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    • 2. 发明申请
    • ELECTRODE MATERIALS AND PROCESS FOR PRODUCING THEM
    • 电极材料及其生产工艺
    • US20120205595A1
    • 2012-08-16
    • US13370927
    • 2012-02-10
    • Martin SCHULZ-DOBRICKBastian EWALDHartmut HIBSTJordan Keith LAMPERT
    • Martin SCHULZ-DOBRICKBastian EWALDHartmut HIBSTJordan Keith LAMPERT
    • H01B1/06H01M4/583
    • H01B1/04H01M4/131H01M4/1391H01M4/505H01M4/525
    • Process for producing electrode materials, wherein (a) (A) iron or at least one iron compound in which Fe is present in the oxidation state zero, +2 or +3, (B) silicon or at least one silicon compound selected from among silicon halides, silicon carbide, SiO, silica gels, silicic acid and silanes having at least one alkyl group or at least one alkoxy group per molecule, (C) at least one lithium compound, (D) at least one carbon source which can be a separate carbon source or at the same time at least one iron compound (A) or silicon compound (B) or lithium compound (C), (E) optionally at least one reducing agent, (F) optionally at least one compound which has a transition metal or metal other than iron of groups 3 to 13 of the Periodic Table of the Elements, (G) optionally water or at least one organic solvent, are mixed with one another, (b) the mixture thus obtained is dried convectively and (c) thermally treated at temperatures in the range from 400 to 1200° C.
    • 制备电极材料的方法,其中(A)(A)铁或至少一种其中Fe以氧化态为零,+2或+3,(B)硅或至少一种选自以下的硅化合物的铁化合物: 每分子具有至少一个烷基或至少一个烷氧基的硅卤化物,碳化硅,SiO,硅胶,硅酸和硅烷,(C)至少一种锂化合物,(D)至少一种可以是 单独的碳源或同时至少一种铁化合物(A)或硅化合物(B)或锂化合物(C),(E)任选至少一种还原剂,(F)任选的至少一种化合物,其具有 (G)任选的水或至少一种有机溶剂中的过渡金属或不同于铁的第3至13族的金属彼此混合,(b)由此获得的混合物对流干燥, (c)在400-1200℃的温度下进行热处理。