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    • 1. 发明授权
    • Electron microscope sample holder and sample observation method
    • 电子显微镜样品架和样品观察法
    • US09159530B2
    • 2015-10-13
    • US14002056
    • 2011-10-28
    • Kotaro HosoyaMasaomi OhnoHaruhiko Hatano
    • Kotaro HosoyaMasaomi OhnoHaruhiko Hatano
    • H01J37/20H01J37/28
    • H01J37/20H01J37/28H01J2237/2001H01J2237/2003
    • The present invention makes it possible, even when using an ordinary electron beam device (not an environment-controlled electron beam device), to create locally a low vacuum condition in the vicinity of a sample and cool said sample by means of a sample holder alone, without modifying the device or adding equipment such as a gas cylinder. The sample to be observed is placed in a sample holder provided with: a vessel that can contain a substance to serve as a gas source; and a through-hole in the bottom of a sample mount on said vessel. Via the through-hole, gas evaporating or volatilizing from the vessel is supplied to the sample under observation, thereby creating a localized low-vacuum state at or in the vicinity of the sample. Also, the heat of vaporization required for volatilization can be used to cool the sample.
    • 本发明使得即使使用普通的电子束装置(不是环境控制的电子束装置)也可以在样品附近局部地产生低真空条件,并且可以通过样品架单独冷却所述样品 ,而不需要修改设备或添加气瓶等设备。 将要观察的样品放置在样品架中,该样品架设有:容纳可用作气体源的物质的容器; 以及在所述容器上的样品架底部的通孔。 通过通孔,从容器蒸发或挥发的气体被供给到观察样品,从而在样品或其附近产生局部低真空状态。 此外,挥发所需的蒸发热可用于冷却样品。
    • 2. 发明申请
    • ELECTRON MICROSCOPE SAMPLE HOLDER AND SAMPLE OBSERVATION METHOD
    • 电子显微镜样品夹具和样品观察方法
    • US20140014835A1
    • 2014-01-16
    • US14002056
    • 2011-10-28
    • Kotaro HosoyaMasaomi OhnoHaruhiko Hatano
    • Kotaro HosoyaMasaomi OhnoHaruhiko Hatano
    • H01J37/20
    • H01J37/20H01J37/28H01J2237/2001H01J2237/2003
    • The present invention makes it possible, even when using an ordinary electron beam device (not an environment-controlled electron beam device), to create locally a low vacuum condition in the vicinity of a sample and cool said sample by means of a sample holder alone, without modifying the device or adding equipment such as a gas cylinder. The sample to be observed is placed in a sample holder provided with: a vessel that can contain a substance to serve as a gas source; and a through-hole in the bottom of a sample mount on said vessel. Via the through-hole, gas evaporating or volatilizing from the vessel is supplied to the sample under observation, thereby creating a localized low-vacuum state at or in the vicinity of the sample. Also, the heat of vaporization required for volatilization can be used to cool the sample.
    • 本发明使得即使使用普通的电子束装置(不是环境控制的电子束装置)也可以在样品附近局部地产生低真空条件,并且可以通过样品架单独冷却所述样品 ,而不需要修改设备或添加气瓶等设备。 将要观察的样品放置在样品架中,该样品架设有:容纳可用作气体源的物质的容器; 以及在所述容器上的样品架底部的通孔。 通过通孔,从容器蒸发或挥发的气体被供给到观察样品,从而在样品或其附近产生局部低真空状态。 此外,挥发所需的蒸发热可用于冷却样品。