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51. 发明授权

US07544847B1 Method for producing 1,4-bis (dichloromethyl) tetrafluorobenzene 有权
标题翻译： 1,4-二（二氯甲基）四氟苯的制备方法
公开(公告)号：US07544847B1
公开(公告)日：2009-06-09
申请号：US12285645
申请日：2008-10-10
申请人： Chan-Yuan Ho , Tsair-Feng Lin , Chun-Hsu Lin , Shieh-Jun Wang
发明人： Chan-Yuan Ho , Tsair-Feng Lin , Chun-Hsu Lin , Shieh-Jun Wang
IPC分类号： C07C17/00
CPC分类号： C07C17/38 , C07C17/18 , C07C17/392 , C07C25/13
摘要： A method for producing 1,4-bis(dichloromethyl)tetrafluorobenzene is disclosed, which is achieved by reacting tetrafluoroterephthaldehyde, SOCl2 and organic solvents. In the synthesis of 1,4-bis(dichloromethyl)-tetrafluorobenzene by adding formamides as catalyst, there are remarkable advantages which include shortening the reaction time; simplifying the synthesizing steps and raising the yield of the product.
摘要翻译：公开了生产1,4-双（二氯甲基）四氟苯的方法，其通过使四氟对苯二甲醛，SOCl 2和有机溶剂反应来实现。通过加入甲酰胺作为催化剂合成1,4-双（二氯甲基） - 四氟苯，有明显的优点，包括缩短反应时间; 简化合成步骤并提高产品的产率。

52. 发明授权

US07504547B2 Method of preparing perfluoroalkadiene 有权
标题翻译：制备全氟二烯的方法
公开(公告)号：US07504547B2
公开(公告)日：2009-03-17
申请号：US11797355
申请日：2007-05-02
申请人： Hae-Seok Ji , Ook-Jae Cho , Jae-Gug Ryu , Young-Hoon Ahn , Bong-Suk Kim , Dong-Hyun Kim
发明人： Hae-Seok Ji , Ook-Jae Cho , Jae-Gug Ryu , Young-Hoon Ahn , Bong-Suk Kim , Dong-Hyun Kim
IPC分类号： C07C17/00 , C07C21/18
CPC分类号： C07C17/23 , C07C21/19
摘要： Disclosed herein is a method of preparing a perfluoroalkadiene. A dihaloperfluorocarbon used as a starting material is added dropwise to a nonpolar organic solvent, a metal powder and an organic metal compound. The dihaloperfluorocarbon is slowly added dropwise in a temperature range from 30° C. to 150° C. for a certain period of time. Moreover, the nonpolar organic solvent used may be benzene, toluene, xylene, etc., and the organic metal compound is used by being dissolved in ethyl ether or tetrahydrofuran at a concentration of 1 to 3M. The metal powder used may be Mg, Zn, Cd, etc.
摘要翻译：本文公开了一种制备全氟二烯的方法。将用作起始原料的二卤碳氟化合物滴加到非极性有机溶剂，金属粉末和有机金属化合物中。在30℃至150℃的温度范围内缓慢滴加二卤氟碳化氢一段时间。此外，所用的非极性有机溶剂可以是苯，甲苯，二甲苯等，有机金属化合物以1〜3M的浓度溶解于乙醚或四氢呋喃中使用。使用的金属粉末可以是Mg，Zn，Cd等

53. 发明授权

US07482498B2 Device and process for nucleophilic fluorination 失效
标题翻译：用于亲核氟化的装置和方法
公开(公告)号：US07482498B2
公开(公告)日：2009-01-27
申请号：US10840429
申请日：2004-05-07
申请人： Peter Maeding , Frank Fuechtner
发明人： Peter Maeding , Frank Fuechtner
IPC分类号： C07C17/00 , G10K11/00 , G01L25/00 , B01L3/00
CPC分类号： C07B59/00 , A61K51/0459
摘要： The invention relates to a device and a process for nucleophilic fluorination of a substance, especially for synthesis of an 18F-labeled substance for examination using a positron emission tomograph. The device comprises an anion exchange device (102) for extraction of [18F]fluoride ions by means of adsorption from a target fluid, whereby the anion exchange device (102) can be charged via a supply device (101) with the target fluid; and a measurement device (104) with a measurement chamber (103) for measuring initial radioactivity of the [18F]fluoride ions, the anion exchange device (102) being arranged at least partially in the measurement chamber (103) of the measurement device (104).
摘要翻译：本发明涉及用于物质的亲核氟化的装置和方法，特别是用于合成用正电子发射断层扫描仪检查的18F标记物质。该装置包括用于通过来自目标流体的吸附提取[18 F]氟化物离子的阴离子交换装置（102），由此阴离子交换装置（102）可以通过供应装置（101）与目标流体进行充电; 以及具有用于测量[18 F]氟离子的初始放射性的测量室（103）的测量装置（104），阴离子交换装置（102）至少部分地布置在测量装置的测量室（103）中 104）。

54. 发明授权

US07468466B2 Process for producing hexafluoroethane and use thereof 有权
标题翻译：六氟乙烷的制造方法及其用途
公开(公告)号：US07468466B2
公开(公告)日：2008-12-23
申请号：US10567757
申请日：2004-08-09
申请人： Hiromoto Ohno , Tatsuharu Arai
发明人： Hiromoto Ohno , Tatsuharu Arai
IPC分类号： C07C17/00 , C07C17/28
CPC分类号： C07C19/08 , B01J23/26 , B01J37/0009 , C07C17/10 , C07C17/206 , C07C17/21 , C07C17/383 , C07C17/395 , C07C19/12
摘要： A process for producing hexafluoroethane, comprising a step of distilling a crude hexafluoroethane containing chlorine compounds each having two carbon atoms to distill out hexafluoroethane as a top flow from the top of a distillation column and separate a hexafluoroethane mixture containing the chlorine compounds as a bottom flow from the bottom, and a step of contacting the bottom flow with hydrogen fluoride in the gas phase at a temperature of 300 to 500° C. in the presence of a fluorination catalyst to fluorinate the chlorine compounds. This process provides hexafluoroethane which can be used mainly as a cleaning gas in the production process of a semiconductor device.
摘要翻译：一种生产六氟乙烷的方法，包括蒸馏含有两个碳原子的氯化合物的粗六氟乙烷从蒸馏塔的顶部馏出六氟乙烷作为顶部流动的步骤，并将含有氯化合物的六氟乙烷混合物作为底部流并且在氟化催化剂的存在下，在300〜500℃的温度下，在气相中将底部流与氟化氢接触以使氯化合物氟化的步骤。该方法提供了在半导体器件的生产过程中主要用作清洁气体的六氟乙烷。

55. 发明申请

US20080207963A1 Preparation of composition containing chromium, oxygen, and either silver or palladium, and their use as catalysts and catalyst precursors 审中-公开
标题翻译：含有铬，氧和银或钯的组合物的制备及其作为催化剂和催化剂前体的用途
公开(公告)号：US20080207963A1
公开(公告)日：2008-08-28
申请号：US12070921
申请日：2008-02-21
申请人： Velliyur Nott Mallikarjuna Rao , Allen Capron Sievert
发明人： Velliyur Nott Mallikarjuna Rao , Allen Capron Sievert
IPC分类号： C07C17/02 , B01J23/26 , C07C17/23 , C07C17/00
CPC分类号： C07C19/08 , B01J23/6522 , B01J23/685 , B01J37/03 , B01J37/14 , B01J37/26 , C07C17/04 , C07C17/206 , C07C17/21 , C07C17/23 , C07C17/25 , C07C21/18 , C07C19/10
摘要： A method for preparing a catalyst composition suitable for increasing the fluorine content in a hydrocarbon or a halogenated hydrocarbon is disclosed. The method involves (a) co-precipitating a solid by adding ammonium hydroxide to an aqueous solution of a soluble trivalent chromium salt and a soluble salt of a modifier metal selected from silver and palladium, that contains at least three moles of nitrate (i.e., NO3−) per mole of chromium (i.e., Cr+3) in the solution and has a modifier metal concentration of from about 0.05 atom % to about 10 atom % of the total concentration of modifier metal and chromium in the solution to form an aqueous mixture containing co-precipitated solid and dissolved ammonium nitrate; and after at least three moles of ammonium hydroxide per mole of chromium in the solution has been added to the solution, (b) drying said aqueous mixture formed in (a); and (c) calcining the dried solid formed in (b) in an atmosphere containing at least 10% oxygen by volume (e.g., air). Also disclosed is a catalyst composition comprising alpha-chromium oxide and a modifier metal selected from silver and palladium prepared by the above method. Also disclosed is a process for increasing the fluorine content in a hydrocarbon or halogenated hydrocarbon in the presence of a catalyst; and processes using a catalyst composition comprising chromium, oxygen and a modifier metal selected from siver and palladium as essential constituent elements (e.g., a catalyst composition prepared by the above process). An azeotropic composition involving CF3CCl═CF2 and HF is also disclosed.
摘要翻译：公开了一种制备适于增加烃或卤代烃中的氟含量的催化剂组合物的方法。该方法包括（a）通过向可溶性三价铬盐和选自银和钯的改性金属的可溶性盐的水溶液中加入氢氧化铵共沉淀固体，所述改性金属含有至少三摩尔硝酸盐（即，在溶液中每摩尔铬（即，Cr + 3 +），具有约0.05原子的改性剂金属浓度在溶液中的改性剂金属和铬的总浓度的约10原子％至约10原子％，以形成含有共沉淀固体和溶解的硝酸铵的含水混合物; 并且在溶液中每摩尔铬至少三摩尔氢氧化铵已加入到溶液中之后，（b）干燥（a）中形成的所述含水混合物; 和（c）在（b）中形成的干燥固体在含有至少10体积％氧（例如空气）的气氛中煅烧。还公开了包含α-氧化铬和通过上述方法制备的选自银和钯的改性金属的催化剂组合物。还公开了一种在催化剂存在下增加烃或卤代烃中的氟含量的方法; 以及使用包含铬，氧和选自硫化银和钯的改性剂的催化剂组合物作为必需组成元素（例如通过上述方法制备的催化剂组合物）的方法。还公开了包含CF 3 CCl-CF 2 H 2和HF的共沸组合物。

56. 发明申请

US20080149472A1 Photochlorination and Fluorination Process for Preparation of Fluorine-Containing Hydrocarbons 审中-公开
标题翻译：用于制备含氟碳氢化合物的光氯化和氟化方法
公开(公告)号：US20080149472A1
公开(公告)日：2008-06-26
申请号：US11792643
申请日：2005-12-19
申请人： Velliyur Nott Mallikarjuna Rao , Allen Capron Sievert
发明人： Velliyur Nott Mallikarjuna Rao , Allen Capron Sievert
IPC分类号： C07C17/00
CPC分类号： C07C19/08 , C07C17/10 , C07C17/206 , C07C19/10 , C07C19/12
摘要： A process is disclosed for increasing the fluorine content of at least one compound selected from halohydrocarbons and hydrocarbons. The process involves (a) directing light from a light source through the wall of a reactor to interact with reactants comprising chlorine and said at least one compound in said reactor, thereby producing a halogenated hydrocarbon having increased chlorine content by photochlorination, and (b) reacting said halogenated hydrocarbon produced by the photochlorination in (a) with HF; and is characterized by the light directed through the reactor wall being directed through a poly(perhaloolefin) polymer.
摘要翻译：公开了用于增加选自卤代烃和烃的至少一种化合物的氟含量的方法。该方法包括（a）将来自光源的光引导通过反应器的壁与所述反应器中包含氯和所述至少一种化合物的反应物相互作用，从而通过光氯化产生具有增加的氯含量的卤代烃，和（b）使（a）中的光氯化生产的卤代烃与HF反应; 并且其特征在于穿过反应器壁的光被引导通过聚（全卤代烯烃）聚合物。

57. 发明授权

US07388117B2 Azeotrope compositions comprising 1,2,3,3,3-pentafluoropropene and hydrogen fluoride and uses thereof 有权
标题翻译：包含1,2,3,3,3-五氟丙烯和氟化氢的共沸组合物及其用途
公开(公告)号：US07388117B2
公开(公告)日：2008-06-17
申请号：US11590448
申请日：2006-10-30
申请人： Ralph Newton Miller , Barbara Haviland Minor , Mario Joseph Nappa , Velliyur Nott Mallikarjuna Rao , Allen Capron Sievert
发明人： Ralph Newton Miller , Barbara Haviland Minor , Mario Joseph Nappa , Velliyur Nott Mallikarjuna Rao , Allen Capron Sievert
IPC分类号： C07C17/00 , C07C17/38
CPC分类号： C07C21/18 , C01B7/196 , C07C17/25 , C07C17/38 , C07C17/383
摘要： Disclosed herein are azeotrope compositions comprising 1,2,3,3,3-pentafluoropropene and hydrogen fluoride. The azeotrope compositions are useful in processes to produce and in processes to purify 1,2,3,3,3-pentafluoropropene.
摘要翻译：本文公开了包含1,2,3,3,3-五氟丙烯和氟化氢的共沸组合物。共沸组合物可用于生产和纯化1,2,3,3,3-五氟丙烯的方法。

58. 发明申请

US20080045758A1 Halocarbon production processes, halocarbon separation processes, and halocarbon separation systems 审中-公开
标题翻译：卤代烃生产工艺，卤代烃分离工艺和卤代烃分离系统
公开(公告)号：US20080045758A1
公开(公告)日：2008-02-21
申请号：US11977357
申请日：2007-10-24
申请人： Mitchel Cohn , John Chien
发明人： Mitchel Cohn , John Chien
IPC分类号： C07C17/383 , C07C17/00
CPC分类号： B01J19/2465 , B01J8/025 , B01J8/06 , B01J19/02 , B01J2219/00006 , B01J2219/0245 , B01J2219/0286 , C07C17/00 , C07C17/206 , C07C17/21 , C07C17/25 , C07C17/275 , C07C17/278 , C07C17/38 , C07C17/383 , C07C17/386 , C07C17/395 , C07C19/08 , C07C21/04 , C07C19/01 , C07C21/18
摘要： Halocarbon production processes are provided that can include reacting at least one C-2 halocarbon with at least one C-1 halocarbon in the presence of a phosphate to produce at least one C-3 chlorocarbon. The processes can include reacting ethylene with carbon tetrachloride in the presence of a phosphate. Halocarbon separation processes are provided that can include providing a reaction product that includes at least one saturated fluorocarbon and at least one unsaturated fluorocarbon and adding at least one hydrohalogen to produce a distillation mixture. Methods and materials are provided for the production and purification of halogenated compounds and intermediates in the production of 1,1,1,3,3-pentafluoropropane.
摘要翻译：提供卤代烃生产方法，其可以包括在磷酸盐存在下使至少一种C-2卤代烃与至少一种C-1卤代烃反应以产生至少一种C-3氯化碳。该方法可包括在磷酸盐存在下使乙烯与四氯化碳反应。提供了卤代烃分离方法，其可以包括提供包含至少一种饱和碳氟化合物和至少一种不饱和氟碳化合物的反应产物，并加入至少一种氢卤素以产生蒸馏混合物。提供了生产和提纯卤代化合物和中间产物1,1,1,3,3-五氟丙烷的方法和材料。

59. 发明申请

US20080012475A1 Pyrene Based Compound, And Light Emitting Transistor Element And Electroluminescence Element Using The Same 审中-公开
标题翻译：芘基化合物和发光晶体管元件和使用它的电致发光元件
公开(公告)号：US20080012475A1
公开(公告)日：2008-01-17
申请号：US11791613
申请日：2005-11-25
申请人： Takahito Oyamada , Hiroyuki Uchiuzou , Chihaya Adachi , Seiji Akiyama , Takayoshi Takahashi
发明人： Takahito Oyamada , Hiroyuki Uchiuzou , Chihaya Adachi , Seiji Akiyama , Takayoshi Takahashi
IPC分类号： C07C13/66 , C07C15/38 , C07C17/00 , C07C25/22 , C07D401/04 , C07D401/14 , C07F5/02 , H01J1/62 , H01L51/54
CPC分类号： C09K11/06 , C07C13/567 , C07C15/38 , C07C15/62 , C07C17/12 , C07C25/22 , C07C43/21 , C07C2603/18 , C07C2603/24 , C07C2603/50 , C07D209/86 , C07D213/06 , C07D213/16 , C07D213/53 , C07D277/22 , C07D333/18 , C07D333/54 , C07D409/10 , C09K2211/1007 , C09K2211/1011 , C09K2211/1029 , H01L51/0054 , H01L51/0058 , H01L51/0067 , H01L51/0068 , H01L51/0074 , H01L51/5012 , H01L51/5048
摘要： It is an object to provide an organic fluorescent substance which can be used in a light emitting transistor element and an organic EL element. The invention provides a light emitting transistor element or an organic electroluminescence element wherein a specific asymmetric pyrene based compound is used in a light emitting layer in the light emitting transistor element, or in a light emitting layer, a hole transporting layer or an electron transporting layer in the organic EL element.
摘要翻译：本发明的目的是提供可用于发光晶体管元件和有机EL元件的有机荧光物质。本发明提供一种发光晶体管元件或有机电致发光元件，其中在发光晶体管元件中的发光层中或在发光层，空穴传输层或电子传输层中使用特定的不对称芘基化合物在有机EL元件中。

60. 发明授权

US07259281B2 Fluorobutene derivatives and process for producing same 失效
标题翻译：氟丁烯衍生物及其制备方法
公开(公告)号：US07259281B2
公开(公告)日：2007-08-21
申请号：US11506963
申请日：2006-08-21
申请人： Richard A. Du Boisson , Adam C. Alty
发明人： Richard A. Du Boisson , Adam C. Alty
IPC分类号： C07C17/00
CPC分类号： C07C17/25 , C07C21/18 , C07C21/20 , Y02P20/584
摘要： The present invention provides novel compounds 2,4,4,4-tetrafluoro-1-butene and (E)- and (Z)-1,1,1,3-tetrafluoro-2-butenes. Furthermore, the present invention provides the following novel first and second processes for producing 2,4,4,4-tetrafluoro-1-butene and (E)- and (Z)-1,1,1,3-tetrafluoro-2-butenes. The first process is a process for producing 2,4,4,4-tetrafluoro-1-butene by heating 1,1,1,3,3-pentafluorobutane at from about 200° C. to about 700° C. The second process is a process for producing (E)- and (Z)-1,1,1,3-tetrafluoro-2-butenes by bringing 1,1,1,3,3-pentafluorobutane with a base. By the first and second processes, it is possible to obtain respective target fluorobutenes with high selectivity.
摘要翻译：本发明提供新的化合物2,4,4,4-四氟-1-丁烯和（E） - 和（Z）-1,1,1,3-四氟-2-丁烯。此外，本发明提供了以下制备2,4,4,4-四氟-1-丁烯和（E） - 和（Z）-1,1,1,3-四氟-2-丁烯的新颖的第一和第二方法，丁烯第一种方法是通过在约200℃至约700℃下加热1,1,1,3,3-五氟丁烷来制备2,4,4,4-四氟-1-丁烯的方法。第二种方法是通过使1,1,1,3,3-五氟丁烷与碱形成（E） - 和（Z）-1,1,1,3-四氟-2-丁烯的方法。通过第一和第二方法，可以以高选择性获得各自的目标氟代丁烯。

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