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1. 发明申请

US20180354923A1 PROCESS FOR THE EPOXIDATION OF AN OLEFIN 审中-公开
公开(公告)号：US20180354923A1
公开(公告)日：2018-12-13
申请号：US15778337
申请日：2016-11-01
申请人： EVONIK DEGUSSA GMBH , THYSSENKRUPP INDUSTRIAL SOLUTIONS AG
发明人： Matthias PASCALY , Manfred BÄRZ , Marc BRENDEL , Robert JAHN , Jürgen SCHEMEL , Michael DOPFER
IPC分类号： C07D301/12 , B01J19/24 , B01J8/04 , B01J29/89
CPC分类号： C07D301/12 , B01J8/0492 , B01J19/2475 , B01J29/89 , B01J2219/0027 , B01J2219/00707 , B01J2219/32279 , C07D303/04
摘要： In a process for the epoxidation of an olefin by continuously reacting the olefin with hydrogen peroxide in a methanol solvent on a fixed bed epoxidation catalyst comprising a titanium zeolite, the hydrogen peroxide is used as an aqueous hydrogen peroxide solution made by an anthraquinone process, the aqueous hydrogen peroxide solution is mixed with methanol to give a feed mixture and this feed mixture is filtered before being contacted with the fixed bed epoxidation catalyst.

2. 发明授权

US10076739B1 Chemical reactor for use with overly reactive chemicals 有权
公开(公告)号：US10076739B1
公开(公告)日：2018-09-18
申请号：US14801004
申请日：2015-07-16
申请人： Precision Combustion, Inc.
发明人： Jeffrey Weissman
IPC分类号： B01J19/00 , B01J19/24 , C07C2/84 , C07C2/58 , C07C29/50
CPC分类号： B01J19/002 , B01D61/145 , B01D63/06 , B01D69/04 , B01D69/145 , B01D2313/22 , B01J19/2475 , B01J19/249 , B01J2219/00076 , B01J2219/00245 , B01J2219/2401 , B01J2219/2454 , B01J2219/246 , B01J2219/2475 , B01J2219/2479 , C07C2/58 , C07C2/84 , C07C29/50 , C07C2521/08 , C07C2523/04 , C07C2523/30 , C07C2523/34 , C07C2529/40 , C07C31/04 , C07C9/16 , C07C11/04
摘要： A chemical reactor for use in a chemical process wherein a reactant and/or a target product is prone to produce undesirable byproducts through secondary reactions. The reactor is configured with a first flow passage for passing a flow of an overly reactive reactant; a permeable first wall for controlled flow of the overly reactive reactant into a second flow passage providing a flow of a second reactant; a permeable second wall having a catalyst supported on an inner surface thereof for catalyzing reaction of the reactants flowing in the second flow passage; the permeable second wall passing through a flow containing the target product; and a non-permeable third wall defining a third flow passage for exiting the product mixture. The reactor can be employed in selective oxidation, oxidative dehydrogenation, and alkylation processes to reduce the formation of byproducts.

3. 发明申请

US20180252686A1 Vortical Thin Film Reactor 审中-公开
公开(公告)号：US20180252686A1
公开(公告)日：2018-09-06
申请号：US15911111
申请日：2018-03-03
申请人： DAVID A. SMITH
发明人： Michael C. Trachtenberg , David A. Smith
IPC分类号： G01N30/42 , B01D11/04 , B04B5/04 , A61M1/36
CPC分类号： G01N30/42 , A61M1/3696 , B01D11/0419 , B01D11/0423 , B01D11/048 , B01D11/0484 , B01J19/1831 , B01J19/1887 , B01J19/1893 , B01J19/243 , B01J19/247 , B01J19/2475 , B01J19/28 , B01J2219/00907 , B04B5/0428 , B04B5/0442 , B04B2005/0457
摘要： We describe vortical thin layer film flow along a spiral channel designed to improve mass and heat transfer efficiency for a multitude of physicochemical reactions and processes. Spiral channels, commonly augmented by centrifugal rotation, support rapid reaction between one or more fluids in a given channel. Dean vortices generate screw-shaped patterns processing axially in the channel, repeatedly refreshing radial interfaces. Fluids self-align, self-assemble, stable, controllable, exhibit thin film geometry. Multiple discrete lamellae can flow with independent velocity separated by density and may be soluble or insoluble in one another. Membranes separating spirals allow other interactions. Energy can be provided and extracted from each flow. Flows can enter or exit independently along the channel length. The pressure within each channel is controlled even when operated at the liquid's vapor pressure. The device is scalable to include a multiplicity of flows in a multiplicity of centrifugally rotating chambers.

4. 发明授权

US09993798B2 Complex comprising oxidative dehydrogenation unit 有权
公开(公告)号：US09993798B2
公开(公告)日：2018-06-12
申请号：US15366277
申请日：2016-12-01
申请人： NOVA Chemicals (International) S.A.
发明人： Vasily Simanzhenkov , Leonid Modestovich Kustov , Aleksey Victorovich Kucherov , Elena Dmitrievna Finashina , Xiaoliang Gao , Edward Christopher Foy , Claire Jeannine Ennis
IPC分类号： B01J19/00 , B01J19/24 , C08F110/02 , C07C5/48 , C07C7/167 , C07C51/16 , C07C67/04 , C07B39/00 , B01J23/28 , B01J23/755 , B01J23/847 , B01J27/02 , B01J27/057 , B01J35/02 , B01J35/06 , B01J35/10 , C07C11/04 , C10G5/04 , C10G9/36 , C10G70/02 , C10G70/04 , C10G70/06
CPC分类号： B01J19/2475 , B01J19/0046 , B01J19/242 , B01J19/245 , B01J23/002 , B01J23/28 , B01J23/755 , B01J23/847 , B01J27/0576 , B01J35/065 , B01J35/1009 , B01J35/1014 , B01J2219/24 , C07B39/00 , C07C5/48 , C07C7/167 , C07C51/16 , C07C67/04 , C08F110/02 , C10G9/36 , C10G27/04 , C10G45/32 , C10G55/04 , C10G70/00 , C10G70/02 , C10G70/046 , C10G70/048 , C10G2300/1081 , C10G2300/4056 , C10G2400/20 , Y02P20/52 , C07C11/04
摘要： Oxidative dehydrogenation of paraffins to olefins provides a lower energy route to produce olefins. Oxidative dehydrogenation processes may be integrated with a number of processes in a chemical plant such as polymerization processes, manufacture of glycols, and carboxylic acids and esters. Additionally, oxidative dehydrogenation processes can be integrated with the back end separation process of a conventional steam cracker to increase capacity at reduced cost.

5. 发明申请

US20180079653A1 AMMONIA SYNTHESIS USING A CATALYTIC NITROGEN-SELECTIVE MEMBRANE 审中-公开
公开(公告)号：US20180079653A1
公开(公告)日：2018-03-22
申请号：US15707007
申请日：2017-09-18
申请人： Jennifer Wilcox , Simona Liguori
发明人： Jennifer Wilcox , Simona Liguori
IPC分类号： C01C1/04 , B01D53/22 , B01D71/02 , B01J35/06 , B01J19/24
CPC分类号： C01C1/0411 , B01D53/228 , B01D67/0072 , B01D69/02 , B01D69/10 , B01D71/022 , B01D71/025 , B01D2256/10 , B01D2257/504 , B01D2258/0283 , B01D2311/2696 , B01D2325/10 , B01J19/2475 , B01J35/065 , C01C1/28 , Y02C10/10 , Y02P20/152 , Y02P20/52
摘要： The invention relates to a metallic membrane for nitrogen separation, the method of making the membrane and methods of using the membrane. The invention also relates to a metallic membrane for disassociation of nitrogen and subsequent reaction with hydrogen to produce ammonia at moderate conditions compared to a conventional Haber-Bosch process.

6. 发明授权

US09908777B2 Method and system for enhancing the mass transfer rate of a soluble gas 有权
公开(公告)号：US09908777B2
公开(公告)日：2018-03-06
申请号：US14782343
申请日：2014-04-15
申请人： Ohio University
发明人： David James Bayless
IPC分类号： C01B31/00 , B01J23/755 , B01J23/06 , B01J35/06 , B01J19/24 , B01D53/14 , B01D53/18 , B01D53/62
CPC分类号： C01B32/00 , B01D53/1475 , B01D53/18 , B01D53/62 , B01D2251/304 , B01D2251/604 , B01D2252/103 , B01D2255/20753 , B01D2255/20792 , B01J19/2475 , B01J23/06 , B01J23/755 , B01J35/065 , B01J2219/24 , Y02C10/06 , Y02P20/152
摘要： A method for enhancing the mass transfer rate of a soluble gas from a gaseous phase to an aqueous phase using a membrane including a catalyst. The method comprises wetting the membrane with a liquid such that a film of the liquid forms on at least a portion of the membrane, the film contacting at least a portion of the catalyst. The method further comprises exposing the wetted membrane to at least one soluble gas, wherein at least a portion of the soluble gas dissolves into the liquid.

7. 发明授权

US09738532B2 Method for the preparation of silanes 有权
公开(公告)号：US09738532B2
公开(公告)日：2017-08-22
申请号：US14782247
申请日：2014-02-28
申请人： Juergen Erwin Lang , Hartwig Rauleder , Ekkehard Mueh
发明人： Juergen Erwin Lang , Hartwig Rauleder , Ekkehard Mueh
IPC分类号： C01B33/04 , B01J12/00 , C07F7/02 , B01J19/24
CPC分类号： C01B33/04 , B01J12/00 , B01J19/088 , B01J19/2475 , B01J2219/00164 , B01J2219/0875 , B01J2219/0896 , B01J2219/24 , C01B33/046 , C07F7/02
摘要： The invention relates to a process for preparing dimeric and/or trimeric silanes by conversion of monosilane in a plasma and to a plant for performance of the process.

8. 发明申请

US20170210849A1 Method Of Forming An Organosilicon Product Using A Membrane Contactor To React A Gas And Liquid 审中-公开
公开(公告)号：US20170210849A1
公开(公告)日：2017-07-27
申请号：US15316272
申请日：2015-06-09
申请人： Dow Corning Corporation
发明人： DONGCHAN AHN , PAUL C. DINH , MICHAEL S. FERRITTO , DON L. KLEYER , JAMES F. THOMPSON
IPC分类号： C08G65/336 , B01J19/02 , B01J19/24
CPC分类号： C08G65/336 , B01D69/08 , B01D71/70 , B01D2325/04 , B01J19/02 , B01J19/2475 , B01J2219/0295 , C08G77/06 , C08G77/46 , C08G2650/04
摘要： Various embodiments disclosed relate to method of forming organosilicon products. In various embodiments, the present invention provides a method of forming an organosilicon product that can include contacting a first side of a silicone membrane with a nonvolatile liquid reactant. The method can include contacting a second side of the membrane with a gaseous reactant. The contacting can be sufficient to react the gaseous reactant with the liquid reactant to form an organosilicon product on the first side of the silicone membrane. The silicone membrane can be substantially impermeable to the liquid reactant and substantially permeable to the gaseous reactant.

9. 发明申请

US20170044021A1 METHOD FOR CONTINUOUSLY PREPARING NANO ZINC OXIDE WITH MEMBRANE REACTOR 审中-公开
标题翻译：用膜反应器连续制备纳米氧化锌的方法
公开(公告)号：US20170044021A1
公开(公告)日：2017-02-16
申请号：US15306491
申请日：2014-09-12
申请人： Nanjing University of Technology
发明人： Weihong XING , Zhilong XU , Nanping XU , Zhaoxiang ZHONG , Feng ZHANG
IPC分类号： C01G9/02 , B01J19/24 , B01J14/00
CPC分类号： C01G9/02 , B01J14/00 , B01J19/2415 , B01J19/2475 , B01J2219/00033 , B82Y30/00 , C01P2002/72 , C01P2004/03
摘要： The present invention relaters to a method for continuously preparing a nano zinc oxide with a membrane reactor. A zinc salt solution and a precipitator solution required for the preparation of a zinc oxide are respectively used as dispersion phases, and under the action of a certain pressure, the two reaction solutions respectively penetrate through a membrane tube at a certain rate and disperse quickly under the action of a shear force and react, producing a precursor precipitate. A precursor suspension penetrates through the membrane tube continuously and circularly after being pressurized by a pump, and at the same time, deionized water as a washing fluid is added to a suspension storage tank, wherein impurity ions penetrate through membrane pores and are discharged along with the liquid medium; after the concentration of the impurity ions meets requirements, the concentrated solution is discharged continuously and then spray-dried to obtain a basic zinc carbonate precursor powder. The basic zinc carbonate powder is calcined under certain conditions to obtain the nanostructured zinc oxide powder. The continuous preparation and washing of a powder can be achieved by coupling a membrane washing technique with a membrane dispersion technique. The procedure is simple, the structure of zinc oxide is easy to control and the yield is high.
摘要翻译：本发明涉及一种用膜反应器连续制备纳米氧化锌的方法。分别使用锌盐溶液和制备氧化锌所需的沉淀剂溶液作为分散相，并且在一定压力的作用下，两种反应溶液分别以一定速率穿过膜管并快速分散在剪切力的作用并反应，产生前体沉淀。前驱体悬浮液在被泵加压之后，连续循环地穿过膜管，同时将去离子水作为洗涤液加入到悬浮储罐中，其中杂质离子穿过膜孔并与液体介质; 杂质离子浓度满足要求后，浓缩溶液连续排出，然后喷雾干燥，得到碱式碳酸锌前体粉末。碱性碳酸锌粉末在一定条件下煅烧得到纳米结构氧化锌粉末。通过将膜洗涤技术与膜分散技术结合可以实现粉末的连续制备和洗涤。操作简单，氧化锌结构易于控制，产量高。

10. 发明授权

US09539558B2 Hydrogen membrane separator 有权
标题翻译：氢分离膜
公开(公告)号：US09539558B2
公开(公告)日：2017-01-10
申请号：US14519735
申请日：2014-10-21
申请人： Intelligent Energy Limited , The Commissariat a L'energie Atomique et Aux Energies Alternatives
发明人： Andrew J. Curello , Michael Curello , Constance R. Stepan
IPC分类号： B01D19/00 , H01M8/06 , B01D53/22 , B01J19/00 , B01D63/06 , B01D67/00 , B01D69/02 , B01D69/12 , B01D71/26 , B01D71/32 , B01D71/34 , B01D71/36 , B01J7/02 , B01J19/24 , C01B3/06 , H01M8/04
CPC分类号： B01J19/00 , B01D19/0031 , B01D53/22 , B01D53/228 , B01D63/06 , B01D67/0088 , B01D69/02 , B01D69/12 , B01D71/26 , B01D71/32 , B01D71/34 , B01D71/36 , B01D2313/16 , B01D2313/90 , B01D2323/04 , B01J7/02 , B01J19/2475 , C01B3/065 , C01B2203/041 , C01B2203/066 , H01M8/04089 , H01M8/04208 , H01M8/065 , H01M8/0687 , Y02E60/324 , Y02E60/362 , Y02E60/364
摘要： The present application is directed to a hydrophobic membrane assembly (28) used within a gas-generating apparatus. Hydrogen is separated from the reaction solution by passing through a hydrophobic membrane assembly (28) having a hydrophobic lattice like member (36) disposed within a hydrogen output composite (32) further enhancing the ability of the hydrogen output composite's ability to separate out hydrogen gas and prolonging its useful life.
摘要翻译：本申请涉及在气体发生设备内使用的疏水膜组件（28）。氢通过穿过设置在氢输出复合材料（32）内的具有疏水晶格状构件（36）的疏水膜组件（28）与反应溶液分离，进一步提高氢输出复合材料分离出氢气的能力并延长其使用寿命。

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