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    • 3. 发明申请
    • Method for Producing Electrolyte Solution for Lithium Ion Battery, and Lithium Ion Battery Using the Electrolyte Solution
    • 生产锂离子电池电解质溶液的方法和使用电解液的锂离子电池
    • US20130071760A1
    • 2013-03-21
    • US13697471
    • 2011-04-20
    • Meguru OeKeiji Sato
    • Meguru OeKeiji Sato
    • H01M10/056
    • H01M10/056C01D15/005H01M10/052H01M10/0568H01M10/0569
    • Disclosed is a method for producing a lithium ion battery electrolyte solution containing lithium hexafluorophosphate as an electrolyte and a lithium ion battery using the electrolyte solution. The electrolyte solution is produced by reacting lithium chloride with phosphorus trichloride and chlorine in a non-aqueous organic solvent, reacting a reaction product generated in the solvent with hydrogen fluoride, reacting unreacted remaining hydrogen fluoride with lithium chloride, and then, separating the resulting reaction solution by filtration into a filtrate and a solid residue. The filtrate is obtained as the lithium ion battery electrolyte solution. The solid product is further reacted with phosphorous trichloride and chlorine in a non-aqueous organic solvent. The reaction product generated in the solvent is reacted with hydrogen fluoride, followed by reacting unreacted remaining hydrogen fluoride with lithium chloride. It is possible to accomplish reduction in production cost with the reuse of the reaction residue as production raw material.
    • 公开了一种生产含锂六氟磷酸盐作为电解质的锂离子电池电解液和使用该电解质溶液的锂离子电池的方法。 电解质溶液是通过氯化锂与三氯化磷和氯在非水有机溶剂中反应制备的,使溶剂中产生的反应产物与氟化氢反应,使未反应的剩余氟化氢与氯化锂反应,然后分离所得反应 通过过滤将溶液滤液和固体残余物。 作为锂离子电池电解液得到滤液。 固体产物进一步与三氯化磷和氯在非水有机溶剂中反应。 在溶剂中产生的反应产物与氟化氢反应,然后使未反应的剩余氟化氢与氯化锂反应。 通过将反应残留物用作生产原料,可以实现生产成本的降低。