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1. 发明授权

US11078172B2 Integrated methods for chemical synthesis 有权
公开(公告)号：US11078172B2
公开(公告)日：2021-08-03
申请号：US16453775
申请日：2019-06-26
申请人： Novomer, Inc.
发明人： Sadesh H. Sookraj , Michael A. Slowik
IPC分类号： C07D307/60 , C07D305/12 , C01B3/50 , C10G2/00
摘要： The integrated processes herein provide improved carbon efficiency for processes based on coal or biomass gasification or steam methane reforming. Provided are also ethylene oxide carbonylation products such as beta-propiolactone and succinic anhydride having a bio-based content between 0% and 100%, and methods for producing and analyzing the same.

2. 发明申请

US20150005513A1 PROCESS FOR THE PRODUCTION OF ACID ANHYDRIDES FROM EPOXIDES 有权
标题翻译：从环氧化物生产酸酐的方法
公开(公告)号：US20150005513A1
公开(公告)日：2015-01-01
申请号：US14378290
申请日：2013-02-12
申请人： Novomer, Inc.
发明人： Han Lee , Michael A. Slowik
IPC分类号： C07D307/60 , B01J31/22 , C07D305/12
CPC分类号： C07D307/60 , B01J31/2295 , B01J2231/48 , B01J2531/31 , B01J2531/845 , C07D303/12 , C07D305/12
摘要： A method of making acid anhydrides from epoxide and carbon monoxide feedstocks is presented. In various aspects, the method includes steps of reacting the contents of a feed stream comprising an epoxide, a solvent, a carbonylation catalyst and carbon monoxide to produce a first carbonylation product stream comprising a beta-lactone, then reacting the contents of the first carbonylation product stream with additional carbon monoxide to produce a second carbonylation product stream comprising an acid anhydride, and separating at least a portion of the acid anhydride from the second carbonylation product stream to produce: i) an acid anhydride product stream comprising the separated portion of acid anhydride; and ii) a recycling stream comprising the carbonylation catalyst, and finally adding the recycling stream to the feed stream.
摘要翻译：提出了从环氧化物和一氧化碳原料制备酸酐的方法。在各个方面，该方法包括使包含环氧化物，溶剂，羰基化催化剂和一氧化碳的进料流的内容物反应以产生包含β-内酯的第一羰基化产物流，然后使第一羰基化反应的内容物产生含有一氧化碳的产物流以产生包含酸酐的第二羰基化产物流，并将至少一部分酸酐与第二羰基化产物流分离以产生：i）包含酸的分离部分的酸酐产物流酐; 和ii）包含羰基化催化剂的再循环流，最后将再循环流加入进料流中。

3. 发明申请

US20200172396A1 INTEGRATED METHODS FOR CHEMICAL SYNTHESIS 审中-公开
公开(公告)号：US20200172396A1
公开(公告)日：2020-06-04
申请号：US16787510
申请日：2020-02-11
申请人： Novomer, Inc.
发明人： Sadesh H. Sookraj , Michael A. Slowik
IPC分类号： C01B3/50 , B01J31/00 , C07C1/20 , C07C29/149 , C10G2/00 , C07C29/151 , C07C51/09 , H01M8/0668 , H01M8/0612 , C07D305/12 , C07D307/60
摘要： Among other things, the present invention encompasses the applicant's recognition that epoxide carbonylation can be performed industrially utilizing syngas streams containing hydrogen, carbon monoxide and varying amounts carbon dioxide. Contrary to expectation, the epoxide carbonylation reaction proceeds selectively in the presence of these mixed gas streams and incorporates excess CO in the syngas stream into valuable chemical precursors, resulting in hydrogen streams substantially free of CO. This is economically and environmentally preferable to performing WSGR which releases the excess carbon as CO2. The integrated processes herein therefore provide improved carbon efficiency for processes based on coal or biomass gasification or steam methane reforming.

4. 发明授权

US09403788B2 Process for the production of acid anhydrides from epoxides 有权
标题翻译：从环氧化物生产酸酐的方法
公开(公告)号：US09403788B2
公开(公告)日：2016-08-02
申请号：US14378290
申请日：2013-02-12
申请人： Novomer, Inc.
发明人： Han Lee , Michael A. Slowik
IPC分类号： C07D307/60 , C07D303/12 , B01J31/22 , C07D305/12
CPC分类号： C07D307/60 , B01J31/2295 , B01J2231/48 , B01J2531/31 , B01J2531/845 , C07D303/12 , C07D305/12
摘要： A method of making acid anhydrides from epoxide and carbon monoxide feedstocks is presented. In various aspects, the method includes steps of reacting the contents of a feed stream comprising an epoxide, a solvent, a carbonylation catalyst and carbon monoxide to produce a first carbonylation product stream comprising a beta-lactone, then reacting the contents of the first carbonylation product stream with additional carbon monoxide to produce a second carbonylation product stream comprising an acid anhydride, and separating at least a portion of the acid anhydride from the second carbonylation product stream to produce: i) an acid anhydride product stream comprising the separated portion of acid anhydride; and ii) a recycling stream comprising the carbonylation catalyst, and finally adding the recycling stream to the feed stream.
摘要翻译：提出了一种从环氧化物和一氧化碳原料制备酸酐的方法。在各个方面，该方法包括使包含环氧化物，溶剂，羰基化催化剂和一氧化碳的进料流的内容物反应以产生包含β-内酯的第一羰基化产物流，然后使第一羰基化反应的内容物产生含有一氧化碳的产物流以产生包含酸酐的第二羰基化产物流，并将至少一部分酸酐与第二羰基化产物流分离以产生：i）包含酸的分离部分的酸酐产物流酐; 和ii）包含羰基化催化剂的再循环流，最后将再循环流加入进料流中。

5. 发明申请

US20210403446A1 INTEGRATED METHODS FOR CHEMICAL SYNTHESIS 有权
公开(公告)号：US20210403446A1
公开(公告)日：2021-12-30
申请号：US17386627
申请日：2021-07-28
申请人： Novomer, Inc.
发明人： Sadesh H. Sookraj , Michael A. Slowik
IPC分类号： C07D305/12 , C07D307/60 , C01B3/50 , C10G2/00
摘要： The integrated processes herein provide improved carbon efficiency for processes based on coal or biomass gasification or steam methane reforming. Provided are also ethylene oxide carbonylation products such as beta-propiolactone and succinic anhydride having a bio-based content between 0% and 100%, and methods for producing and analyzing the same.

6. 发明授权

US10829372B2 Integrated methods for chemical synthesis 有权
公开(公告)号：US10829372B2
公开(公告)日：2020-11-10
申请号：US16787510
申请日：2020-02-11
申请人： Novomer, Inc.
发明人： Sadesh H. Sookraj , Michael A. Slowik
IPC分类号： H01M8/0612 , H01M8/0668 , C01B3/50 , C07D307/60 , C07C51/09 , C07C29/151 , C10G2/00 , C07C29/149 , C07C1/20 , B01J31/00 , C07D305/12 , B01J31/20
摘要： Among other things, the present invention encompasses the applicant's recognition that epoxide carbonylation can be performed industrially utilizing syngas streams containing hydrogen, carbon monoxide and varying amounts carbon dioxide. Contrary to expectation, the epoxide carbonylation reaction proceeds selectively in the presence of these mixed gas streams and incorporates excess CO in the syngas stream into valuable chemical precursors, resulting in hydrogen streams substantially free of CO. This is economically and environmentally preferable to performing WSGR which releases the excess carbon as CO2. The integrated processes herein therefore provide improved carbon efficiency for processes based on coal or biomass gasification or steam methane reforming.

7. 发明授权

US10597294B2 Integrated methods for chemical synthesis 有权
公开(公告)号：US10597294B2
公开(公告)日：2020-03-24
申请号：US15314429
申请日：2015-05-29
申请人： Novomer, Inc.
发明人： Sadesh H. Sookraj , Michael A. Slowik
IPC分类号： H01M8/0612 , H01M8/0668 , C01B3/50 , C07D307/60 , C07C51/09 , C07C29/151 , C10G2/00 , C07C29/149 , C07C1/20 , B01J31/00 , C07D305/12 , B01J31/20
摘要： Among other things, the present invention encompasses the applicant's recognition that epoxide carbonylation can be performed industrially utilizing syngas streams containing hydrogen, carbon monoxide and varying amounts carbon dioxide. Contrary to expectation, the epoxide carbonylation reaction proceeds selectively in the presence of these mixed gas streams and incorporates excess CO in the syngas stream into valuable chemical precursors, resulting in hydrogen streams substantially free of CO. This is economically and environmentally preferable to performing WSGR which releases the excess carbon as CO2. The integrated processes herein therefore provide improved carbon efficiency for processes based on coal or biomass gasification or steam methane reforming.

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