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    • 47. 发明授权
    • Microwave heating device
    • 微波加热装置
    • US4760228A
    • 1988-07-26
    • US3846
    • 1987-01-16
    • Minoru Kudo
    • Minoru Kudo
    • B29C35/08B29C35/10B29C45/00B29C45/74B29C47/00B29C47/86B29C47/92H05B6/78H05B9/06
    • B29C47/92B29C35/10B29C45/74B29C47/86B29C47/862H05B6/788B29C2035/0855B29C2947/92514B29C2947/92704B29C2947/92895B29C45/00B29C47/00B29C47/0009
    • A microwave heating device for using microwave energy to heat a high polymer material or the like being conveyed under pressure comprises a hollow, cylindrical microwave waveguide closed at one end and having a metallic shell capable of withstanding high internal pressures, a pressure partition made from a dielectric material provided within said waveguide near an open end thereof so as to define a sealed space between itself and the closed end of said waveguide and to define a path for introduction of microwaves between itself and the open end of said waveguide, a solid or liquid dielectric packing material filling said sealed space and thereby forming a packed dielectric region, said packing material having a lower specific inductive capacity than that of the material to be heated, a passage for pressurized conveyance of the material to be heated, said passage running transversely through said waveguide at said packed dielectric region thereof, and a microwave generator for transmitting microwaves into said waveguide, the pressure within said passage is supported by said waveguide, said pressure partition and the closed end of said waveguide.
    • 用于使用微波能量加热在压力下输送的高聚物材料等的微波加热装置包括一个中空的圆柱形微波波导,其在一端封闭并具有能承受高内压的金属壳,由 电介质材料设置在所述波导内靠近其开口端,以便在其自身和所述波导的封闭端之间限定一个密封空间,并且限定用于在其与所述波导的开口端之间引入微波的路径,固体或液体 电介质填充材料填充所述密封空间,从而形成填充介质区域,所述包装材料具有比待加热材料低的比感应能力,用于被加热材料的加压输送的通道,所述通道横向穿过 所述波导在其所述堆叠的介电区域,以及用于透射的微波发生器 微波进入所述波导,所述通道内的压力由所述波导,所述压力分隔和所述波导的封闭端支撑。
    • 48. 发明授权
    • Melt-extrusion of polymer which is capable of forming an anisotropic
melt phase to form large shaped articles exhibiting improved polymeric
orientation
    • 能够形成各向异性熔融相的聚合物的熔融挤出以形成具有改进的聚合物取向的大型制品
    • US4734240A
    • 1988-03-29
    • US822091
    • 1986-01-24
    • Tai-Shung ChungSunil K. GargDaniel Palangio
    • Tai-Shung ChungSunil K. GargDaniel Palangio
    • B29C47/00B29C47/28B29C47/86B29C47/88
    • B29C47/28B29C47/0004B29C47/86B29C47/864B29C47/0014B29C47/0021B29C47/0026B29C47/003B29K2105/0079
    • An improved technique is provided to melt-extrude a liquid crystalline polymer to form large elongated solid shaped articles which exhibit significantly improved polymeric orientation. The molten polymer which is capable of forming an anisotropic melt phase is extruded through a converging die that is provided with at least one enclosed cooling zone at an interior location within the flowing molten polymer wherein a cooling fluid is circulated. This cools the molten polymer adjacent the cooling zone with the concomitant increase in its melt viscosity. Such increased melt viscosity at the interior of the stream of the molten polymer contributes to the uniformity of the polymeric orientation imparted within the converging die as well as during subsequent drawdown outside the extrusion orifice. Such improved polymeric orientation leads to the formation of an improved product (e.g., a three-dimensional rod) which exhibits an unusually high tensile modulus in the direction of its length. The present invention accordingly overcomes difficulties encountered in the prior art wherein melt-extruded shaped articles significantly larger than fibers heretofore often have exhibited substantial internal heterogeneity and a highly oriented skin and a core of a substantially lesser polymeric orientation.
    • 提供了一种改进的技术来熔融挤出液晶聚合物以形成显着改善的聚合物取向的大型细长固体成形制品。 能够形成各向异性熔融相的熔融聚合物通过在流动的熔融聚合物内的内部位置设置有冷却流体循环的至少一个封闭的冷却区的会聚模挤出。 这样使冷却区附近的熔融聚合物冷却,伴随着其熔体粘度的增加。 在熔融聚合物流内部的这种增加的熔体粘度有助于在会聚模具内以及随后在挤压孔外部的压下之间施加的聚合物取向的均匀性。 这种改进的聚合物取向导致形成在其长度方向表现出非常高的拉伸模量的改进的产品(例如,三维棒)。 因此,本发明克服了现有技术中遇到的困难,其中明显大于迄今为止的纤维的熔融挤出成型制品经常表现出显着的内部异质性和高度取向的皮肤和基本上较小的聚合物取向的芯。