标题翻译：用于稳定活性物质的聚合物水分散体
公开(公告)号：US20070128260A1
公开(公告)日：2007-06-07
申请号：US11605150
申请日：2006-11-28
申请人： Willie Lau , Miao-Hsun Sheng , Robert Solomon
发明人： Willie Lau , Miao-Hsun Sheng , Robert Solomon
IPC分类号： A61F13/02 , A61L15/16
CPC分类号： C08F220/18 , A61L15/44 , A61L17/005 , A61L24/0015 , A61L2300/00 , A61L2300/602 , C08F265/04 , C08J3/05 , C08L51/003 , C08L2666/02 , C09D133/08 , C09D151/003 , C09J151/003
摘要： An aqueous dispersion comprising: a) from 5 to 99.9% by weight, based on the weight of solids in the aqueous dispersion, of one or more polymers having a number average molecular weight less than 10,000; b) from 0.1 to 94.9% by weight, based on the weight of solids in the aqueous dispersion, of one or more active ingredients selected from the group consisting of water soluble active ingredients, partially water soluble active ingredients, water insoluble active ingredients and combinations thereof; and c) from 30% to 95% by weight of water.
摘要翻译：一种水性分散体，其包含：a）基于水分散体中固体重量的5至99.9重量％的数均分子量小于10,000的一种或多种聚合物; b）0.1至94.9重量％，基于水分散体中固体的重量，选自水溶性活性成分，部分水溶性活性成分，水不溶性活性成分和组合的一种或多种活性成分的; 和c）30重量％至95重量％的水。

48. 发明授权

US07001949B2 Aqueous dispersions of comb copolymers and coatings produced therefrom 有权
标题翻译：梳状共聚物及其制备的涂料的水分散体
公开(公告)号：US07001949B2
公开(公告)日：2006-02-21
申请号：US09951639
申请日：2001-09-13
申请人： David M. Fasano , Karl A. Bromm , Willie Lau , Jack C. Thibeault , David A. Larson , Paul R. Van Rheenen
发明人： David M. Fasano , Karl A. Bromm , Willie Lau , Jack C. Thibeault , David A. Larson , Paul R. Van Rheenen
IPC分类号： C08L51/00
CPC分类号： C09J133/10 , B32B27/08 , C08F257/02 , C08F265/04 , C08F265/06 , C08F290/00 , C08F290/04 , C08F290/046 , C08F290/06 , C08F290/061 , C08F291/00 , C08F293/005 , C08L23/0815 , C08L23/10 , C08L23/16 , C08L23/20 , C08L23/22 , C08L25/12 , C08L27/06 , C08L27/24 , C08L33/00 , C08L33/06 , C08L33/10 , C08L51/003 , C08L53/00 , C08L53/02 , C08L55/02 , C08L67/02 , C08L67/06 , C08L69/00 , C08L77/00 , C08L77/02 , C08L77/06 , C08L101/00 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09D151/003 , C09D153/00 , C09J133/00 , C09J151/003 , C09J2201/606 , Y10T428/31536 , Y10T428/3175 , Y10T428/31797 , Y10T428/31913 , Y10T428/31917 , Y10T428/3192 , Y10T428/31928 , Y10T428/31931 , Y10T428/31935 , C08L2666/24 , C08L2666/14 , C08L51/00
摘要： An aqueous coating composition comprising a comb copolymer is disclosed. A method of forming a coating from the aqueous coating composition, and a coating formed by that method are also disclosed, as is a method of forming the comb copolymer. The comb copolymer is characterized in that aqueous dispersions of the comb copolymer have a Hard/Soft Balance Advantage value of at least 25%. The aqueous coating composition is capable of producing coatings having an excellent balance of hard and soft properties.
摘要翻译：公开了一种包含梳状共聚物的水性涂料组合物。还公开了从水性涂料组合物形成涂料的方法和通过该方法形成的涂层，以及形成梳状共聚物的方法。梳状共聚物的特征在于梳状共聚物的水分散体具有至少25％的硬/软平衡优势值。水性涂料组合物能够生产具有优异的硬和软性能平衡的涂料。

49. 发明授权

US06864309B2 Method for preparing graft copolymers and compositions produced therefrom 有权
标题翻译：制备接枝共聚物的方法及由其制备的组合物
公开(公告)号：US06864309B2
公开(公告)日：2005-03-08
申请号：US10763790
申请日：2004-01-23
申请人： Willie Lau , Karl Allen Bromm , Paul Ralph Van Rheenen
发明人： Willie Lau , Karl Allen Bromm , Paul Ralph Van Rheenen
IPC分类号： C08J5/18 , B32B27/08 , C08F4/00 , C08F4/16 , C08F257/02 , C08F265/04 , C08F265/06 , C08F290/00 , C08F290/04 , C08F290/06 , C08F291/00 , C08F293/00 , C08J3/02 , C08K3/20 , C08L23/08 , C08L23/10 , C08L23/16 , C08L23/20 , C08L23/22 , C08L25/12 , C08L27/04 , C08L27/06 , C08L27/24 , C08L33/00 , C08L33/06 , C08L33/10 , C08L51/00 , C08L53/00 , C08L53/02 , C08L55/00 , C08L55/02 , C08L67/02 , C08L67/06 , C08L69/00 , C08L77/00 , C08L77/02 , C08L77/06 , C08L101/00 , C09D5/02 , C09D133/02 , C09D151/00 , C09D153/00 , C09D155/00 , C09D157/00 , C09J133/00 , C09J133/10 , C09J151/00
CPC分类号： C09J133/10 , B32B27/08 , C08F257/02 , C08F265/04 , C08F265/06 , C08F290/00 , C08F290/04 , C08F290/046 , C08F290/06 , C08F290/061 , C08F291/00 , C08F293/005 , C08L23/0815 , C08L23/10 , C08L23/16 , C08L23/20 , C08L23/22 , C08L25/12 , C08L27/06 , C08L27/24 , C08L33/00 , C08L33/06 , C08L33/10 , C08L51/003 , C08L53/00 , C08L53/02 , C08L55/02 , C08L67/02 , C08L67/06 , C08L69/00 , C08L77/00 , C08L77/02 , C08L77/06 , C08L101/00 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09D151/003 , C09D153/00 , C09J133/00 , C09J151/003 , C09J2201/606 , Y10T428/31536 , Y10T428/3175 , Y10T428/31797 , Y10T428/31913 , Y10T428/31917 , Y10T428/3192 , Y10T428/31928 , Y10T428/31931 , Y10T428/31935 , C08L2666/24 , C08L2666/14 , C08L51/00
摘要： An aqueous polymerization method for preparing graft copolymers is disclosed. Copolymer compositions produced therefrom are also disclosed. The method of the present invention includes (a) forming a macromonomer aqueous emulsion containing water insoluble macromonomer particles; (b) forming a monomer composition containing at least one ethylenically unsaturated monomer; and (c) combining at least a portion of the macromonomer aqueous emulsion and at least a portion of the monomer composition and polymerizing the resulting polymerization reaction mixture in the presence of an initiator to form a copolymer composition. The copolymer composition produced contains water insoluble particles of graft copolymer.
摘要翻译：公开了一种用于制备接枝共聚物的水性聚合方法。还公开了由其制备的共聚物组合物。本发明的方法包括（a）形成含有水不溶性大分子单体颗粒的大分子单体水乳液; （b）形成含有至少一种烯属不饱和单体的单体组合物; 和（c）将大分子单体水乳液和至少一部分单体组合物的至少一部分组合并在引发剂的存在下聚合所得聚合反应混合物以形成共聚物组合物。制备的共聚物组合物含有接枝共聚物的水不溶性颗粒。

50. 发明授权

US06809141B2 Segmental copolymers and aqueous dispersions and films therefrom 有权
标题翻译：分段共聚物和水分散体及其膜
公开(公告)号：US06809141B2
公开(公告)日：2004-10-26
申请号：US09951944
申请日：2001-09-13
申请人： David M. Fasano , Karl A. Bromm , Willie Lau , Jack C. Thibeault , David A. Larson , Paul R. Van Rheenen
发明人： David M. Fasano , Karl A. Bromm , Willie Lau , Jack C. Thibeault , David A. Larson , Paul R. Van Rheenen
IPC分类号： C08J302
CPC分类号： C09J133/10 , B32B27/08 , C08F257/02 , C08F265/04 , C08F265/06 , C08F290/00 , C08F290/04 , C08F290/046 , C08F290/06 , C08F290/061 , C08F291/00 , C08F293/005 , C08L23/0815 , C08L23/10 , C08L23/16 , C08L23/20 , C08L23/22 , C08L25/12 , C08L27/06 , C08L27/24 , C08L33/00 , C08L33/06 , C08L33/10 , C08L51/003 , C08L53/00 , C08L53/02 , C08L55/02 , C08L67/02 , C08L67/06 , C08L69/00 , C08L77/00 , C08L77/02 , C08L77/06 , C08L101/00 , C08L2314/06 , C08L2666/02 , C08L2666/04 , C09D151/003 , C09D153/00 , C09J133/00 , C09J151/003 , C09J2201/606 , Y10T428/31536 , Y10T428/3175 , Y10T428/31797 , Y10T428/31913 , Y10T428/31917 , Y10T428/3192 , Y10T428/31928 , Y10T428/31931 , Y10T428/31935 , C08L2666/24 , C08L2666/14 , C08L51/00
摘要： An aqueous dispersion of a segmental copolymer, wherein the aqueous dispersion has a Hard/Soft Balance Advantage value of at least 25% is disclosed. A method for preparing the aqueous dispersion of a segmental copolymer is also disclosed, as is a film produced thereby.
摘要翻译：公开了一种分段共聚物的水分散体，其中水分散体具有至少25％的硬/软平衡优势值。还公开了一种制备段共聚物的水分散体的方法，以及由此制备的膜。

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