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1. 发明授权

US09745409B2 Liquid epoxy resin formulations 有权
公开(公告)号：US09745409B2
公开(公告)日：2017-08-29
申请号：US14351273
申请日：2011-11-01
申请人： Rajesh H. Turakhia , Cui-ping Chen , Bill Z. Dellinger , Ludovic Valette , Itaru Kudose , Ha Q. Pham
发明人： Rajesh H. Turakhia , Cui-ping Chen , Bill Z. Dellinger , Ludovic Valette , Itaru Kudose , Ha Q. Pham
IPC分类号： C08G59/24 , C08G59/42 , C08G59/50 , C08L63/00 , C09D163/00 , C09J163/00 , C08G59/06
CPC分类号： C08G59/063 , C08L63/00
摘要： A liquid epoxy resin composition having a reduced tendency to crystallize including at least one liquid epoxy resin having the following generic chemical Structure (I): where n is 0 or an integer of 1 or more; and wherein n=0 is in the range of between about 1 wt % and about 90 wt %; wherein; n=1 is in the range of between about 7 wt % and about 20 wt %; n=2 is in the range of between about 0.8 wt % and about 3 wt %; and n=3 and above is in the range of about 0 wt % and about 2 wt %.

2. 发明授权

US09695272B2 Divinylarene dioxide resin compositions 有权
公开(公告)号：US09695272B2
公开(公告)日：2017-07-04
申请号：US13169358
申请日：2011-06-27
申请人： James Wells Carter , Maurice J. Marks , Ludovic Valette , Gyongyi Gulyas
发明人： James Wells Carter , Maurice J. Marks , Ludovic Valette , Gyongyi Gulyas
IPC分类号： C08G59/22 , C08G59/24 , C08G59/68 , C08G65/18 , C09D11/101 , C09D11/322
CPC分类号： C08G59/22 , C08G59/245 , C08G59/68 , C08G65/18 , C09D11/101 , C09D11/322
摘要： A curable divinylarene dioxide resin composition including (a) at least one divinylarene dioxide, (b) at least one cationic photoinitiator, and (c) optionally, at least one pigment material; a process for making the curable divinylarene dioxide resin composition; and a cured divinylarene dioxide resin composition made therefrom. The cured product made from the above curable divinylarene dioxide resin composition offers improved properties and are useful for various applications including ink formulations.

3. 发明授权

US09056942B2 Curable resin compositions 有权
标题翻译：可固化树脂组合物
公开(公告)号：US09056942B2
公开(公告)日：2015-06-16
申请号：US14236934
申请日：2012-07-18
申请人： Angela I. Padilla-Acevedo , Ludovic Valette , Michael J. Mullins , Kandathil E. Verghese , Mark B. Wilson
发明人： Angela I. Padilla-Acevedo , Ludovic Valette , Michael J. Mullins , Kandathil E. Verghese , Mark B. Wilson
IPC分类号： C09D163/00 , C08G59/24 , C08J5/24 , C08G59/02 , C08G59/50 , C08G59/56
CPC分类号： C08G59/245 , C08G59/027 , C08G59/24 , C08G59/50 , C08G59/56 , C08J5/24 , C08J2363/00 , C09D163/00
摘要： A solvent-free curable epoxy resin composition including (a) at least one divinylarene dioxide; and (b) at least one hardener; wherein the solvent-free curable epoxy resin composition is substantially free of solvent and has at least two exotherm peaks and wherein the exothermic peak difference of the two exotherm peaks is sufficient to allow the curable solvent-free epoxy resin composition of being B-staged.
摘要翻译：一种无溶剂的可固化环氧树脂组合物，其包含（a）至少一种二乙烯基芳烃二氧化物; 和（b）至少一种硬化剂; 其中所述无溶剂的可固化环氧树脂组合物基本上不含溶剂并且具有至少两个放热峰，并且其中两个放热峰的放热峰差足以使得无固化无溶剂的环氧树脂组合物为B阶段。

4. 发明授权

US08877866B2 Curable epoxy resin compositions having improved adhesion to metal substrates and processes for making and using the same 有权
标题翻译：可固化的环氧树脂组合物具有改进的与金属基材的粘附性及其制备和使用方法
公开(公告)号：US08877866B2
公开(公告)日：2014-11-04
申请号：US12445823
申请日：2007-10-10
申请人： Terri J. Carson , Ludovic Valette
发明人： Terri J. Carson , Ludovic Valette
IPC分类号： B05D3/02 , B29C65/02 , B32B17/02 , B32B37/10 , C08L33/02 , C08L61/10 , C08L63/04 , C08L63/00 , C08G59/42 , C08G59/62 , C08L53/02 , H05K1/03
CPC分类号： C08L63/00 , C08G59/42 , C08G59/621 , C08L53/02 , H05K1/0326 , Y10T428/2915 , Y10T442/20 , Y10T442/2934 , Y10T442/3415 , C08L2666/24
摘要： Thermosettable compositions are described having improved adhesion to metal substrates when cured comprising (a) at least one curable epoxy resin; (b) at least one hardener, each hardener having less than 1 primary amine group per molecule and not more than 1 secondary amine group per molecule, the hardener(s) comprising at least one polyhydroxy hydrocarbon, hydrocarbon capable of generating multiple hydroxy groups per molecule during curing of the thermosettable material, or poly(acid anhydride)hydrocarbon other than a blend of (1) a copolymer of an ethylenically unsaturated anhydride and a vinyl compound and (2) a copolymer of an ethylenically unsaturated anhydride and an elastomer, and (c) at least one triblock copolymer comprising at least one elastomeric block and at least one acrylic block. Processes for making a coated article, a fiber-reinforced composite article, prepregs and laminates using the thermosettable compositions are also described, which are useful for making coated articles, fiber-reinforced composites, prepregs, laminates and printed wiring boards.
摘要翻译：描述了可热固化组合物，其在固化时具有改善的对金属基材的粘合性，包括（a）至少一种可固化环氧树脂; （b）至少一种固化剂，每个分子中每个固化剂具有小于1个伯胺基，每分子具有不超过1个仲胺基，该硬化剂包含至少一个多羟基烃，能够产生多个羟基的烃可热固化材料固化期间的分子，或（1）烯键式不饱和酸酐和乙烯基化合物的共聚物和（2）烯属不饱和酸酐和弹性体的共聚物的共混物以外的聚（酸酐）烃，以及（c）至少一种包含至少一个弹性体嵌段和至少一个丙烯酸嵌段的三嵌段共聚物。还描述了制备涂层制品，纤维增强复合制品，预浸料和使用该可热固组合物的层压材料的方法，其可用于制备涂覆制品，纤维增强复合材料，预浸料，层压板和印刷线路板。

5. 发明授权

US08829143B2 Reactive inorganic clusters 有权
标题翻译：活性无机簇
公开(公告)号：US08829143B2
公开(公告)日：2014-09-09
申请号：US13265660
申请日：2010-04-29
申请人： Hynek Benes , Jean-Francois Gerard , Ludovic Valette
发明人： Hynek Benes , Jean-Francois Gerard , Ludovic Valette
IPC分类号： C08G77/06 , C08G77/26
CPC分类号： C08G77/26
摘要： Storage-stable reactive inorganic clusters and a process for preparing such storage-stable reactive inorganic clusters (e.g., silica structures) having, for example, reactive amino groups. The storage-stable reactive inorganic clusters may be used as a curing agent for thermosetting resin compositions such as epoxy resins.
摘要翻译：储存稳定的活性无机簇和制备具有例如反应性氨基的这种储存稳定的活性无机簇（例如二氧化硅结构）的方法。储存稳定的活性无机簇可以用作热固性树脂组合物如环氧树脂的固化剂。

6. 发明授权

US08722798B2 Thermosettable composition containing a combination of an amphiphilic block copolymer and a polyol and a thermoset product therefrom 有权
标题翻译：含有两亲性嵌段共聚物和多元醇的组合的热固性组合物及其热固性产物
公开(公告)号：US08722798B2
公开(公告)日：2014-05-13
申请号：US13201630
申请日：2009-03-09
申请人： Leiming Ji , Yong-Jiang Li , Ludovic Valette
发明人： Leiming Ji , Yong-Jiang Li , Ludovic Valette
IPC分类号： C08L63/00 , C08L63/02 , C08G59/06 , C08G59/42 , C08K3/00 , C08K3/36 , C08L71/02 , C08L87/00
CPC分类号： C08G59/4284 , C08G18/4045 , C08G18/42 , C08G18/58 , C08G18/584 , C08G18/80 , C08G59/4028 , C08G2650/58 , C08K3/36 , C08L63/00 , C08L71/02 , C09D5/02 , C09D5/08 , C09D5/44 , C09D5/4496 , C09D163/00 , C09D167/00 , C25D13/06 , C08L67/00
摘要： A thermosettable composition including (a) at least an amphophilic block copolymer, (b) at least a polyol, (c) at least an epoxy resin containing an average at least 2 oxirane rings per molecule, (d) at least an anhydride hardener containing an average at least 1 anhydride ring per molecule, and (e) at least a catalyst; and a thermoset product prepared from said thermosettable composition.
摘要翻译：一种可热固组合物，其包含（a）至少两亲嵌段共聚物，（b）至少一种多元醇，（c）至少一种每分子含有平均至少2个环氧乙烷环的环氧树脂，（d）至少一种含有每个分子平均至少1个酸酐环，和（e）至少一种催化剂; 和由所述可热固组合物制备的热固性产品。

7. 发明授权

US08404310B2 Thermoset dampener material 有权
标题翻译：热固性阻尼器材料
公开(公告)号：US08404310B2
公开(公告)日：2013-03-26
申请号：US12668825
申请日：2008-07-28
申请人： Martine Rousse , Ludovic Valette
发明人： Martine Rousse , Ludovic Valette
IPC分类号： B05D3/02
CPC分类号： C09D163/00 , C08G59/4042 , C08G59/5086 , C08G2261/3444 , C08L63/00 , C08L65/00 , C09D125/06 , C09D159/00 , C09D161/02 , C09D165/00 , C09D169/00 , C09D171/08 , C09D179/08 , C09D181/04 , C09D181/06
摘要： Thermoset compositions useful for dampening vibrations at elevated temperatures are disclosed. The thermoset compositions may have a glass transition temperature of 1500 C. or greater, a tan δ peak of 0.2 or greater, and a tan δ peak width measured at half-height larger than about 400 C., each as measured by dynamic mechanical thermal analysis (DMTA) at a frequency of 1 Hz. The thermoset compositions may be used to dampen vibrations at temperatures in excess of 100° C.
摘要翻译：公开了用于在高温下抑制振动的热固性组合物。热固性组合物可以具有1500℃或更高的玻璃化转变温度，0.2或更大的tanδ峰，以及在半高度处测量的tanδ峰宽度大于约400℃，每个通过动态机械热测量分析（DMTA）频率为1Hz。热固性组合物可用于在超过100℃的温度下抑制振动。

8. 发明申请

US20100281964A1 DEVICE AND METHOD FOR ASSESSING THE MACHINABILITY OF LAMINATES 失效
标题翻译：用于评估层压板机械性能的装置和方法
公开(公告)号：US20100281964A1
公开(公告)日：2010-11-11
申请号：US12811953
申请日：2008-12-22
申请人： Hamed Lakrout , Stephanie K Anderson , Ludovic Valette , Nikhil Eapen Verghese
发明人： Hamed Lakrout , Stephanie K Anderson , Ludovic Valette , Nikhil Eapen Verghese
IPC分类号： G01N3/42
CPC分类号： G01N3/42 , G01N3/20 , G01N3/58 , G01N19/04 , G01N2203/0647
摘要： A device and method for assessing the machinability, particularly the drillability, of epoxy resin laminates by reproducible indentation and analysis of the delamination area of a laminate sample thus provoked.
摘要翻译：通过可重复的压痕评估环氧树脂层压板的可切削性，特别是可钻性的装置和方法，并且分析了由此引起的层压样品的分层面积。

9. 发明申请

US20100193725A1 THERMOSET DAMPENER MATERIAL 有权
标题翻译：热门防震材料
公开(公告)号：US20100193725A1
公开(公告)日：2010-08-05
申请号：US12668825
申请日：2008-07-28
申请人： Martine Rousse , Ludovic Valette
发明人： Martine Rousse , Ludovic Valette
IPC分类号： E04B1/74 , B05D3/12
CPC分类号： C09D163/00 , C08G59/4042 , C08G59/5086 , C08G2261/3444 , C08L63/00 , C08L65/00 , C09D125/06 , C09D159/00 , C09D161/02 , C09D165/00 , C09D169/00 , C09D171/08 , C09D179/08 , C09D181/04 , C09D181/06
摘要： Thermoset compositions useful for dampening vibrations at elevated temperatures are disclosed. The thermoset compositions may have a glass transition temperature of 1500 C or greater, a tan δ peak of 0.2 or greater, and a tan δ peak width measured at half-height larger than about 400 C, each as measured by dynamic mechanical thermal analysis (DMTA) at a frequency of 1 Hz. The thermoset compositions may be used to dampen vibrations at temperatures in excess of 100° C.
摘要翻译：公开了用于在高温下抑制振动的热固性组合物。热固性组合物可以具有1500℃或更高的玻璃化转变温度，0.2或更大的tanδ峰和在大于约400℃的半高度处测量的tanδ峰宽度，每个通过动态机械热分析测量 DMTA），频率为1Hz。热固性组合物可用于在超过100℃的温度下抑制振动。

10. 发明申请

US20090321117A1 A CURABLE EPOXY RESIN COMPOSITION HAVING A MIXED CATALYST SYSTEM AND LAMINATES MADE THEREFROM 审中-公开
标题翻译：具有混合催化剂体系的可固化环氧树脂组合物及其制备的层压体
公开(公告)号：US20090321117A1
公开(公告)日：2009-12-31
申请号：US12097639
申请日：2006-12-19
申请人： Ludovic Valette , Tomoyuki Aoyama
发明人： Ludovic Valette , Tomoyuki Aoyama
IPC分类号： C08L67/00 , B05D5/12 , B32B27/04 , B32B27/38 , B32B17/10 , B32B15/092 , H05K1/00
CPC分类号： C08G59/621 , C08G59/686 , C08G59/688 , H05K1/0326 , Y10T428/31525 , Y10T428/31529 , Y10T442/2418
摘要： A curable halogen-containing epoxy resin composition comprising: (a) at least one epoxy resin; (b) at least one hardener; wherein the hardener is a compound containing a phenolic hydroxyl functionality or a compound capable of generating a phenolic hydroxyl functionality upon heating; and (c) a catalytic amount of a catalyst system comprising a combination of: (i) at least a first catalyst compound comprising at least one nitrogen-containing catalyst compound; and (ii) at least a second catalyst compound comprising at least one phosphorus-containing catalyst compound; wherein at least one or more of the above components (a)-(c) is halogenated or contains halogen; or if none of the above components are halogenated wherein the resin composition includes (d) a halogenated or halogen-containing flame retardant compound that does not contain nitrogen. The stroke cure gel time of the resin composition is maintained from 90 seconds to 600 seconds when measured at 170° C.; and the cured product formed by curing the curable epoxy resin composition contains well-balanced properties. The composition may be used to obtain a prepreg or a metal-coated foil, or a laminate by laminating the above prepreg and/or the above metal-coated foil. The laminate shows a combination of superior glass transition temperature, decomposition temperature, time to delamination at 288° C., adhesion to copper foil, and excellent flame retardancy.
摘要翻译：一种可固化含卤素的环氧树脂组合物，其包含：（a）至少一种环氧树脂; （b）至少一种硬化剂; 其中所述固化剂是含有酚羟基官能团的化合物或在加热时能够产生酚羟基官能团的化合物; 和（c）催化量的催化剂体系，其包含以下组合的组合：（i）至少包含至少一种含氮催化剂化合物的第一催化剂化合物; 和（ii）至少一种包含至少一种含磷催化剂化合物的第二催化剂化合物; 其中至少一种或多种上述组分（a） - （c）被卤化或含有卤素; 或者如果上述组分都不是卤化的，其中树脂组合物包括（d）不含氮的卤化或含卤阻燃化合物。当在170℃下测量时，树脂组合物的冲程固化凝胶时间保持在90秒至600秒; 并且通过固化可固化环氧树脂组合物形成的固化产物包含良好平衡的性质。该组合物可以用于通过层压上述预浸料和/或上述金属涂覆的箔来获得预浸料或金属涂覆的箔或层压体。该层压板显示优异的玻璃化转变温度，分解温度，288℃下分层时间，对铜箔的粘附性和优异的阻燃性的组合。

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