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    • 1. 发明申请
    • COATED SILVER NANOPARTICLES AND MANUFACTURING METHOD THEREFOR
    • 包覆银纳米颗粒及其制造方法
    • US20120043510A1
    • 2012-02-23
    • US13264204
    • 2010-03-31
    • Masato KuriharaMasaomi Sakamoto
    • Masato KuriharaMasaomi Sakamoto
    • H01B1/22B82B3/00B82Y99/00
    • H01B1/22B05D5/12B22F1/0022B22F1/0062B22F9/30B22F2998/00B22F2999/00B82Y30/00C09D5/24H05K1/097B22F2301/255B22F2304/054
    • The present invention provides coated silver nanoparticles for use as an electrically conductive material capable of sintering at lower temperatures that is able to be used even with flexible printed substrates having low heat resistance, and a manufacturing method therefor. The coated silver nanoparticles of the present invention have a mean particle diameter of 30 nm or less and are coated with protective molecules amine, and are characterized in that the weight loss rate when heated to 160° C. in thermogravimetric measurement is 30% or more. The coated silver nanoparticles of the present invention are also characterized in that a silver-colored sintered film can be formed by sintering at a temperature of 100° C. or lower for 1 hour or less. These coated silver nanoparticles are manufactured by mixing a silver compound that forms metallic silver when decomposed by heating, an alkylamine and an alkyldiamine to prepare a complex compound, and by thermally decomposing the silver compound by heating the complex compound.
    • 本发明提供了用作能够在较低温度下烧结的导电材料的涂覆银纳米颗粒,即使在具有低耐热性的柔性印刷基板的情况下也能够使用它们及其制造方法。 本发明的被覆银纳米粒子的平均粒径为30nm以下,并涂有保护分子胺,其特征在于,在热重量测定中加热至160℃时的重量损失率为30%以上 。 本发明的涂覆银纳米粒子的特征还在于,可以在100℃以下的温度下烧结1小时以下,形成银色烧结膜。 通过加热分解形成金属银的银化合物,烷基胺和烷基二胺制备复合化合物,通过加热配位化合物热分解银化合物来制造这些被覆银纳米粒子。
    • 2. 发明授权
    • Coated silver nanoparticles and manufacturing method therefor
    • 涂覆银纳米粒子及其制造方法
    • US09496068B2
    • 2016-11-15
    • US13264204
    • 2010-03-31
    • Masato KuriharaMasaomi Sakamoto
    • Masato KuriharaMasaomi Sakamoto
    • H01B1/22B05D5/12C09D5/24B22F1/00B22F9/30B82Y30/00H05K1/09
    • H01B1/22B05D5/12B22F1/0022B22F1/0062B22F9/30B22F2998/00B22F2999/00B82Y30/00C09D5/24H05K1/097B22F2301/255B22F2304/054
    • The present invention provides coated silver nanoparticles for use as an electrically conductive material capable of sintering at lower temperatures that is able to be used even with flexible printed substrates having low heat resistance, and a manufacturing method therefor. The coated silver nanoparticles of the present invention have a mean particle diameter of 30 nm or less and are coated with protective molecules amine, and are characterized in that the weight loss rate when heated to 160° C. in thermogravimetric measurement is 30% or more. The coated silver nanoparticles of the present invention are also characterized in that a silver-colored sintered film can be formed by sintering at a temperature of 100° C. or lower for 1 hour or less. These coated silver nanoparticles are manufactured by mixing a silver compound that forms metallic silver when decomposed by heating, an alkylamine and an alkyldiamine to prepare a complex compound, and by thermally decomposing the silver compound by heating the complex compound.
    • 本发明提供了用作能够在较低温度下烧结的导电材料的涂覆银纳米颗粒,即使在具有低耐热性的柔性印刷基板的情况下也能够使用它们及其制造方法。 本发明的被覆银纳米粒子的平均粒径为30nm以下,并涂有保护分子胺,其特征在于,在热重量测定中加热至160℃时的重量损失率为30%以上 。 本发明的涂覆银纳米粒子的特征还在于,可以在100℃以下的温度下烧结1小时以下,形成银色烧结膜。 通过加热分解形成金属银的银化合物,烷基胺和烷基二胺制备复合化合物,通过加热配位化合物热分解银化合物来制造这些被覆银纳米粒子。