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1. 发明授权

US08357773B1 Steam purification of polyimide resins 有权
标题翻译：聚酰亚胺树脂的蒸汽净化
公开(公告)号：US08357773B1
公开(公告)日：2013-01-22
申请号：US13286161
申请日：2011-10-31
申请人： Robert R. Gallucci , Robert Hossan , Daniel F. Lowery
发明人： Robert R. Gallucci , Robert Hossan , Daniel F. Lowery
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： C08G73/1046 , C08G73/1003 , C08G73/1064
摘要： The disclosure relates to a steam stripping process for producing purified polyimides, e.g., polyetherimide homopolymers and polyetherimide copolymers. The process can include contacting an initial polyimide with steam to remove a volatile species from the initial polyimide to produce a purified polyimide. The purified polyimide can have a weight average molecular weight of from 5,000 to 80,000 Daltons. The weight average molecular weight of the purified polyimide can be greater than or equal to 90% of the weight average molecular weight of the initial polyimide. The purified polyimide can have less than 44 ppm of a volatile species, having a molecular weight of less than 250 Daltons. The polyimide can have less than 10 ppm of a metal cation.
摘要翻译：本公开涉及用于生产纯化的聚酰亚胺的蒸汽汽提方法，例如聚醚酰亚胺均聚物和聚醚酰亚胺共聚物。该方法可以包括使初始聚酰亚胺与蒸汽接触以从初始聚酰亚胺中除去挥发性物质以产生纯化的聚酰亚胺。纯化的聚酰亚胺可以具有5,000至80,000道尔顿的重均分子量。纯化的聚酰亚胺的重均分子量可以大于或等于初始聚酰亚胺的重均分子量的90％。纯化的聚酰亚胺可以具有小于44ppm的分子量小于250道尔顿的挥发性物质。聚酰亚胺可以具有小于10ppm的金属阳离子。

2. 发明申请

US20130108854A1 SOLVENTLESS PROCESS FOR THE PREPARATION OF AMINE FUNCTIONAL POLYETHERIMIDE RESINS WITH IMPROVED MELT FLOW 有权
标题翻译：用于制备具有改进的熔融流动的胺功能性聚己酰胺树脂的无溶剂方法
公开(公告)号：US20130108854A1
公开(公告)日：2013-05-02
申请号：US13286093
申请日：2011-10-31
申请人： Robert R. Gallucci , Roy Odle , Daniel F. Lowery , Richard Peters
发明人： Robert R. Gallucci , Roy Odle , Daniel F. Lowery , Richard Peters
IPC分类号： B32B5/00 , C08G75/23 , D02G3/00 , C08G73/10
CPC分类号： C08G73/1071 , C08G73/10 , C08G73/1017 , C08G73/1028 , C08G73/1046 , C08G73/1053 , C08G73/106 , C08G73/1064 , C08G75/23 , C08G77/382 , C08L79/08 , D01D5/08 , D01F6/74 , D01F6/78 , D04H1/4326 , Y10T428/249921 , Y10T428/2933 , Y10T428/2969
摘要： The disclosure relates to a process that includes blending a polyimide resin and a primary alky amine organic compound to produce an aryl amine functionalized polyimide, having aryl amine functionality in excess of any anhydride functionality. The polyimide resin can have a weight average molecular weight (Mw) from 5,000 to 100,000 daltons. The organic compound can include at least one primary aliphatic amine without a direct linkage of a nitrogen to an aryl group and without a functionality selected from a halogen functionality, a hydroxyl functionality, a sulfonic acid functionality, a sulfonic acid salt functionality, and combinations thereof. The disclosure also relates to alkyl imide functionalized polyimides also with aryl amine functionalized polyimides, having aryl amine functionality in excess of any anhydride functionality and articles produced therefrom.
摘要翻译：本公开涉及一种方法，其包括将聚酰亚胺树脂和伯烷基胺有机化合物混合以制备芳基胺官能化聚酰亚胺，其芳基胺官能度超过任何酸酐官能度。聚酰亚胺树脂的重均分子量（Mw）可以为5,000至100,000道尔顿。有机化合物可以包括至少一种伯脂族胺，而不将氮直接连接到芳基上，而不具有选自卤素官能团，羟基官能团，磺酸官能团，磺酸盐官能团及其组合的官能团。本公开还涉及具有芳基胺官能化聚酰亚胺的烷基酰亚胺官能化聚酰亚胺，其具有超过任何酸酐官能团的芳基胺官能团和由其制备的制品。

3. 发明授权

US08722187B2 Solventless process for the preparation of amine functional polyetherimide resins with improved melt flow 有权
标题翻译：用于制备具有改进的熔体流动的胺官能聚醚酰亚胺树脂的无溶剂方法
公开(公告)号：US08722187B2
公开(公告)日：2014-05-13
申请号：US13286093
申请日：2011-10-31
申请人： Robert R. Gallucci , Roy Odle , Daniel F. Lowery , Richard Peters
发明人： Robert R. Gallucci , Roy Odle , Daniel F. Lowery , Richard Peters
IPC分类号： B32B27/34
CPC分类号： C08G73/1071 , C08G73/10 , C08G73/1017 , C08G73/1028 , C08G73/1046 , C08G73/1053 , C08G73/106 , C08G73/1064 , C08G75/23 , C08G77/382 , C08L79/08 , D01D5/08 , D01F6/74 , D01F6/78 , D04H1/4326 , Y10T428/249921 , Y10T428/2933 , Y10T428/2969
摘要： The disclosure relates to a process that includes blending a polyimide resin and a primary alky amine organic compound to produce an aryl amine functionalized polyimide, having aryl amine functionality in excess of any anhydride functionality. The polyimide resin can have a weight average molecular weight (Mw) from 5,000 to 100,000 daltons. The organic compound can include at least one primary aliphatic amine without a direct linkage of a nitrogen to an aryl group and without a functionality selected from a halogen functionality, a hydroxyl functionality, a sulfonic acid functionality, a sulfonic acid salt functionality, and combinations thereof. The disclosure also relates to alkyl imide functionalized polyimides also with aryl amine functionalized polyimides, having aryl amine functionality in excess of any anhydride functionality and articles produced therefrom.
摘要翻译：本公开涉及一种方法，其包括将聚酰亚胺树脂和伯烷基胺有机化合物混合以制备芳基胺官能化聚酰亚胺，其芳基胺官能度超过任何酸酐官能度。聚酰亚胺树脂的重均分子量（Mw）可以为5,000至100,000道尔顿。有机化合物可以包括至少一种伯脂族胺，而不将氮直接连接到芳基上，而不具有选自卤素官能团，羟基官能团，磺酸官能团，磺酸盐官能团及其组合的官能团。本公开还涉及具有芳基胺官能化聚酰亚胺的烷基酰亚胺官能化聚酰亚胺，其具有超过任何酸酐官能团的芳基胺官能团和由其制备的制品。

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