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1. 发明授权

US08609767B2 Thermosetting resins with gelled nanometer-sized rubber particles 有权
标题翻译：具有凝胶状纳米尺寸橡胶颗粒的热固性树脂
公开(公告)号：US08609767B2
公开(公告)日：2013-12-17
申请号：US10266976
申请日：2002-10-08
申请人： Fan Huang , Jinliang Qiao , Yiqun Liu , Xiaohong Zhang , Jianming Gao , Zhihai Song
发明人： Fan Huang , Jinliang Qiao , Yiqun Liu , Xiaohong Zhang , Jianming Gao , Zhihai Song
IPC分类号： C08L61/10 , C08L61/20 , C08L67/06 , C08L83/04
CPC分类号： C08L63/00 , C08G77/04 , C08L19/003 , C08L61/06 , C08L67/06 , C08L83/04 , C08L2666/08 , C08L2666/04
摘要： Toughened thermosetting resins comprising thermosetting resins and rubber particles having an average particle size in the range of 20 to 500nm. The toughened resins are obtained by mixing a fully vulcanized powdery rubber having an average particle size in the range of 20 to 500nm with thermosetting resin prepolymers and then curing them. The toughened thermosetting resins comprise rubber phases having a small, uniform and stable particle size, which results in a very significant toughening effect, especially when crazes rapidly grow (as in a standard Izod impact test). The toughened thermosetting resins are excellent in impact resistance, strength, modulus and heat resistance, and when appropriately toughened, the thermosetting resins can be enhanced in terms of impact strength, glass transition temperature and heat distortion temperature. The toughened thermosetting resins are useful for many application areas and the method for preparing the same can be carried out in a simple and easy manner and is suitable for toughening various thermosetting resins.
摘要翻译：包含热固性树脂和平均粒径在20至500nm范围内的橡胶颗粒的增韧的热固性树脂。增韧树脂通过将平均粒度在20-500nm范围内的完全硫化的粉末橡胶与热固性树脂预聚物混合，然后固化而得到。增韧的热固性树脂包括具有小的，均匀和稳定的粒度的橡胶相，这导致非常显着的增韧效果，特别是当快速生长时（如在标准艾佐德冲击试验中）。增韧的热固性树脂的耐冲击性，强度，模量和耐热性优异，并且在适当增韧时，可以在冲击强度，玻璃化转变温度和热变形温度方面提高热固性树脂。增韧的热固性树脂可用于许多应用领域，并且其制备方法可以简单和容易地进行，并且适合于增韧各种热固性树脂。

2. 发明授权

US09200149B2 Modified rubber masterbatch, and rubber composition and vulcanized rubber produced therefrom, and the preparation processes for them 有权
公开(公告)号：US09200149B2
公开(公告)日：2015-12-01
申请号：US14354233
申请日：2012-10-26
申请人： Jinliang Qiao , Yuexin Cong , Xiaohong Zhang , Ying Li , Jianming Gao , Qianmin Zhang , Zhihai Song , Yanling Sun , Jinmei Lai , Peijun Song , Chuanlun Cai , Guoxun Zhao , Hongbin Zhang , Guicun Qi , Ya Wang , Binghai Li
发明人： Jinliang Qiao , Yuexin Cong , Xiaohong Zhang , Ying Li , Jianming Gao , Qianmin Zhang , Zhihai Song , Yanling Sun , Jinmei Lai , Peijun Song , Chuanlun Cai , Guoxun Zhao , Hongbin Zhang , Guicun Qi , Ya Wang , Binghai Li
IPC分类号： C08L21/00 , C08L9/02 , C08L7/00 , C08L9/00 , C08L9/06 , C08F20/44 , B60C1/00
摘要： The present application relates to a modified rubber masterbatch and preparation method thereof, rubber composition prepared therewith and vulcanized rubber and preparation method thereof. The modified rubber component comprises uncrosslinked rubber and rubber particles having crosslinked structure dispersed therein, wherein the rubber particles having crosslinked structure are synthetic rubber particles and/or natural rubber particles, have an average particle size of 20-500 nm and a gel content of 60% by weight or higher, and wherein the uncrosslinked rubber is styrene-butadiene rubber. The weight ratio of the rubber particles having crosslinked structure to the uncrosslinked rubber is greater than 20:80 and less than or equal to 80:20. The rubber composition comprises a blend of modified rubber component and base rubber, in which the modified rubber masterbatch is present in an amount of 1 to 70 parts by weight, relative to per 100 parts by weight of the base rubber. The vulcanized rubber of the rubber composition has not only low rolling resistance and excellent wet skid resistance, but also excellent wear resistance, and thus can be used for producing high performance tread rubber.

3. 发明授权

US08957135B2 Composite powder, preparation and use thereof 有权
标题翻译：复合粉末及其制备及应用
公开(公告)号：US08957135B2
公开(公告)日：2015-02-17
申请号：US13731895
申请日：2012-12-31
申请人： Yiqun Liu , Jinliang Qiao , Xiaohong Zhang , Fan Huang , Jianming Gao , Banghui Tan , Genshuan Wei , Zhihai Song , Zhida Chen
发明人： Yiqun Liu , Jinliang Qiao , Xiaohong Zhang , Fan Huang , Jianming Gao , Banghui Tan , Genshuan Wei , Zhihai Song , Zhida Chen
IPC分类号： C08J3/215 , C08K3/26 , C08J3/12 , C08J3/20 , C08K3/00 , C08K3/08 , C08K3/22 , C08K3/34 , C08K3/36
CPC分类号： C08K3/26 , C08J3/122 , C08J3/20 , C08J2309/00 , C08J2321/00 , C08K3/013 , C08K3/08 , C08K3/22 , C08K3/346 , C08K3/36 , Y10T428/2982 , Y10T428/2998 , Y10T428/31707 , C08K3/0033 , C08L21/00
摘要： The present invention relates to a composite powder, preparation and use thereof. The composite powder according to the present invention is prepared by intimately mixing an irradiated or non-irradiated rubber latex with a slurry of inorganic particles in a ratio corresponding to that of rubber particles to inorganic particles in the composite powder according to the present invention, and then drying the resultant mixture. The composite powder according to the present invention comprises agglomerates composed of powdery rubber particles and inorganic particles, with inorganic particles being uniformly distributed either inside the agglomerats or both inside the agglomerates and on the surfaces thereof. The composite powder according to the present invention can be easily dispersed in plastic matrixes and thus can be compounded with plastics to produce toughened plastics and thermoplastic elastomers.
摘要翻译：本发明涉及一种复合粉末，其制备和用途。根据本发明的复合粉末是通过将照射的或未经照射的橡胶胶乳与根据本发明的复合粉末中的无机颗粒的比例将无机颗粒的浆料与橡胶颗粒的浆料相当的比例与无机颗粒紧密混合而制备的，然后干燥所得混合物。根据本发明的复合粉末包括由粉末状橡胶颗粒和无机颗粒组成的附聚物，其中无机颗粒均匀地分布在凝聚体内部或两者在凝聚体内部及其表面上。根据本发明的复合粉末可以容易地分散在塑料基体中，因此可以与塑料混合以生产增韧的塑料和热塑性弹性体。

4. 发明申请

US20130225713A1 COMPOSITE POWDER, PREPARATION AND USE THEREOF 有权
标题翻译：复合粉末，其制备和使用
公开(公告)号：US20130225713A1
公开(公告)日：2013-08-29
申请号：US13731895
申请日：2012-12-31
申请人： Yiqun Liu , Jinliang Qiao , Xiaohong Zhang , Fan Huang , Jianming Gao , Banghui Tan , Genshuan Wei , Zhihai Song , Zhida Chen
发明人： Yiqun Liu , Jinliang Qiao , Xiaohong Zhang , Fan Huang , Jianming Gao , Banghui Tan , Genshuan Wei , Zhihai Song , Zhida Chen
IPC分类号： C08K3/26 , C08K3/08 , C08K3/22 , C08K3/34 , C08K3/36
CPC分类号： C08K3/26 , C08J3/122 , C08J3/20 , C08J2309/00 , C08J2321/00 , C08K3/013 , C08K3/08 , C08K3/22 , C08K3/346 , C08K3/36 , Y10T428/2982 , Y10T428/2998 , Y10T428/31707 , C08K3/0033 , C08L21/00
摘要： The present invention relates to a composite powder, preparation and use thereof. The composite powder according to the present invention is prepared by intimately mixing an irradiated or non-irradiated rubber latex with a slurry of inorganic particles in a ratio corresponding to that of rubber particles to inorganic particles in the composite powder according to the present invention, and then drying the resultant mixture. The composite powder according to the present invention comprises agglomerates composed of powdery rubber particles and inorganic particles, with inorganic particles being uniformly distributed either inside the agglomerats or both inside the agglomerates and on the surfaces thereof. The composite powder according to the present invention can be easily dispersed in plastic matrixes and thus can be compounded with plastics to produce toughened plastics and thermoplastic elastomers.
摘要翻译：本发明涉及一种复合粉末，其制备和用途。根据本发明的复合粉末是通过将照射的或未经照射的橡胶胶乳与根据本发明的复合粉末中的无机颗粒的比例将无机颗粒的浆料与橡胶颗粒的浆料相当的比例与无机颗粒紧密混合而制备的，然后干燥所得混合物。根据本发明的复合粉末包括由粉末状橡胶颗粒和无机颗粒组成的附聚物，其中无机颗粒均匀地分布在凝聚体内部或两者在凝聚体内部及其表面上。根据本发明的复合粉末可以容易地分散在塑料基体中，因此可以与塑料混合以生产增韧的塑料和热塑性弹性体。

5. 发明授权

US08362128B2 Composite powder, preparation and use thereof 有权
公开(公告)号：US08362128B2
公开(公告)日：2013-01-29
申请号：US10818950
申请日：2004-04-05
申请人： Yiqun Liu , Jinliang Qiao , Xiaohong Zhang , Fan Huang , Jianming Gao , Banghui Tan , Genshuan Wei , Zhihai Song , Zhida Chen
发明人： Yiqun Liu , Jinliang Qiao , Xiaohong Zhang , Fan Huang , Jianming Gao , Banghui Tan , Genshuan Wei , Zhihai Song , Zhida Chen
IPC分类号： C08K5/04
CPC分类号： C08K3/26 , C08J3/122 , C08J3/20 , C08J2309/00 , C08J2321/00 , C08K3/013 , C08K3/08 , C08K3/22 , C08K3/346 , C08K3/36 , Y10T428/2982 , Y10T428/2998 , Y10T428/31707 , C08K3/0033 , C08L21/00
摘要： The present invention relates to a composite powder, preparation and use thereof. The composite powder according to the present invention is prepared by intimately mixing an irradiated or non-irradiated rubber latex with a slurry of inorganic particles in a ratio corresponding to that of rubber particles to inorganic particles in the composite powder according to the present invention, and then drying the resultant mixture. The composite powder according to the present invention comprises agglomerates composed of powdery rubber particles and inorganic particles, with inorganic particles being uniformly distributed either inside the agglomerats or both inside the agglomerates and on the surfaces thereof. The composite powder according to the present invention can be easily dispersed in plastic matrixes and thus can be compounded with plastics to produce toughened plastics and thermoplastic elastomers.

6. 发明授权

US06423760B1 Fully vulcanized powdery rubber having a controllable particle size, preparation and use thereof 有权
标题翻译：具有可控粒度的全硫化粉末状橡胶，其制备和用途
公开(公告)号：US06423760B1
公开(公告)日：2002-07-23
申请号：US09702038
申请日：2000-10-30
申请人： Jinliang Qiao , Genshuan Wei , Xiaohong Zhang , Shijun Zhang , Jianming Gao , Wei Zhang , Yiqun Liu , Jiuqiang Li , Fengru Zhang , Renli Zhai , Jingbo Shao , Kunkai Yan , Hua Yin
发明人： Jinliang Qiao , Genshuan Wei , Xiaohong Zhang , Shijun Zhang , Jianming Gao , Wei Zhang , Yiqun Liu , Jiuqiang Li , Fengru Zhang , Renli Zhai , Jingbo Shao , Kunkai Yan , Hua Yin
IPC分类号： C08F246
CPC分类号： C08J3/26 , C08J3/28 , C08J2321/00 , Y10T428/2982
摘要： The present invention provides a fully vulcanized powdery rubber having a particle size of from 20 to 2000 nm, its preparation and use. The vulcanized powdery rubber is obtained by irradiating a rubber latex having a particle size of from 20 to 2000 nm with a high-energy irradiation. The vulcanized powdery rubber is very easily to be dispersed into various plastics, and thus can be mixed with various plastics to prepare toughened plastics and fully valcanized thermoplastic elastomers.
摘要翻译：本发明提供了粒径为20〜2000nm的完全硫化粉末状橡胶，其制备和用途。通过高能量照射照射粒径为20〜2000nm的橡胶胶乳，得到硫化粉末状橡胶。硫化粉末状橡胶非常容易分散在各种塑料中，因此可以与各种塑料混合，制备增韧塑料和完全硫化的热塑性弹性体。

7. 发明授权

US09424959B2 Conductive full vulcanized thermoplastic elastomer and its preparation method 有权
标题翻译：导电全硫化热塑性弹性体及其制备方法
公开(公告)号：US09424959B2
公开(公告)日：2016-08-23
申请号：US14001948
申请日：2012-03-02
申请人： Xiaohong Zhang , Jinliang Qiao , Guicun Qi , Zhihai Song , Chuanlun Cai , Ya Wang , Jianming Gao , Hongbin Zhang , Jinmei Lai , Binghai Li , Haosheng Wang , Yilei Zhu
发明人： Xiaohong Zhang , Jinliang Qiao , Guicun Qi , Zhihai Song , Chuanlun Cai , Ya Wang , Jianming Gao , Hongbin Zhang , Jinmei Lai , Binghai Li , Haosheng Wang , Yilei Zhu
IPC分类号： H01B1/24 , C08J5/00 , C08K5/54 , C08L101/00 , C08L9/02 , C08L9/06 , C08L23/08 , C08K3/04
CPC分类号： H01B1/24 , C08J5/005 , C08J2309/06 , C08J2325/10 , C08K3/04 , C08K3/041 , C08K5/54 , C08K7/06 , C08K2201/001 , C08K2201/011 , C08L9/02 , C08L9/06 , C08L13/00 , C08L23/06 , C08L23/0815 , C08L23/12 , C08L51/06 , C08L77/02 , C08L83/04 , C08L101/00
摘要： The invention provides a conductive full vulcanized thermoplastic elastomer and its preparation method, and relates to the technical field of full vulcanized thermoplastic elastomer. The full vulcanized thermoplastic elastomer is obtained by melt-blending components including rubber particles having crosslinking structure with mean particle diameter of 0.02 to 1 μm, carbon nanotubes as conductive fillers and thermoplastic plastics once, wherein the weight ratio of the rubber particles and the thermoplastic plastics is from 30:70 to 75:25 and the content of conductive fillers is from 0.3 to 10 weight parts based on the total weight of rubber particles and thermoplastic plastics of 100 weight parts. The resulting conductive full vulcanized thermoplastic elastomers have low content of conductive fillers and excellent combination performances. It can be prepared by conventional rubber processing methods and can be used to produce electronic production equipment, means, electronic instrument, instrument housing and decorative materials of clean production workshop having static resistance, electro magnetic interference resistance and clean requirement.
摘要翻译：本发明提供导电全硫化热塑性弹性体及其制备方法，涉及全硫化热塑性弹性体的技术领域。完全硫化的热塑性弹性体通过将包括平均粒径为0.02-1μm的交联结构的橡胶颗粒，碳纳米管作为导电填料和热塑性塑料的组分熔融共混获得，其中橡胶颗粒和热塑性塑料的重量比为30:70〜75:25，导电填料的含量为100〜100重量份的橡胶粒子和热塑性塑料的总重量的0.3〜10重量份。所得的导电全硫化热塑性弹性体具有低含量的导电填料和优异的组合性能。可以通过常规橡胶加工方法制备，可用于生产具有静电阻，电磁干扰电阻和清洁要求的电子生产设备，手段，电子仪器，仪表外壳和清洁生产车间的装饰材料。

8. 发明授权

US09290643B2 Modified rubber masterbatch, and rubber composition and vulcanized rubber produced therefrom, and the preparation processes for them 有权
标题翻译：改性橡胶母料，由其制备的橡胶组合物和硫化橡胶及其制备方法
公开(公告)号：US09290643B2
公开(公告)日：2016-03-22
申请号：US14354233
申请日：2012-10-26
申请人： Jinliang Qiao , Yuexin Cong , Xiaohong Zhang , Ying Li , Jianming Gao , Qianmin Zhang , Zhihai Song , Yanling Sun , Jinmei Lai , Peijun Song , Chuanlun Cai , Guoxun Zhao , Hongbin Zhang , Guicun Qi , Ya Wang , Binghai Li
发明人： Jinliang Qiao , Yuexin Cong , Xiaohong Zhang , Ying Li , Jianming Gao , Qianmin Zhang , Zhihai Song , Yanling Sun , Jinmei Lai , Peijun Song , Chuanlun Cai , Guoxun Zhao , Hongbin Zhang , Guicun Qi , Ya Wang , Binghai Li
IPC分类号： C08L21/00 , C08L9/02 , C08L7/00 , C08L9/00 , C08L9/06 , C08F20/44 , B60C1/00
CPC分类号： C08L9/02 , B60C1/0016 , C08F20/44 , C08L7/00 , C08L9/00 , C08L9/06 , C08L21/00 , C08L2205/22 , Y02T10/862
摘要： The present application relates to a modified rubber masterbatch and preparation method thereof, rubber composition prepared therewith and vulcanized rubber and preparation method thereof. The modified rubber component comprises uncrosslinked rubber and rubber particles having crosslinked structure dispersed therein, wherein the rubber particles having crosslinked structure are synthetic rubber particles and/or natural rubber particles, have an average particle size of 20-500 nm and a gel content of 60% by weight or higher, and wherein the uncrosslinked rubber is styrene-butadiene rubber. The weight ratio of the rubber particles having crosslinked structure to the uncrosslinked rubber is greater than 20:80 and less than or equal to 80:20. The rubber composition comprises a blend of modified rubber component and base rubber, in which the modified rubber masterbatch is present in an amount of 1 to 70 parts by weight, relative to per 100 parts by weight of the base rubber. The vulcanized rubber of the rubber composition has not only low rolling resistance and excellent wet skid resistance, but also excellent wear resistance, and thus can be used for producing high performance tread rubber.
摘要翻译：本发明涉及改性橡胶母料及其制备方法，由其制备的橡胶组合物和硫化橡胶及其制备方法。改性橡胶组分包括未交联的橡胶和其中分散有交联结构的橡胶颗粒，其中具有交联结构的橡胶颗粒是合成橡胶颗粒和/或天然橡胶颗粒，其平均粒度为20-500nm，凝胶含量为60 重量％以上，其中未交联橡胶为苯乙烯 - 丁二烯橡胶。具有交联结构的橡胶颗粒与未交联橡胶的重量比大于20:80且小于或等于80:20。橡胶组合物包含改性橡胶组分和基础橡胶的共混物，其中相对于100重量份的基础橡胶，改性橡胶母料的存在量为1至70重量份。橡胶组合物的硫化橡胶不仅具有低滚动阻力和优异的抗湿滑性，而且具有优异的耐磨性，因此可用于生产高性能的胎面橡胶。

9. 发明申请

US20050031870A1 Composite powder, preparation and use thereof 有权
标题翻译：复合粉末及其制备及应用
公开(公告)号：US20050031870A1
公开(公告)日：2005-02-10
申请号：US10818950
申请日：2004-04-05
申请人： Yiqun Liu , Jinliang Qiao , Xiaohong Zhang , Fan Huang , Jianming Gao , Banghui Tan , Genshuan Wei , Zhihai Song , Zhida Chen
发明人： Yiqun Liu , Jinliang Qiao , Xiaohong Zhang , Fan Huang , Jianming Gao , Banghui Tan , Genshuan Wei , Zhihai Song , Zhida Chen
IPC分类号： C08J3/12 , C08J3/20 , C08K3/00 , B32B5/16
CPC分类号： C08K3/26 , C08J3/122 , C08J3/20 , C08J2309/00 , C08J2321/00 , C08K3/013 , C08K3/08 , C08K3/22 , C08K3/346 , C08K3/36 , Y10T428/2982 , Y10T428/2998 , Y10T428/31707 , C08K3/0033 , C08L21/00
摘要： The present invention relates to a composite powder, preparation and use thereof. The composite powder according to the present invention is prepared by intimately mixing an irradiated or non-irradiated rubber latex with a slurry of inorganic particles in a ratio corresponding to that of rubber particles to inorganic particles in the composite powder according to the present invention, and then drying the resultant mixture. The composite powder according to the present invention comprises agglomerates composed of powdery rubber particles and inorganic particles, with inorganic particles being uniformly distributed either inside the agglomerats or both inside the agglomerates and on the surfaces thereof. The composite powder according to the present invention can be easily dispersed in plastic matrixes and thus can be compounded with plastics to produce toughened plastics and thermoplastic elastomers.
摘要翻译：本发明涉及一种复合粉末，其制备和用途。根据本发明的复合粉末是通过将照射的或未经照射的橡胶胶乳与根据本发明的复合粉末中的无机颗粒的比例将无机颗粒的浆料与橡胶颗粒的浆料相当的比例与无机颗粒紧密混合而制备的，然后干燥所得混合物。根据本发明的复合粉末包括由粉末状橡胶颗粒和无机颗粒组成的附聚物，其中无机颗粒均匀地分布在凝聚体内部或两者在凝聚体内部及其表面上。根据本发明的复合粉末可以容易地分散在塑料基体中，因此可以与塑料混合以生产增韧的塑料和热塑性弹性体。

10. 发明申请

US20140054512A1 CONDUCTIVE FULL VULCANIZED THERMOPLASTIC ELASTOMER AND ITS PREPARATION METHOD 有权
标题翻译：导电全氟化物热塑性弹性体及其制备方法
公开(公告)号：US20140054512A1
公开(公告)日：2014-02-27
申请号：US14001948
申请日：2012-03-02
申请人： Xiaohong Zhang , Jinliang Qiao , Guicun Qi , Zhihai Song , Chuanlun Cai , Ya Wang , Jianming Gao , Hongbin Zhang , Jinmei Lai , Binghai Li , Haosheng Wang , Yilei Zhu
发明人： Xiaohong Zhang , Jinliang Qiao , Guicun Qi , Zhihai Song , Chuanlun Cai , Ya Wang , Jianming Gao , Hongbin Zhang , Jinmei Lai , Binghai Li , Haosheng Wang , Yilei Zhu
IPC分类号： H01B1/24
CPC分类号： H01B1/24 , C08J5/005 , C08J2309/06 , C08J2325/10 , C08K3/04 , C08K3/041 , C08K5/54 , C08K7/06 , C08K2201/001 , C08K2201/011 , C08L9/02 , C08L9/06 , C08L13/00 , C08L23/06 , C08L23/0815 , C08L23/12 , C08L51/06 , C08L77/02 , C08L83/04 , C08L101/00
摘要： The invention provides a conductive full vulcanized thermoplastic elastomer and its preparation method, and relates to the technical field of full vulcanized thermoplastic elastomer. The full vulcanized thermoplastic elastomer is obtained by melt-blending components including rubber particles having crosslinking structure with mean particle diameter of 0.02 to 1 μm, carbon nanotubes as conductive fillers and thermoplastic plastics once, wherein the weight ratio of the rubber particles and the thermoplastic plastics is from 30:70 to 75:25 and the content of conductive fillers is from 0.3 to 10 weight parts based on the total weight of rubber particles and thermoplastic plastics of 100 weight parts. The resulting conductive full vulcanized thermoplastic elastomers have low content of conductive fillers and excellent combination performances. It can be prepared by conventional rubber processing methods and can be used to produce electronic production equipment, means, electronic instrument, instrument housing and decorative materials of clean production workshop having static resistance, electro magnetic interference resistance and clean requirement.
摘要翻译：本发明提供导电全硫化热塑性弹性体及其制备方法，涉及全硫化热塑性弹性体的技术领域。完全硫化的热塑性弹性体通过将包括平均粒径为0.02-1μm的交联结构的橡胶颗粒，碳纳米管作为导电填料和热塑性塑料的组分熔融共混获得，其中橡胶颗粒和热塑性塑料的重量比为30:70〜75:25，导电填料的含量为100〜100重量份的橡胶粒子和热塑性塑料的总重量的0.3〜10重量份。所得的导电全硫化热塑性弹性体具有低含量的导电填料和优异的组合性能。可以通过常规橡胶加工方法制备，可用于生产具有静电阻，电磁干扰电阻和清洁要求的电子生产设备，手段，电子仪器，仪表外壳和清洁生产车间的装饰材料。

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