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1. 发明授权

US09193870B2 Fibre-reactive dyes, their preparation and their use 有权
标题翻译：纤维活性染料，其制备及其用途
公开(公告)号：US09193870B2
公开(公告)日：2015-11-24
申请号：US14400581
申请日：2013-05-24
申请人： Huntsman International LLC
发明人： Georg Roentgen , Jean-Christophe Graciet , Rainer Hildebrand , Laszlo Fekete , Marie Schmidlin , Hubert Jean-Luc Christnacher
IPC分类号： C09B62/02 , C09B62/80 , C09B62/44 , C09B62/825 , C09B62/83 , C09B62/835 , C09B62/84
CPC分类号： C09B62/80 , C09B62/4405 , C09B62/4407 , C09B62/4409 , C09B62/4413 , C09B62/4415 , C09B62/4416 , C09B62/4418 , C09B62/825 , C09B62/83 , C09B62/835 , C09B62/84
摘要： Reactive dyes of formula (1) wherein Q1 and Q2 are each independently of the other hydrogen or unsubstituted or substituted C1-C4alkyl, A is the radical of a monoazo, polyazo, metal complex azo, anthraquinone, phthalocyanine, formazan or dioxazine chromophore, X is halogen, 3- or 4-carboxypyridin-1-yl, or 3- or 4-carbamoylpyridin-1-yl, Y is vinyl or a radical —CH2—CH2—U and U is a group removable under alkaline conditions, and q is the number 1 or 2, are suitable for dyeing and printing cellulosic or amide-group-containing fiber materials.
摘要翻译：式（1）的活性染料其中Q1和Q2各自独立于另一个氢或未取代或取代的C1-C4烷基，A是单偶氮，多偶氮，金属络合物偶氮，蒽醌，酞菁，甲an或二恶嗪发色团的基团，X 是卤素，3-或4-羧基吡啶-1-基，或3-或4-氨基甲酰基吡啶-1-基，Y是乙烯基或基团-CH 2 -CH 2 -U，U是在碱性条件下可除去的基团，q 是数字1或2，适用于染色和印刷含纤维素或含酰胺基的纤维材料。

2. 发明授权

US08961621B2 Azo dyes 有权
标题翻译：偶氮染料
公开(公告)号：US08961621B2
公开(公告)日：2015-02-24
申请号：US14362931
申请日：2012-11-26
申请人： Huntsman International LLC
发明人： Alexander Mueller , Rainer Hildebrand , Siro Dalle-Nogare
IPC分类号： D06P1/02 , D06P1/06 , C09B33/06
CPC分类号： D06P1/06 , C09B33/06 , C09B67/0041 , C09B67/0046 , D06P1/0096 , D06P1/02
摘要： The present invention relates to dyes of formula (1), wherein each of the residues D1 and D2 represents a radical of formula (2), wherein Ar1 represents the tetravalent radical of a carbocylic or heterocyclic aromatic compound, R1, R2 and R3 are each independently of the other hydrogen, C1-C12alkyl, C1-C12alkoxy, halogen, —OH, —CN, —NO2, —CF3, —SO3H, —NHCOR4, —COOR5, —CONR6R7, —SO2NR8R9, —NR10SO2R11, —SO2R13— or —ZCH2CH2Q, wherein Z is —O—, —SO2—, —NR12—, —CONH— or —NHCO—, Q represents —OH, C1-C12alkyl, —SO2R13—, —NHR14—, —OCH2CH2OH, —SO2CH2CH2OH or —NHCH2CH2OH, R4 is C1-C12alkyl, R5, R6, R7, R8, R9, R10, R12, R13 and R14 are each independently of the others hydrogen or C1-C12alkyl, and R11 is C1-C122alkyl, with the proviso that at least one of the residues D1 and D2 is a radical of formula (2) wherein R3 is —COOR5, —SO2NR8R9, —SO2R13— or —ZCH2CH2Q, dichromatic and trichromatic mixtures containing these dyes and the use of these dyes for dyeing or printing hydroxyl group-containing or nitrogen-containing fibre materials.
摘要翻译：本发明涉及式（1）的染料，其中残基D1和D2各自表示式（2）的基团，其中Ar1表示碳环或杂环芳族化合物的四价基团，R 1，R 2和R 3各自为独立于其它氢，C1-C12烷基，C1-C12烷氧基，卤素，-OH，-CN，-NO2，-CF3，-SO3H，-NHCOR4，-COOR5，-CONR6R7，-SO2NR8R9，-NR10SO2R11，-SO2R13-或 -ZCH 2 CH 2 Q，其中Z是-O - ， - SO 2 - ， - NR 12 - ， - CONH-或-NHCO-，Q表示-OH，C 1 -C 12烷基，-SO 2 R 13 - ， - NHR 14 - ， - OCH 2 CH 2 OH，-SO 2 CH 2 CH 2 OH或 - NHCH 2 CH 2 OH，R 4是C 1 -C 12烷基，R 5，R 6，R 7，R 8，R 9，R 10，R 12，R 13和R 14各自独立地是氢或C 1 -C 12烷基，R 11是C 1 -C 12烷基，条件是至少残基D1和D2之一是式（2）的基团，其中R3是-COOR5，-SO2NR8R9，-SO2R13-或-ZCH2CH2Q，含有这些染料的二色和三色混合物 e使用这些染料染色或印刷含羟基或含氮纤维材料。

3. 发明授权

US09346958B2 Reactive dyes, their preparation and their use 有权
标题翻译：活性染料，它们的制备及其用途
公开(公告)号：US09346958B2
公开(公告)日：2016-05-24
申请号：US14400563
申请日：2013-04-25
申请人： Huntsman International LLC
发明人： Alexander Mueller , Kurt Plattner , Damien Schoehn , Rainer Hildebrand
IPC分类号： D06P5/17 , C09B62/095 , C09B62/44 , D06P1/38 , D06P3/24 , D06P3/66 , C07F11/00 , D06P1/384 , D06P5/30
CPC分类号： C09B62/095 , C07F11/005 , C09B62/4416 , D06P1/38 , D06P1/384 , D06P3/248 , D06P3/66 , D06P5/30
摘要： Reactive dyes of, for example, formula (101) especially suitable for dyeing synthetic polyamide fibre materials and which yield dyeings or prints having good wet-fastness properties, and a process for their preparation.
摘要翻译：特别适用于染色合成聚酰胺纤维材料并且产生具有良好耐湿性的染色或印花的式（101）的活性染料及其制备方法。

4. 发明申请

US20150096131A1 Fibre-Reactive Dyes, Their Preparation and Their Use 有权
标题翻译：纤维活性染料及其制备及其应用
公开(公告)号：US20150096131A1
公开(公告)日：2015-04-09
申请号：US14400581
申请日：2013-05-24
申请人： Huntsman International LLC
发明人： Georg Roentgen , Jean-Christophe Graciet , Rainer Hildebrand , Laszlo Fekete , Marie Schmidlin , Hubert Jean-Luc Christnacher
IPC分类号： C09B62/80 , C09B62/84 , C09B62/83 , C09B62/835 , C09B62/825
CPC分类号： C09B62/80 , C09B62/4405 , C09B62/4407 , C09B62/4409 , C09B62/4413 , C09B62/4415 , C09B62/4416 , C09B62/4418 , C09B62/825 , C09B62/83 , C09B62/835 , C09B62/84
摘要： Reactive dyes of formula (1) wherein Q1 and Q2 are each independently of the other hydrogen or unsubstituted or substituted C1-C4alkyl, A is the radical of a monoazo, polyazo, metal complex azo, anthraquinone, phthalocyanine, formazan or dioxazine chromophore, X is halogen, 3- or 4-carboxypyridin-1-yl, or 3- or 4-carbamoylpyridin-1-yl, Y is vinyl or a radical —CH2—CH2—U and U is a group removable under alkaline conditions, and q is the number 1 or 2, are suitable for dyeing and printing cellulosic or amide-group-containing fibre materials.
摘要翻译：式（1）的活性染料其中Q1和Q2各自独立于另一个氢或未取代或取代的C1-C4烷基，A是单偶氮，多偶氮，金属络合物偶氮，蒽醌，酞菁，甲an或二恶嗪发色团的基团，X 是卤素，3-或4-羧基吡啶-1-基，或3-或4-氨基甲酰基吡啶-1-基，Y是乙烯基或基团-CH 2 -CH 2 -U，U是在碱性条件下可除去的基团，q 是数字1或2，适用于染色和印刷含纤维素或含酰胺基的纤维材料。

5. 发明授权

US10550268B2 Fibre reactive formazan dyes, their preparation and their use 有权
公开(公告)号：US10550268B2
公开(公告)日：2020-02-04
申请号：US16047969
申请日：2016-12-06
申请人： Huntsman International LLC
发明人： Hubert Jean-Luc Christnacher , Fanny Ehret , Athanassios Tzikas , Rainer Hildebrand , Michael Nicollet
IPC分类号： C09B62/503 , C09D11/328 , D06P5/30 , D06P1/38 , D06P3/66
摘要： A reactive dye of formula wherein Z1 and Z2 are each independently of the other vinyl or a radical —CH2—CH2—Y and Y is a group removable under alkaline conditions, n is the number 1, 2, 3 or 4, m is the number 2, 3 or 4, q is the number 0 or 1, and the substituents —(SO3H)n, —SO2—Z1 and —NH—CO—(CH2)m—SO2—Z2 are bound to the benzene rings A, B and/or C, said benzene rings A, B and/or C are optionally further substituted by at least one substituent selected from the group C1-C4alkyl, C1-C4alkoxy and halogen, is suitable for dyeing and printing cellulosic or amide-group-containing fibre materials.

6. 发明申请

US20150143639A1 Reactive Dyes, Their Preparation and Their Use 有权
标题翻译：活性染料及其制备及其应用
公开(公告)号：US20150143639A1
公开(公告)日：2015-05-28
申请号：US14400563
申请日：2013-04-25
申请人： Huntsman International LLC
发明人： Alexander Mueller , Kurt Plattner , Damien Schoehn , Rainer Hildebrand
IPC分类号： C09B62/095 , D06P1/384 , D06P5/30 , C07F11/00
CPC分类号： C09B62/095 , C07F11/005 , C09B62/4416 , D06P1/38 , D06P1/384 , D06P3/248 , D06P3/66 , D06P5/30
摘要： Reactive dyes of formula (1), wherein Me is chromium, cobalt or iron, R1 is hydrogen or unsubstituted or substituted C1-C4alkyl, E is a bivalent radical of formula (1a), (1b) or (1c) wherein X denotes chlorine or fluorine, T is a fibre-reactive radical of formula (2a), (2b), (2c), (2d), (2e), or (2f), (R3)0-2 denotes from 0 to 2 identical or different substituents from the group halogen, C1-C4alkyl, C1-C4alkoxy and sulfo, Z is vinyl or a —CH2—CH2—U radical and U is a group that is removable under alkaline conditions, Q is a —CH(Hal)-CH2-Hal or —C(Hal)=CH2 group, q is the number 0 or 1, G is a bivalent radical of formula (1d) or (1e) wherein (R2)s denotes s identical or different substituents from the group halogen, nitro, unsubstituted or halo-substituted C1-C4alkyl, C2-C4alkanoylamino, C1-C4alkylsulfonyl, carbamoyl, sulfamoyl, sulfo and -E-T, wherein E and T are as defined above, s is the number 0, 1, 2 or 3, A denotes a bivalent radical of formula (3a), (3b) or (3c), wherein R1, R2, X, T, q and s are as defined above, R4 and R7 denote hydrogen, C1-C4alkyl, —COOH or —COO—C1-C4alkyl, R5 and R6 represent, each independently of the other, identical or different substituents from the group hydroxyl, halogen, nitro, unsubstituted or halo-substituted C1-C4alkyl, C1-C4alkoxy, C2-C4alkanoylamino, C1-C4alkylsulfonyl, carbamoyl, sulfamoyl and sulfo, and t and u are each independently of the other the number 0, 1, 2 or 3, are especially suitable for dyeing synthetic polyamide fibre materials and yield dyeings or prints having good wet-fastness properties.
摘要翻译：式（1）的活性染料其中Me为铬，钴或铁，R1为氢或未取代或取代的C1-C4烷基，E为式（1a），（1b）或（1c）的二价基团，其中X表示氯或氟，T是式（2a），（2b），（2c），（2d），（2e）或（2f）的纤维反应性基团，（R3）0-2表示0至2个相同或不同的取代基为卤素，C 1 -C 4烷基，C 1 -C 4烷氧基和磺基，Z为乙烯基或-CH 2 -CH 2 -U基，U为在碱性条件下可除去的基团，Q为-CH（Hal） - CH 2 Hal或-C（Hal）= CH 2基，q是数字0或1，G是式（1d）或（1e）的二价基团，其中（R2）s表示与基团卤素相同或不同的取代基硝基，未取代或卤素取代的C 1 -C 4烷基，C 2 -C 4烷酰基氨基，C 1 -C 4烷基磺酰基，氨基甲酰基，氨磺酰基，磺基和-ET，其中E和T如上所定义，s是0,1,2或3， A表示式（3a），（3b）或（3c）的二价基团，其中 n R 1，R 2，X，T，q和s如上所定义，R 4和R 7表示氢，C 1 -C 4烷基，-COOH或-COO-C 1 -C 4烷基，R 5和R 6各自独立地表示相同或相同的与羟基，卤素，硝基，未取代或卤素取代的C 1 -C 4烷基，C 1 -C 4烷氧基，C 2 -C 4烷酰基氨基，C 1 -C 4烷基磺酰基，氨基甲酰基，氨磺酰基和磺基的不同取代基和t和u各自独立地为数 0,1,2或3特别适用于染色合成聚酰胺纤维材料，并产生具有良好耐湿性能的染色或印花。

7. 发明申请

US20140304926A1 Azo Dyes 有权
标题翻译：偶氮染料
公开(公告)号：US20140304926A1
公开(公告)日：2014-10-16
申请号：US14362931
申请日：2012-11-26
申请人： Huntsman International LLC
发明人： Alexander Mueller , Rainer Hildebrand , Siro Dalle-Nogare
IPC分类号： D06P1/06 , C09B33/06
CPC分类号： D06P1/06 , C09B33/06 , C09B67/0041 , C09B67/0046 , D06P1/0096 , D06P1/02
摘要： The present invention relates to dyes of formula (1), wherein each of the residues D1 and D2 represents a radical of formula (2), wherein Ar1 represents the tetravalent radical of a carbocylic or heterocyclic aromatic compound, R1, R2 and R3 are each independently of the other hydrogen, C1-C12alkyl, C1-C12alkoxy, halogen, —OH, —CN, —NO2, —CF3, —SO3H, —NHCOR4, —COOR5, —CONR6R7, —SO2NR8R9, —NR10SO2R11, —SO2R13— or —ZCH2CH2Q, wherein Z is —O—, —SO2—, —NR12—, —CONH— or —NHCO—, Q represents —OH, C1-C12alkyl, —SO2R13—, —NHR14—, —OCH2CH2OH, —SO2CH2CH2OH or —NHCH2CH2OH, R4 is C1-C12alkyl, R5, R6, R7, R8, R9, R10, R12, R13 and R14 are each independently of the others hydrogen or C1-C12alkyl, and R11 is C1-C122alkyl, with the proviso that at least one of the residues D1 and D2 is a radical of formula (2) wherein R3 is —COOR5, —SO2NR8R9, —SO2R13— or —ZCH2CH2Q, dichromatic and trichromatic mixtures containing these dyes and the use of these dyes for dyeing or printing hydroxyl group-containing or nitrogen-containing fibre materials.
摘要翻译：本发明涉及式（1）的染料，其中残基D1和D2各自表示式（2）的基团，其中Ar1表示碳环或杂环芳族化合物的四价基团，R 1，R 2和R 3各自为独立于其它氢，C1-C12烷基，C1-C12烷氧基，卤素，-OH，-CN，-NO2，-CF3，-SO3H，-NHCOR4，-COOR5，-CONR6R7，-SO2NR8R9，-NR10SO2R11，-SO2R13-或 -ZCH 2 CH 2 Q，其中Z是-O - ， - SO 2 - ， - NR 12 - ， - CONH-或-NHCO-，Q表示-OH，C 1 -C 12烷基，-SO 2 R 13 - ， - NHR 14 - ， - OCH 2 CH 2 OH，-SO 2 CH 2 CH 2 OH或 - NHCH2CH2OH，R4是C1-C12烷基，R5，R6，R7，R8，R9，R10，R12，R13和R14各自独立地是氢或C1-C12烷基，R11是C1-C12-2烷基，条件是至少残基D1和D2之一是式（2）的基团，其中R3是-COOR5，-SO2NR8R9，-SO2R13-或-ZCH2CH2Q，含有这些染料的二色和三色混合物 e使用这些染料染色或印刷含羟基或含氮纤维材料。

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