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61. 发明授权

US5545778A Single stage process for producing hydrofluorocarbons from perchloroethylene 失效
标题翻译：从全氯乙烯生产氢氟烃的单阶段工艺
公开(公告)号：US5545778A
公开(公告)日：1996-08-13
申请号：US248981
申请日：1994-05-25
申请人： Hsueh S. Tung , Addison M. Smith , Charles F. Swain
发明人： Hsueh S. Tung , Addison M. Smith , Charles F. Swain
IPC分类号： C07C17/087 , C07B61/00 , C07C17/21 , C07C17/35 , C07C17/38 , C07C17/383 , C07C19/08 , C07C19/12 , C07C17/08
CPC分类号： C07C17/21 , C07C17/383
摘要： A process for the preparation of one or more of CHClFCF.sub.3 (HCFC-124), CHF.sub.2 CClF.sub.2 (HCFC-124a) and CHF.sub.2 CF.sub.3 (HFC-125) by reaction of perchloroethylene with hydrogen fluoride in a single stage reaction vessel in the presence of a fluorination catalyst. These compounds are useful in a variety of industrial applications including blowing agents, refrigerants, sterilant gases and solvent applications. Distilling the reaction product produces a distillate comprising HCl, CHClFCF.sub.3, CHF.sub.2 CClF.sub.2 and CHF.sub.2 CF.sub.3 and a minor amount of HF which distillate is scrubbed to remove the acids. The bottoms product comprises perchloroethylene, hydrogen fluoride and organic by-products which is phase separated to sequester the hydrogen fluoride from the mixture of perchloroethylene and organic by-products. The hydrogen fluoride and mixture of perchloroethylene with organic by-products are then preferably re-mixed at a controlled rate and recycled to the reaction vessel.
摘要翻译：在氟化催化剂存在下，在单级反应容器中通过全氯乙烯与氟化氢的反应制备CHClFCF3（HCFC-124），CHF2CClF2（HCFC-124a）和CHF2CF3（HFC-125）中的一种或多种的方法。这些化合物可用于各种工业应用，包括发泡剂，制冷剂，灭菌气体和溶剂应用。蒸馏反应产物产生包含HCl，CHClFCF 3，CHF 2 CClF 2和CHF 2 CF 3的馏出物和少量HF，该馏出物被洗涤以除去酸。底部产物包括全氯乙烯，氟化氢和有机副产物，其相分离以从全氯乙烯和有机副产物的混合物中隔离氟化氢。然后将氟化氢和全氯乙烯与有机副产物的混合物优选以受控的速率重新混合并再循环至反应容器。

62. 发明授权

US4937398A Process for the preparation of fluorinated alkanes from alkenes 失效
标题翻译：从烯烃制备氟化烷烃的方法
公开(公告)号：US4937398A
公开(公告)日：1990-06-26
申请号：US290129
申请日：1988-12-27
申请人： Hsueh S. Tung , Richard E. Eibeck , Bernard Sukornick
发明人： Hsueh S. Tung , Richard E. Eibeck , Bernard Sukornick
IPC分类号： C07C17/02 , C07C17/04 , C07C19/08
CPC分类号： C07C17/02 , C07C17/04
摘要： The present invention provides a process for the preparation of luorinated alkanes. The process comprises the step of: reacting an alkene with carbon having fluorine absorbed therein at a temperature and for a time sufficient to form fluorinated alkanes. The alkene used is not perhalogenated at the double-bonded carbons. Preferably, the alkene used is vinylidene fluoride or ethylene.The process produces products such as 1,1,1,2-tetrafluoroethane (known in the art as 134a) which may be used as a refrigerant and 1,1,1-trifluoroethane (known in the art as R143a) and 1,2-difluoroethane (known in the art as R152) which may be used as blowing agents or solvents.
摘要翻译：本发明提供了一种制备罗氏化烷烃的方法。该方法包括以下步骤：在足以形成氟化烷烃的温度和时间下使烯烃与其中吸收有氟的碳反应。所用的烯烃在双键碳上不是全卤代的。优选使用的烯烃是偏二氟乙烯或乙烯。该方法产生可用作制冷剂的1,1,1,2-四氟乙烷（本领域已知的134a）和1,1,1-三氟乙烷（本领域已知的R143a）和1,2 二氟乙烷（本领域已知为R152），其可用作发泡剂或溶剂。

63. 发明授权

US4737423A Cathode active material for metal of CFX battery 失效
标题翻译： CFX电池金属阴极活性材料
公开(公告)号：US4737423A
公开(公告)日：1988-04-12
申请号：US932984
申请日：1986-11-20
申请人： Hsueh S. Tung
发明人： Hsueh S. Tung
IPC分类号： C01B31/00 , H01M4/58 , H01M4/583 , H01M4/36 , H01M10/40
CPC分类号： H01M4/583 , C01B31/005 , H01M4/5835
摘要： Improved fluorinated carbon made from an amorphous carbon or heat treated amorphous carbon having a lattice constant (d.sub.002) of 3.37A or greater for use as a positive electrode of a battery is provided. Such improved fluorinated carbon has low free oxidizing power, high utility factor and high capacity upon discharge in a Li/CF.sub.x battery. The free oxidizing power is found to be dependent on reaction temperature; the higher the fluorination temperature the lower the free oxidizing power. Low free oxidizing power is obtained at reaction temperatures of at least 460.degree. C. Residual free oxidizing power can be further reduced by washing with an alkanol. Such alkanol wash can also be used to reduce free oxidizing power in fluorinated carbons prepared at lower temperatures.
摘要翻译：提供由非晶碳制成的改进的氟化碳或具有3.37A或更大的晶格常数（d002）为3.37A或更大的热处理非晶碳用作电池的正极。这种改进的氟化碳在Li / CFx电池中放电时具有低的游离氧化能力，高效用因子和高容量。发现游离氧化力取决于反应温度; 氟化温度越高，游离氧化能力越低。在至少460℃的反应温度下获得低的游离氧化能力。通过用烷醇洗涤可以进一步降低残留的游离氧化能力。这种链烷醇洗涤也可用于降低在较低温度下制备的氟化碳中的游离氧化能力。

64. 发明授权

US08075797B2 Azeotrope-like compositions of pentafluoropropane, chlorotrifluoropropene, and hydrogen fluoride 有权
标题翻译：五氟丙烷，三氟氟丙烯和氟化氢的类共沸组合物
公开(公告)号：US08075797B2
公开(公告)日：2011-12-13
申请号：US12693208
申请日：2010-01-25
申请人： Ryan Hulse , Rajiv R. Singh , Hsueh S. Tung , Ian Shankland
发明人： Ryan Hulse , Rajiv R. Singh , Hsueh S. Tung , Ian Shankland
IPC分类号： C09K5/00 , C09K5/04 , C07C17/00 , C07C19/08 , C07C21/18 , C07C23/00 , C07C25/13 , C11D7/50 , C11D17/00 , C11D17/08
CPC分类号： C07C19/08 , C07C17/206 , C07C17/25 , C07C17/383 , C07C21/18
摘要： The invention is directed to a ternary azeotrope-like mixture consisting essentially of effective amounts of 1,1,1,3,3-pentafluoropropane, 1-chloro-3,3,3-trifluoropropene, and hydrogen fluoride.
摘要翻译：本发明涉及基本上由有效量的1,1,1,3,3-五氟丙烷，1-氯-3,3,3-三氟丙烯和氟化氢组成的三元共沸混合物。

65. 发明申请

US20100022809A1 Manufacturing Process for HFO-1234ze 有权
标题翻译： HFO-1234ze的制造工艺
公开(公告)号：US20100022809A1
公开(公告)日：2010-01-28
申请号：US12125045
申请日：2008-05-21
申请人： Stephen A. Cottrell , Hsueh S. Tung , Haiyou Wang
发明人： Stephen A. Cottrell , Hsueh S. Tung , Haiyou Wang
IPC分类号： C07C17/00
CPC分类号： C07C17/25 , C07C17/358 , C07C21/18
摘要： Disclosed is a method for forming HFO-1234ze, and for forming compositions comprising HFO-1234ze, by (a) converting, preferably by dehydrofluorination, pentafluorpropane (HFC-245), preferably 1,1,1,3,3-pentafluorpropane (HFC-245fa), preferably by contact with a caustic solution, to a reaction product comprising cis-HFO-1234ze and trans-HFO-1234ze; and (b) contacting at least a portion, preferably substantially portion, and in certain embodiments substantially all of said reaction product with at least one isomerization catalyst to convert at least a portion, and preferably at least a substantial portion, of cis-HFO-1234ze in said reaction product to trans-HFO-1234ze.
摘要翻译：公开了形成HFO-1234ze的方法，以及用于形成包含HFO-1234ze的组合物的方法，通过（a）优选通过脱氟化氢转化五氟丙烷（HFC-245），优选1,1,1,3,3-五氟丙烷（HFC -245fa），优选通过与苛性碱溶液接触，加入到包含顺-HFO-1234ze和反-HFO-1234ze的反应产物中; 并且（b）使至少一部分，优选基本上部分，在某些实施方案中使基本上所有的所述反应产物与至少一种异构化催化剂接触，以将至少一部分，优选至少大部分的顺-HFO- 1234ze在所述反应产物中以反式HFO-1234ze。

66. 发明授权

US06235950B1 Method of making hydrofluorocarbons 失效
标题翻译：制备氢氟烃的方法
公开(公告)号：US06235950B1
公开(公告)日：2001-05-22
申请号：US09470231
申请日：1999-12-22
申请人： Hsueh S. Tung , Robert S. Wedinger
发明人： Hsueh S. Tung , Robert S. Wedinger
IPC分类号： C07C1908
CPC分类号： C07C17/16 , C07C19/08 , C07C29/145 , C07C45/63 , C07C49/167 , C07C49/16 , C07C31/38
摘要： A method of producing hydrofluorocarbons and methods of producing other commercially attractive compounds formed as by-products of hydrofluorocarbon production by using ketones as a principal reactant.
摘要翻译：一种生产氢氟烃的方法，以及通过使用酮作为主要反应物，生产作为氢氟烃生产副产物的其它商业上有吸引力的化合物的方法。

67. 发明授权

US4681823A Lithium/fluorinated carbon battery with no voltage delay 失效
标题翻译：无电压延迟的锂/氟化碳电池
公开(公告)号：US4681823A
公开(公告)日：1987-07-21
申请号：US864242
申请日：1986-05-19
申请人： Hsueh S. Tung , David J. Friedland , Bernard Sukornick , Lynn E. McCurry , Richard E. Eibeck , George D. Lockyer
发明人： Hsueh S. Tung , David J. Friedland , Bernard Sukornick , Lynn E. McCurry , Richard E. Eibeck , George D. Lockyer
IPC分类号： C01B31/00 , H01M4/08 , H01M4/58 , H01M4/36 , H01M6/16
CPC分类号： H01M4/5835 , C01B31/005 , Y02P70/54
摘要： A process is disclosed for producing fluorinated carbon (CF.sub.x) admixed which can be used in a lithium battery to eliminate low voltage at the beginning of discharge. The process uses a thick carbon bed to assure proper degree and type of underfluorination of the CF.sub.x. The inhomogeneous fluorinated carbon produced is a fully, or overfluorinated CF.sub.x with a small amount of underfluorinated material to eliminate voltage suppression in Li/CF.sub.x batteries.

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