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1. 发明授权

US06403670B1 Thermosetting composition containing polyhemiacetal ester resin and powdery thermosetting composition 失效
标题翻译：含有聚缩醛酯树脂和粉末状热固性组合物的热固性组合物
公开(公告)号：US06403670B1
公开(公告)日：2002-06-11
申请号：US09623127
申请日：2000-10-13
申请人： Masahiro Ishidoya , Masayuki Takemoto , Atsushi Sato , Koji Sato , Shun Saito
发明人： Masahiro Ishidoya , Masayuki Takemoto , Atsushi Sato , Koji Sato , Shun Saito
IPC分类号： C08F400
CPC分类号： C09D167/025 , C08G18/683 , C08G18/8077 , C08G2150/20 , C08K5/0025 , C08L63/00 , C08L67/025 , C08L101/02 , Y10S525/934 , C08L2666/02 , C08L2666/28
摘要： The present invention relates to a thermosetting composition which comprises: (A) a polyhemiacetal ester resin having a repeat unit represented by formula (1): wherein R1 and R2 are a bivalent organic group, and Y is an oxygen atom or a sulfur atom, and (B) a compound having in the molecule two or more reactive functional groups which can form a chemical bond with the carboxyl group, and optionally, (C) an acid catalyst. The thermosetting composition gives cured products having excellent chemical properties, physical properties, adhesion, smoothness and weathering resistance at relatively lower temperatures and have excellent storage stability, and can be utilized as solvent cutback type, solventless liquid type of 100% effective component or powder thermosetting compositions.
摘要翻译：本发明涉及一种热固性组合物，其包含：（A）具有由式（1）表示的重复单元的聚缩醛酯树脂：其中R1和R2是二价有机基团，Y是氧原子或硫原子，和（B）在分子中具有两个或更多个与羧基形成化学键的反应性官能团的化合物，和任选的（C）酸催化剂。热固性组合物在相对较低的温度下提供具有优异的化学性质，物理性质，粘合性，光滑性和耐候性的固化产物，并且具有优异的储存稳定性，并且可以用作溶剂切割型，无溶剂型的100％有效成分或粉末热固性组合物。

2. 发明授权

US5993909A Thermosetting compositions, methods of coating and coated articles 失效
标题翻译：热固组合物，涂层方法和涂层制品
公开(公告)号：US5993909A
公开(公告)日：1999-11-30
申请号：US776974
申请日：1997-04-21
申请人： Hiroki Mizutani , Yoshinori Nakane , Masahiro Ishidoya
发明人： Hiroki Mizutani , Yoshinori Nakane , Masahiro Ishidoya
IPC分类号： C08F290/06 , B05D3/02
CPC分类号： C08F290/061
摘要： A thermosetting composition which comprises (A) an epoxy group-containing modified polyester polymer comprising a structural moiety of (a) a carboxyl group-containing polyester resin having a number average molecular weight of 1,500 to 50,000 and a resin acid value of 2 to 30 mgKOH/g and a structural moiety of a polymer of (b) an epoxy group-containing vinyl monomer, the carboxyl groups and a part of the epoxy groups being bonded in an equivalent ratio of the carboxyl groups in the component (a) to the epoxy groups in the polymer of the component (b) of 0.1 or less, and having an epoxy equivalent weight of 200 to 2,000 g/mol, and (B) a compound having two or more functional groups which are blocked by a vinyl ether, vinyl thioether or heterocyclic group carrying oxygen or sulfur as the heteroatom and having a double bond of the vinyl type. The composition can give cured articles excellent in hardness, chemical resistance, stain resistance, processability, impact resistance, elasticity and weathering resistance and has a good storage stability.
摘要翻译： PCT No.PCT / JP96 / 01522 Sec。 371日期1997年04月21日 102（e）1997年4月21日PCT PCT 1996年6月5日PCT公布。公开号WO96 / 39454 日本1996年12月12日一种热固性组合物，其包含（A）含环氧基的改性聚酯聚合物，其包含（a）数均分子量为1,500〜50,000的含羧基的聚酯树脂的结构部分和树脂酸值为2〜30mgKOH / g，（b）含有环氧基的乙烯基单体的聚合物的结构部分，羧基和一部分环氧基以组分中的羧基的当量比结合（a）组分（b）的聚合物中的环氧基为0.1以下，环氧当量为200〜2000g / mol，（B）具有2个以上被封闭的官能团的化合物通过乙烯基醚，乙烯基硫醚或携带氧或硫作为杂原子并具有乙烯基类型的双键的杂环基。该组合物可以得到硬度，耐化学性，耐污染性，加工性，耐冲击性，弹性和耐候性优异的固化物，具有良好的储存稳定性。

3. 发明授权

US5549932A Thermosetting compositions, methods of coating and coated articles 失效
标题翻译：热固组合物，涂层方法和涂层制品
公开(公告)号：US5549932A
公开(公告)日：1996-08-27
申请号：US401198
申请日：1995-03-09
申请人： Masahiro Ishidoya , Kishio Shibato , Keiji Komoto , Kenji Shibamoto , Mitsuyuki Mashita , Osamu Ohe
发明人： Masahiro Ishidoya , Kishio Shibato , Keiji Komoto , Kenji Shibamoto , Mitsuyuki Mashita , Osamu Ohe
IPC分类号： B32B27/30 , B32B27/36 , B32B27/38 , C08L29/00 , C08L33/00 , C08L33/02 , C08L33/06 , C08L37/00 , C08L63/00 , C08L67/00 , C08L67/02 , C08L101/02 , C09D133/10 , C09D163/00 , C09D167/00 , C09D201/02 , C09J167/00
CPC分类号： C08L67/00 , C08L101/02 , C09D133/10 , C09D163/00 , C09D167/00 , C09D201/02 , C09J167/00 , C08L33/06 , C08L63/00 , Y10T428/31511 , Y10T428/31518 , Y10T428/31529 , Y10T428/31551 , Y10T428/31699 , Y10T428/31786 , Y10T428/31794 , Y10T428/31797 , Y10T428/31928 , Y10T428/31935
摘要： Thermosetting composition comprises a compound having in the molecule two or more carboxyl groups blocked by a vinyl ether compound, a vinyl thioether compound or a hetero compound having a vinyl type double bond and oxygen or sulfur as the hetero atom, a compound having two or more reactive functional groups which can form a chemical bond with the blocked carboxyl compound by heating, a specific vinyl ether or vinyl thioether and a thermal latent acid catalyst. The blocked carboxy group of the first compound and the reactive functional group of the second compound may be comprised in the same molecule. The thermosetting composition gives cured products having excellent chemical properties, physical properties, weathering resistant and storage stability and is advantageously utilized for coating compositions, ink, adhesive and molded plastics.
摘要翻译：热固性组合物包含在分子中具有被乙烯基醚化合物封闭的两个或多个羧基的化合物，乙烯基硫醚化合物或具有乙烯基型双键的杂化合物和氧或硫作为杂原子的化合物，具有两个或更多个可通过加热与封端的羧基化合物形成化学键的反应性官能团，特定的乙烯基醚或乙烯基硫醚和热潜在酸催化剂。第一化合物的封端羧基和第二化合物的反应性官能团可以包含在相同的分子中。热固性组合物提供具有优异的化学性质，物理性质，耐候性和储存稳定性的固化产物，并且有利地用于涂料组合物，油墨，粘合剂和模制塑料。

4. 发明授权

US5213618A Method for the preparation of chromatic-color metal flake pigments 失效
标题翻译：彩色金属薄片颜料的制备方法
公开(公告)号：US5213618A
公开(公告)日：1993-05-25
申请号：US801740
申请日：1991-12-03
申请人： Thoru Souma , Masahiro Ishidoya , Toshihiko Nakamichi , Naoe Takai
发明人： Thoru Souma , Masahiro Ishidoya , Toshihiko Nakamichi , Naoe Takai
IPC分类号： A61K8/11 , A61Q1/02 , A61Q1/10 , C08K9/02 , C09C1/00 , C09C1/62 , C09D5/36 , C09D11/02
CPC分类号： C09C1/0021 , A61K8/0254 , A61K8/29 , A61Q1/02 , A61Q1/10 , B82Y30/00 , C08K9/02 , C09C1/62 , C09C1/64 , C09D11/037 , C09D5/36 , A61K2800/412 , A61K2800/436 , A61K2800/621 , C01P2004/20 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2004/80 , C01P2006/12 , C01P2006/60 , C01P2006/65 , C01P2006/80 , C09C2200/1054 , C09C2200/1058 , C09C2200/301 , C09C2220/10 , C09C2220/106
摘要： A titanium oxide-coated chromatic-color metal flake pigment is prepared by hydrolyzing an organic titanate ester compound, e.g., tetraisopropoxy titanium, in the presence of the base metal flakes suspended in an organic medium having a pH of 4 to 8. The pigment exhibits iridescent color tones of great aesthetic value delicately varying depending on the thickness of the titanium oxide coating layer. The pigment has high chemical stability, for example, against acids, by virtue of the very uniform and dense coating layer of titanium oxide so that the inventive pigment is useful as a coloring agent in a water-borne composition.
摘要翻译：通过在悬浮在pH4〜8的有机介质中的贱金属薄片的存在下水解有机钛酸酯化合物，例如四异丙氧基钛来制备氧化钛涂覆的彩色金属薄片颜料。根据氧化钛涂层的厚度，微妙的美观价值的彩虹色调微调。该颜料由于氧化钛非常均匀且致密的涂层而具有高的化学稳定性，例如抗酸，因此本发明的颜料可用作水性组合物中的着色剂。

5. 发明授权

US5091492A Resin composition for use as paint 失效
标题翻译：用作涂料的树脂组合物
公开(公告)号：US5091492A
公开(公告)日：1992-02-25
申请号：US564024
申请日：1990-08-07
申请人： Masahiro Ishidoya , Kishio Shibato , Osamu Ohe , Masaaki Kawasaki
发明人： Masahiro Ishidoya , Kishio Shibato , Osamu Ohe , Masaaki Kawasaki
IPC分类号： C09D133/06 , C08F220/18 , C09D4/00 , C09D133/04
CPC分类号： C08F220/18 , C09D4/00
摘要： A resin composition for use as a paint contains a copolymer prepared by copolymerizing a monomer (I) represented by the following formula (I): ##STR1## wherein either one of X.sub.1 and X.sub.2 stands for an acryloyloxy or methacryloyloxy group, the other being a hydrogen atom or an alkyl group having 1 to 6 carbon atoms; R.sub.1 to R.sub.10 each stand for a hydrogen atom or an alkyl group having 1 to 6 carbon atoms; and n is an integer of 1 to 4; with an .alpha.,.beta.-ethylenically unsaturated monomer having a reactive functional group and an .alpha.,.beta.-ethylenically unsaturated monomer having no reactive functional group. A monomer mixture for preparing the copolymer contains 5 to 95 wt % of the monomer (I).

6. 发明授权

US5660937A Thermosetting compositions, methods of coating and coated articles 失效
标题翻译：热固组合物，涂层方法和涂层制品
公开(公告)号：US5660937A
公开(公告)日：1997-08-26
申请号：US401368
申请日：1995-03-09
申请人： Masahiro Ishidoya , Kishio Shibato , Keiji Komoto , Kenji Shibamoto , Mitsuyuki Mashita , Osamu Ohe
发明人： Masahiro Ishidoya , Kishio Shibato , Keiji Komoto , Kenji Shibamoto , Mitsuyuki Mashita , Osamu Ohe
IPC分类号： B32B27/30 , B32B27/36 , B32B27/38 , C08L29/00 , C08L33/00 , C08L33/02 , C08L33/06 , C08L37/00 , C08L63/00 , C08L67/00 , C08L67/02 , C08L101/02 , C09D133/10 , C09D163/00 , C09D167/00 , C09D201/02 , C09J167/00
CPC分类号： C08L67/00 , C08L101/02 , C09D133/10 , C09D163/00 , C09D167/00 , C09D201/02 , C09J167/00 , C08L33/06 , C08L63/00 , Y10T428/31511 , Y10T428/31518 , Y10T428/31529 , Y10T428/31551 , Y10T428/31699 , Y10T428/31786 , Y10T428/31794 , Y10T428/31797 , Y10T428/31928 , Y10T428/31935
摘要： Thermosetting composition comprises a compound having in the molecule two or more carboxyl groups blocked by a vinyl ether compound, a vinyl thioether compound or a hetero compound having a vinyl type double bond and oxygen or sulfur as the hetero atom, a compound having two or more reactive functional groups which can form a chemical bond with the blocked carboxyl compound by heating, a specific vinyl ether or vinyl thioether and a thermal latent acid catalyst. The blocked carboxyl group of the first compound and the reactive functional group of the second compound may be comprised in the same molecule. The thermosetting composition gives cured products having excellent chemical properties, physical properties, weathering resistance and storage stability and is advantageously utilized for coating compositions, ink, adhesive and molded plastics.
摘要翻译：热固性组合物包含在分子中具有被乙烯基醚化合物封闭的两个或多个羧基的化合物，乙烯基硫醚化合物或具有乙烯基型双键的杂化合物和氧或硫作为杂原子的化合物，具有两个或更多个可通过加热与封端的羧基化合物形成化学键的反应性官能团，特定的乙烯基醚或乙烯基硫醚和热潜在酸催化剂。第一化合物的封端羧基和第二化合物的反应性官能团可以包含在相同的分子中。热固性组合物提供具有优异的化学性质，物理性能，耐候性和储存稳定性的固化产物，并且有利地用于涂料组合物，油墨，粘合剂和模制塑料。

7. 发明授权

US5516839A Thermal latent carboxyl compounds and methods of preparation thereof 失效
标题翻译：热潜羧基化合物及其制备方法
公开(公告)号：US5516839A
公开(公告)日：1996-05-14
申请号：US260002
申请日：1994-06-15
申请人： Masahiro Ishidoya , Kishio Shibato , Keiji Komoto , Kenji Shibamoto , Mitsuyuki Mashita , Osamu Ohe
发明人： Masahiro Ishidoya , Kishio Shibato , Keiji Komoto , Kenji Shibamoto , Mitsuyuki Mashita , Osamu Ohe
IPC分类号： C08F299/02 , C07C69/00 , C08F8/14 , C08F290/00 , C08G18/42 , C08G18/82 , C08G59/00 , C08G59/20 , C08G59/32 , C08G59/40 , C08G59/68 , C08G63/00 , C08G63/91 , C08G69/00 , C08L33/02 , C08L63/00 , C08L67/00 , C08L67/02 , C08L67/06 , C09D163/00 , C09D167/00 , C09D167/06 , C09J167/00 , C09J167/06
CPC分类号： C09D167/00 , C08L67/00 , C09D163/00 , C09J167/00
摘要： A thermal latent compound which is prepared by a reaction of a polycarboxyl compound having two or more carboxyl groups in the molecule, having an acid equivalent of not more than 1000 g/mole and a number average molecular weight of not more than 4000, with a monovinyl ether compound, wherein at least two carboxyl groups are transformed into a functional group of the formula (1): ##STR1## wherein R.sup.1, R.sup.2 and R.sup.3 are each a hydrogen atom or an organic group of 1 to 18 carbon atoms, R.sup.4 is an organic group of 1 to 18 carbon atoms, Y.sup.1 is an oxygen atom or R.sup.3 and R.sup.4 are bonded together to form a heterocyclic with Y.sup.1 as a heteroatom.
摘要翻译：通过在分子中具有两个以上羧基的多羧基化合物反应制备的热潜组合物，其酸当量不大于1000克/摩尔，数均分子量不大于4000，与其中至少两个羧基被转化成式（1）的官能团：其中R 1，R 2和R 3各自为氢原子或1至18个碳原子的有机基团 R4是1〜18个碳原子的有机基团，Y1是氧原子，R3和R4键合在一起形成与Y1作为杂原子的杂环。

8. 发明授权

US5202364A Aqueous dispersion coating material containing epoxy denatured alkyd 失效
标题翻译：含环氧树脂变性醇酸树脂的水性分散涂料
公开(公告)号：US5202364A
公开(公告)日：1993-04-13
申请号：US719668
申请日：1991-06-24
申请人： Hitoshi Taniguchi , Masahiro Ishidoya , Ken Nakashima , Hisao Ogawa
发明人： Hitoshi Taniguchi , Masahiro Ishidoya , Ken Nakashima , Hisao Ogawa
IPC分类号： C09D163/00 , C09D167/00
CPC分类号： C09D167/00 , C09D163/00
摘要： An aqueous dispersion coating material containing, as a film-forming constituent, an aqueous dispersion that can be obtained by contacting with an aqueous medium, a base-neutralized resin reaction product with an acid value of 10 to 30 which can be obtained by reacting a water-soluble epoxy-denatured alkyd resin with an epoxy resin in solid state at ordinary temperature and by adding and polymerizing at least a part of these resins and then neutralizing the resin reaction product with a base.Because this coating material has been emulsified in a translucent colloidal emulsion region with an aqueous medium, its finished appearance and corrosion resistance are superior and its structural viscosity can be controlled without damaging the storage stability through the addition of organic solvents, and the excellent finished appearance can also be obtained by atomization coating in addition to immersion coating, flow coating and the like, of vertical areas, and this coating material has applicability to a variety of coating methods.
摘要翻译：一种含水分散体涂料，其包含作为成膜组分的水分散体，其可以通过与水性介质接触而获得的水分散体，酸值为10〜30的碱中和树脂反应产物，其可以通过使水溶性环氧改性醇酸树脂与环氧树脂在常温下为固态，并通过加入和聚合至少一部分这些树脂，然后用碱中和树脂反应产物。由于该涂料已经在具有水性介质的半透明胶体乳剂区域中乳化，其外观和耐腐蚀性优异，可以通过加入有机溶剂而不损害储存稳定性而控制其结构粘度，并且优异的成品外观也可以通过除垂直面积的浸渍涂布，流动涂布等之外的雾化涂料获得，并且该涂料具有适用于各种涂布方法。

9. 发明授权

US06228816B1 Aqueous cutting fluid, aqueous cutting agent, and process for cutting hard brittle materials with the same 失效
标题翻译：水性切削液，水性切削剂，以及用于切割硬脆性材料的方法
公开(公告)号：US06228816B1
公开(公告)日：2001-05-08
申请号：US09380706
申请日：1999-10-06
申请人： Kenji Ito , Shunji Maemichi , Hutoshi Nakanishi , Masahiro Ishidoya , Takashi Tanaka , Toshihiko Nakamichi , Kazuyuki Mori , Shigehiro Hayashi , Hideki Yokoyama
发明人： Kenji Ito , Shunji Maemichi , Hutoshi Nakanishi , Masahiro Ishidoya , Takashi Tanaka , Toshihiko Nakamichi , Kazuyuki Mori , Shigehiro Hayashi , Hideki Yokoyama
IPC分类号： C10M17302
CPC分类号： B28D1/025 , C10M125/08 , C10M125/26 , C10M125/30 , C10M149/00 , C10M149/12 , C10M149/14 , C10M173/02 , C10M2201/00 , C10M2201/02 , C10M2201/061 , C10M2201/087 , C10M2201/10 , C10M2201/102 , C10M2201/103 , C10M2201/105 , C10M2201/14 , C10M2201/16 , C10M2201/18 , C10M2217/00 , C10M2217/02 , C10M2217/022 , C10M2217/04 , C10M2217/041 , C10M2217/042 , C10M2217/043 , C10N2240/401 , C10N2250/02
摘要： An aqueous cutting liquid comprises a cationic water-soluble resin having an amine value of 20 to 200 mgKOH/g, and at least one rheology control agent selected from the group consisting of an inorganic bentonite, an organic bentonite and an aqueous silica sol, wherein the content of a nonvolatile matter of the rheology control agent is 0.1 to 30 percent by weight of the amount of the nonvolatile matter of the cationic water-soluble resin. An aqueous cutting agent comprises the aqueous cutting liquid, and an abrasive grain, wherein the content of the abrasive grain is 100 to 1000 percent by weight of the amount of the nonvolatile matter of the aqueous cutting liquid. A hard and brittle material is cut by a cutting device using the aqueous cutting agent. The present invention provides an aqueous cutting agent which is excellent in dispersion stability of the abrasive grain and viscosity stability during cutting/slicing operations, aqueous cutting liquid usable for the aqueous cutting agent, and a cutting/slicing method excellent in cutting performance, cleanability and the like of the work material on cutting/slicing hard and brittle material by using the cutting agent.
摘要翻译：水性切削液包含胺值为20-200mgKOH / g的阳离子水溶性树脂和至少一种选自无机膨润土，有机膨润土和含水硅溶胶的流变控制剂，其中流变控制剂的不挥发成分的含量为阳离子性水溶性树脂的不挥发成分量的0.1〜30重量％。水性切削剂包括水性切削液和磨料颗粒，其中磨粒的含量为水性切削液的不挥发物质量的100至1000重量％。通过使用水性切割剂的切割装置切割硬脆的材料。本发明提供了一种水性切割剂，其在磨粒的分散稳定性和切割/切片操作期间的粘度稳定性，可用于水性切割剂的水性切割液以及切割性能，可清洁性和切割性优异的切割/切片方法中，通过使用切割剂切割/切割硬脆的材料的工作材料的类似物。

10. 发明授权

US5352740A Thermosetting compositions, thermal latent carboxyl compounds and methods of preparation thereof 失效
标题翻译：热固性组合物，热潜伏性羧基化合物及其制备方法
公开(公告)号：US5352740A
公开(公告)日：1994-10-04
申请号：US680356
申请日：1991-04-04
申请人： Masahiro Ishidoya , Kishio Shibato , Keiji Komoto , Kenji Shibamoto , Mitsuyuki Mashita , Osamu Ohe
发明人： Masahiro Ishidoya , Kishio Shibato , Keiji Komoto , Kenji Shibamoto , Mitsuyuki Mashita , Osamu Ohe
IPC分类号： C08F299/02 , C07C69/00 , C08F8/14 , C08F290/00 , C08G18/42 , C08G18/82 , C08G59/00 , C08G59/20 , C08G59/32 , C08G59/40 , C08G59/68 , C08G63/00 , C08G63/91 , C08G69/00 , C08L33/02 , C08L63/00 , C08L67/00 , C08L67/02 , C08L67/06 , C09D163/00 , C09D167/00 , C09D167/06 , C09J167/00 , C09J167/06
CPC分类号： C09D167/00 , C08L67/00 , C09D163/00 , C09J167/00
摘要： Thermosetting composition is excellent in storage stability, useful as one component thermosetting composition, gives cured products having excellent chemical properties, physical properties and weathering resistance and is favorably utilized in coating compositions, ink, adhesive and molded plastics.The thermosetting composition comprises a compound having in the molecule two or more carboxyl groups blocked by a vinyl ether compound, a vinyl thioether compound or a hetero compound having a vinyl type double bond and oxygen or sulfur as the hetero atom, a compound having two or more reactive functional groups which can form a chemical bond with the blocked carboxyl compound by heating and optionally a thermal latent acid catalyst. The blocked carboxyl group of the first compound and the reactive functional group of the second compound may be comprised in the same molecule.
摘要翻译：热固性组合物的储存稳定性优异，可用作一种组分的热固性组合物，具有优异的化学性质，物理性能和耐候性的固化产物，并且有利地用于涂料组合物，油墨，粘合剂和模塑料中。热固性组合物包含在分子中具有被乙烯基醚化合物封闭的两个或多个羧基，乙烯基硫醚化合物或具有乙烯基型双键的杂化合物和氧或硫作为杂原子的化合物，具有两个或多个可以通过加热和任选的热潜酸催化剂与封端的羧基化合物形成化学键的更多的反应性官能团。第一化合物的封端羧基和第二化合物的反应性官能团可以包含在相同的分子中。

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