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    • 1. 发明授权
    • Method of selecting silicon having improved performance
    • 选择具有改进性能的硅的方法
    • US07569716B2
    • 2009-08-04
    • US10590749
    • 2005-03-15
    • Vishu Dutt DosajMichael George KroupaPaul Jacques Marion
    • Vishu Dutt DosajMichael George KroupaPaul Jacques Marion
    • C01B33/02C01B33/08C07F7/00
    • C01B33/025
    • Chemical grade silicon metalloid having improved performance in the direct process for making organohalosilanes is selected by (A) measuring the temperature of each batch of silicon metalloid during both the refining and the casting of the silicon metalloid; (B) measuring the elemental impurity levels in each batch of the silicon metalloid after refining of the silicon metalloid; (C) predicting the properties of the slag phase produced during refining of the silicon metalloid based on equilibrium calculations using the elemental impurity levels and the measured temperatures of each batch of silicon metalloid; and (D) selecting a chemical grade silicon metalloid for use in the direct process for making organohalosilanes based upon the predicted slag properties; such that the slag density, the viscosity, and the melting point of the slag, are within acceptable and predetermined ranges for each individual batch.
    • 通过(A)在硅准金属的精炼和铸造两者中测量每批硅准金属的温度来选择在直接制备有机卤代硅烷的方法中具有改进性能的化学级硅准金属; (B)在精炼硅准金属之后,测量每批硅准金属中的元素杂质水平; (C)基于使用元素杂质水平和每批硅准金属的测量温度的平衡计算,预测在精炼期间产生的渣相的性质; 和(D)根据预测的炉渣性质,选择用于直接制备有机卤代硅烷的化学级硅准金属; 使得渣的渣密度,粘度和熔点在每个单独的批次之内在可接受的和预定的范围内。
    • 5. 发明申请
    • Method of Selecting Silicon Having Improved Performance
    • 选择具有改进性能的硅的方法
    • US20080233035A1
    • 2008-09-25
    • US10590749
    • 2005-03-15
    • Vishu Dutt DosajMichael George KroupaPaul Jacques Marion
    • Vishu Dutt DosajMichael George KroupaPaul Jacques Marion
    • C01B33/021
    • C01B33/025
    • Chemical grade silicon metalloid having improved performance in the direct process for making organohalosilanes is selected by (A) measuring the temperature of each batch of silicon metalloid during both the refing and the casting of the silicon metalloid; (B) measuring the elemental impurity levels in each batch of the silicon metalloid after refining of the silicon metalloid; (C) predicting the properties of the slag phase produced during refining of the silicon metalloid, based on equilibrium calculations, using the elemental impurity levels and the measured temperatures of each batch of silicon metalloid; and (D) selecting a chemical grade silicon metalloid for use in the direct process for making organohalsilanes, based upon the predicted slag properties; such that the slag density, the viscosity, and the melting point of the slag, are within acceptable and predetermined ranges for each individual batch.
    • 通过(A)在硅准金属的铸造和铸造期间测量每批硅准金属的温度来选择在制备有机卤代硅烷的直接方法中具有改进性能的化学级硅准金属; (B)在精炼硅准金属之后,测量每批硅准金属中的元素杂质水平; (C)使用元素杂质水平和每批硅准金属的测量温度,基于平衡计算预测在硅准金属的精炼期间产生的渣相的性质; 和(D)基于预测的炉渣性质选择用于制造有机橡胶的直接方法的化学级硅准金属; 使得渣的渣密度,粘度和熔点在每个单独的批次之内在可接受的和预定的范围内。