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1. 发明授权

US08262957B2 Ceramic porous body with communication macropores and process for producing the ceramic porous body 有权
标题翻译：具有连通大孔的陶瓷多孔体和陶瓷多孔体的制造方法
公开(公告)号：US08262957B2
公开(公告)日：2012-09-11
申请号：US12527924
申请日：2008-02-20
申请人： Manabu Fukushima , Masayuki Nakata , Yuichi Yoshizawa
发明人： Manabu Fukushima , Masayuki Nakata , Yuichi Yoshizawa
IPC分类号： B29C65/00 , C04B38/00
CPC分类号： B28B1/007 , B28B11/243 , C04B35/111 , C04B35/486 , C04B35/565 , C04B35/6263 , C04B35/63444 , C04B38/062 , C04B2103/0053 , C04B2103/445 , C04B2235/3217 , C04B2235/3244 , C04B2235/3826 , C04B2235/5409 , C04B2235/5445 , C04B2235/6023 , C04B2235/606 , C04B2235/96 , C04B35/00 , C04B38/0045 , C04B38/0051 , C04B38/0058 , C04B38/0074 , C04B38/061 , C04B38/0605
摘要： The present invention is a method for producing a ceramic porous body with high porosity and continuous macropores, which comprises mixing a ceramic powder with an aqueous solution of a gelable water-soluble polymer to form a slurry, gelling for a while to fix the tissue structure, freezing it to produce ice crystals in the gel tissue and creating structures that become continuous pores, thawing the ice by controlled atmospheric substitution-type drying method with the resulting water being replaced without damaging the gel, and then sintering it to produce a ceramic porous body having various porosities, pore diameters and pore shapes, while conventionally cracks and contraction were likely to occur during drying when the solids concentration of the slurry is less than 20 vol %, with the method of the present invention it is possible to control these problems even at a solids concentration of 10 vol % or less, manufacture and provide a ceramic porous body with a porosity of 72% to 99% and a compression strength of 0.4 MPa or more.
摘要翻译：本发明是一种生产具有高孔隙率和连续大孔的陶瓷多孔体的方法，其包括将陶瓷粉末与可凝胶化的水溶性聚合物的水溶液混合以形成浆料，凝胶化一段时间以固定组织结构，将其冷冻以在凝胶组织中产生冰晶，并产生变成连续孔的结构，通过受控的大气取代型干燥方法解冻冰，所得到的水被更换而不损坏凝胶，然后烧结以产生陶瓷多孔具有各种孔隙率，孔径和孔形状的物体，而当浆料的固体浓度小于20体积％时，在干燥期间可能发生常规的裂缝和收缩，采用本发明的方法可以控制这些问题即使固体浓度为10体积％以下，制造并提供孔隙率为72％〜99％的陶瓷多孔体，压缩强度为0.4MPa以上。

2. 发明申请

US20120121498A1 MESOPOROUS CARBON MATERIALS 有权
标题翻译：多孔碳材料
公开(公告)号：US20120121498A1
公开(公告)日：2012-05-17
申请号：US13353722
申请日：2012-01-19
申请人： Sheng Dai , Xiqing Wang
发明人： Sheng Dai , Xiqing Wang
IPC分类号： C01B31/02
CPC分类号： C04B38/0022 , C01B32/00 , C04B35/524 , C04B35/62218 , C04B2111/00793 , C04B2111/0081 , C04B2111/00853 , C04B2235/48 , Y10S977/755 , Y10T428/24165 , Y10T428/249967 , Y10T428/249978 , Y10T428/249979 , C04B38/0054 , C04B38/062
摘要： The invention is directed to a method for fabricating a mesoporous carbon material, the method comprising subjecting a precursor composition to a curing step followed by a carbonization step, the precursor composition comprising: (i) a templating component comprised of a block copolymer, (ii) a phenolic compound or material, (iii) a crosslinkable aldehyde component, and (iv) at least 0.5 M concentration of a strong acid having a pKa of or less than −2, wherein said carbonization step comprises heating the precursor composition at a carbonizing temperature for sufficient time to convert the precursor composition to a mesoporous carbon material. The invention is also directed to a mesoporous carbon material having an improved thermal stability, preferably produced according to the above method.
摘要翻译：本发明涉及一种制备中孔碳材料的方法，所述方法包括使前体组合物经历固化步骤，随后进行碳化步骤，所述前体组合物包含：（i）由嵌段共聚物组成的模板组分，（ii ）酚类化合物或材料，（iii）可交联的醛组分，和（iv）至少0.5M浓度的pKa或小于-2的强酸，其中所述碳化步骤包括在碳化作用下加热前体组合物温度足以将前体组合物转化成介孔碳材料。本发明还涉及具有改进的热稳定性的中孔碳材料，优选根据上述方法制备。

3. 发明授权

US07850942B2 Porous carbons 有权
标题翻译：多孔碳
公开(公告)号：US07850942B2
公开(公告)日：2010-12-14
申请号：US11800805
申请日：2007-05-07
申请人： Stephen Robert Tennison , Oleksundr Prokopovych Kozynchenko , Volodymyr Vasyljovych Strelko , Andrew John Blackburn
发明人： Stephen Robert Tennison , Oleksundr Prokopovych Kozynchenko , Volodymyr Vasyljovych Strelko , Andrew John Blackburn
IPC分类号： C09C1/44
CPC分类号： C04B35/524 , C01B32/00 , C01B32/30 , C04B38/0064 , C04B38/009 , C04B2235/77 , Y10T428/24273 , Y10T428/2982 , C04B35/52 , C04B38/0022 , C04B38/0054 , C04B38/062
摘要： A method of making mesoporous carbon beads comprises steps of providing a nucleophilic component such as phenolic compound or phenol condensation prepolymer, dissolving the nucleophilic component in a pore former, together with at least one electrophilic cross-linking agent such as formaldehyde, paraformaldehyde, furfural and hexamethylene tetramine, dispersing the resulting solution into a mineral oil to form beads, condensing both the component and the agent in the presence of the pore former to form beads of porous resin, removing the beads from the mineral oil and carbonizing the beads to form mesoporous carbon beads.
摘要翻译：制备介孔碳珠的方法包括以下步骤：提供亲核成分如酚类化合物或苯酚缩合预聚物，将亲核成分溶解在成孔剂中，以及至少一种亲电性交联剂如甲醛，多聚甲醛，糠醛和六亚甲基四胺，将所得溶液分散到矿物油中以形成珠粒，在成孔剂存在下将组分和试剂两者冷凝以形成多孔树脂珠，从矿物油中除去珠粒并使珠粒碳化以形成中孔碳珠。

4. 发明授权

US07842736B2 Porous carbons 有权
标题翻译：多孔碳
公开(公告)号：US07842736B2
公开(公告)日：2010-11-30
申请号：US11786072
申请日：2007-04-10
申请人： Stephen Robert Tennison , Oleksundr Prokopovych Kozynchenko , Volodymyr Vasyljovych Strelko , Andrew John Blackburn
发明人： Stephen Robert Tennison , Oleksundr Prokopovych Kozynchenko , Volodymyr Vasyljovych Strelko , Andrew John Blackburn
IPC分类号： C08G8/04 , C08J9/12 , C01B31/02
CPC分类号： C04B35/524 , C01B32/00 , C01B32/30 , C04B38/0064 , C04B38/009 , C04B2235/77 , Y10T428/24273 , Y10T428/2982 , C04B35/52 , C04B38/0022 , C04B38/0054 , C04B38/062
摘要： A method is provided for making mesoporous resin. It comprises: (a) providing a nucleophilic component which comprises a phenolic compound or a phenol condensation prepolymer optionally with one or more modifying reagents selected from hydroquinone, resorcinol, urea, aromatic amines and heteroaromatic amines; (b) dissolving the nucleophilic component in a pore former selected from the group consisting of a diol, a diol ether, a cyclic ester, a substituted cyclic ester, a substituted linear amide, a substituted cyclic amide, an amino alcohol and a mixture of any of the above with water, together with at least one electrophilic cross-linking agent selected from the group consisting of formaldehyde, paraformaldehyde, furfural and hexamethylene tetramine; and (c) condensing the nucleophilic component and the electrophilic cross-linking agent in the presence of the pore former to form a porous resin. The resin may be formed in situ by pouring the partially cross-linked resin into hot oil. Mesoporous resin beads are obtained which can be carbonized into mesoporous carbon beads.
摘要翻译：提供了制备介孔树脂的方法。其包括：（a）提供亲核组分，其包含酚类化合物或酚缩合预聚物，任选地含有一种或多种选自氢醌，间苯二酚，脲，芳族胺和杂芳族胺的改性剂; （b）将亲核组分溶解在选自二醇，二醇醚，环酯，取代的环酯，取代的直链酰胺，取代的环状酰胺，氨基醇和上述任何一种与水一起连同至少一种选自甲醛，多聚甲醛，糠醛和六亚甲基四胺的亲电子交联剂; 和（c）在成孔剂存在下将亲核成分和亲电子交联剂缩合形成多孔树脂。可以通过将部分交联的树脂倒入热油中来原位形成树脂。获得可以碳化成介孔碳珠的介孔树脂珠。

5. 发明申请

US20100035058A1 Porous carbons 审中-公开
标题翻译：多孔碳
公开(公告)号：US20100035058A1
公开(公告)日：2010-02-11
申请号：US12459554
申请日：2009-07-01
申请人： Stephen Robert Tennison , Oleksundr Prokopovych Kozynchenko , Volodymyr Vasyljovych Strelko , Andrew John Blackburn
发明人： Stephen Robert Tennison , Oleksundr Prokopovych Kozynchenko , Volodymyr Vasyljovych Strelko , Andrew John Blackburn
IPC分类号： C08J9/00 , B32B5/18
CPC分类号： C04B35/524 , C01B32/00 , C01B32/30 , C04B38/0064 , C04B38/009 , C04B2235/77 , Y10T428/24273 , Y10T428/2982 , C04B35/52 , C04B38/0022 , C04B38/0054 , C04B38/062
摘要： A method is provided for making mesoporous resin. It comprises: (a) providing a nucleophilic component which comprises a phenolic compound or a phenol condensation prepolymer optionally with one or more modifying reagents selected from hydroquinone, resorcinol, urea, aromatic amines and heteroaromatic amines; (b) dissolving the nucleophilic component in a pore former selected from the group consisting of a diol, a diol ether, a cyclic ester, a substituted cyclic ester, a substituted linear amide, a substituted cyclic amide, an amino alcohol and a mixture of any of the above with water, together with at least one electrophilic cross-linking agent selected from the group consisting of formaldehyde, paraformaldehyde, furfural and hexamethylene tetramine; and (c) condensing the nucleophilic component and the electrophilic cross-linking agent in the presence of the pore former to form a porous resin. The resin may be formed in situ by pouring the partially cross-linked resin into hot oil. Mesoporous resin beads are obtained which can be carbonised into mesoporous carbon beads.
摘要翻译：提供了制备介孔树脂的方法。其包括：（a）提供亲核组分，其包含酚类化合物或酚缩合预聚物，任选地含有一种或多种选自氢醌，间苯二酚，脲，芳族胺和杂芳族胺的改性剂; （b）将亲核组分溶解在选自二醇，二醇醚，环酯，取代的环酯，取代的直链酰胺，取代的环状酰胺，氨基醇和上述任何一种与水一起连同至少一种选自甲醛，多聚甲醛，糠醛和六亚甲基四胺的亲电子交联剂; 和（c）在成孔剂存在下将亲核成分和亲电子交联剂缩合形成多孔树脂。可以通过将部分交联的树脂倒入热油中而原位形成树脂。得到的介孔树脂珠可以碳化成中孔碳珠。

6. 发明申请

US20080090924A1 Porous carbons 审中-公开
公开(公告)号：US20080090924A1
公开(公告)日：2008-04-17
申请号：US11786073
申请日：2007-04-10
申请人： Stephen Tennison , Oleksundr Kozynchenko , Volodymyr Strelko , Andrew Blackburn
发明人： Stephen Tennison , Oleksundr Kozynchenko , Volodymyr Strelko , Andrew Blackburn
IPC分类号： C08G63/00
CPC分类号： C04B35/524 , C01B32/00 , C01B32/30 , C04B38/0064 , C04B38/009 , C04B2235/77 , Y10T428/24273 , Y10T428/2982 , C04B35/52 , C04B38/0022 , C04B38/0054 , C04B38/062
摘要： A method is provided for making mesoporous resin. It comprises: (a) providing a nucleophilic component which comprises a phenolic compound or a phenol condensation prepolymer optionally with one or more modifying reagents selected from hydroquinone, resorcinol, urea, aromatic amines and heteroaromatic amines; (b) dissolving the nucleophilic component in a pore former selected from the group consisting of a diol, a diol ether, a cyclic ester, a substituted cyclic ester, a substituted linear amide, a substituted cyclic amide, an amino alcohol and a mixture of any of the above with water, together with at least one electrophilic cross-linking agent selected from the group consisting of formaldehyde, paraformaldehyde, furfural and hexamethylene tetramine; and (c) condensing the nucleophilic component and the electrophilic cross-linking agent in the presence of the pore former to form a porous resin. The resin may be formed in situ by pouring the partially cross-linked resin into hot oil. Mesoporous resin beads are obtained which can be carbonised into mesoporous carbon beads.

7. 发明申请

US20080063591A1 POROUS CARBON MATERIAL AND METHOD OF MANUFACTURING THE SAME 有权
标题翻译：多孔碳材料及其制造方法
公开(公告)号：US20080063591A1
公开(公告)日：2008-03-13
申请号：US11852009
申请日：2007-09-07
申请人： Dong-min Im , Jeong-hee Lee , Yong-nam Ham , Chan-ho Pak
发明人： Dong-min Im , Jeong-hee Lee , Yong-nam Ham , Chan-ho Pak
IPC分类号： C01B31/02 , C01B31/00
CPC分类号： C04B38/062 , B01J21/18 , B01J23/755 , B01J32/00 , B01J35/1014 , B01J35/1061 , C04B2111/0081 , H01M4/133 , H01M4/587 , H01M4/9083 , Y10S977/70 , C04B35/524
摘要： Porous carbon materials and methods of manufacturing the same are provided. One method includes forming a carbon-metal oxide composite by heating a coordination polymer to form a carbon-metal oxide composite, and then removing the metal oxide from the carbon-metal oxide composite. The porous carbon material has an average pore diameter ranging from about 10 nm to about 100 nm, and a d002 ranging from about 3.35 to 3.50 Å.
摘要翻译：提供了多孔碳材料及其制造方法。一种方法包括通过加热配位聚合物形成碳 - 金属氧化物复合物，然后从碳 - 金属氧化物复合物中除去金属氧化物，形成碳 - 金属氧化物复合物。多孔碳材料的平均孔径为约10nm至约100nm，d 002 002范围为约3.35至3.50。

8. 发明申请

US20080032092A1 Porous carbons 审中-公开
标题翻译：多孔碳
公开(公告)号：US20080032092A1
公开(公告)日：2008-02-07
申请号：US11786074
申请日：2007-04-10
申请人： Stephen Tennison , Oleksundr Kozynchenko , Volodymyr Strelko , Andrew Blackburn
发明人： Stephen Tennison , Oleksundr Kozynchenko , Volodymyr Strelko , Andrew Blackburn
IPC分类号： B32B3/10
CPC分类号： C04B35/524 , C01B32/00 , C01B32/30 , C04B38/0064 , C04B38/009 , C04B2235/77 , Y10T428/24273 , Y10T428/2982 , C04B35/52 , C04B38/0022 , C04B38/0054 , C04B38/062
摘要： A method is provided for making mesoporous resin. It comprises: (a) providing a nucleophilic component which comprises a phenolic compound or a phenol condensation prepolymer optionally with one or more modifying reagents selected from hydroquinone, resorcinol, urea, aromatic amines and heteroaromatic amines; (b) dissolving the nucleophilic component in a pore former selected from the group consisting of a diol, a diol ether, a cyclic ester, a substituted cyclic ester, a substituted linear amide, a substituted cyclic amide, an amino alcohol and a mixture of any of the above with water, together with at least one electrophilic cross-linking agent selected from the group consisting of formaldehyde, paraformaldehyde, furfural and hexamethylene tetramine; and (c) condensing the nucleophilic component and the electrophilic cross-linking agent in the presence of the pore former to form a porous resin. The resin may be formed in situ by pouring the partially cross-linked resin into hot oil. Mesoporous resin beads are obtained which can be carbonised into mesoporous carbon beads.
摘要翻译：提供了制备介孔树脂的方法。其包括：（a）提供亲核组分，其包含酚类化合物或酚缩合预聚物，任选地含有一种或多种选自氢醌，间苯二酚，脲，芳族胺和杂芳族胺的改性剂; （b）将亲核组分溶解在选自二醇，二醇醚，环酯，取代的环酯，取代的直链酰胺，取代的环状酰胺，氨基醇和上述任何一种与水一起连同至少一种选自甲醛，多聚甲醛，糠醛和六亚甲基四胺的亲电子交联剂; 和（c）在成孔剂存在下将亲核成分和亲电子交联剂缩合形成多孔树脂。可以通过将部分交联的树脂倒入热油中而原位形成树脂。得到的介孔树脂珠可以碳化成中孔碳珠。

9. 发明申请

US20020052662A1 Porous ceramics body for in vivo or in vitro use 失效
标题翻译：用于体内或体外使用的多孔陶瓷体
公开(公告)号：US20020052662A1
公开(公告)日：2002-05-02
申请号：US09973079
申请日：2001-10-10
发明人： Kohichi Imura , Takashi Umezawa , Akihiko Ichikawa , Katsuhiro Chaki
IPC分类号： A61F002/28
CPC分类号： C04B35/447 , A61F2/28 , A61F2002/30011 , A61F2002/30968 , A61F2250/0023 , A61F2310/00293 , A61L24/0036 , A61L24/0042 , A61L24/0063 , C04B38/0064 , C04B38/062 , C04B2111/00836 , C04B38/0054 , C04B38/0058 , C04B38/0074
摘要： A porous ceramics body for in vivo or in vitro luse in which a number of pores are closely distributed in three dimensional directions, adjoining pores thereof being partitioned by wall portions with respective communication ports to bring said adjoining pores into communication with each other such that a series of connected spherical pores are formed therewithin, said porous ceramics body being made of a sintered calcium phosphate body, characterized in that, within said sintered calcium phosphate body, pores each having a diameter of 5 microns (nullm) or more account for 80% or more of all the pores in terms of volume whereas pores having a diameter of less than 5 microns (nullm) account for less than 20% of all the pores in terms of volume as subjected to a mercury porosimeter measurement.
摘要翻译：一种用于体内或体外洗涤的多孔陶瓷体，其中许多孔在三维方向上紧密分布，其邻接的孔被壁部与相应的连通口隔开，以使所述相邻的孔彼此连通，使得所述多孔陶瓷体由磷酸钙烧结体构成，其特征在于，在所述烧结磷酸钙体内，直径为5微米（以上）以上的孔为80％以上，或更多的孔，而直径小于5微米（母体）的孔占经过水银孔隙率计测量的体积方面的所有孔的小于20％。

10. 发明授权

US06345663B1 Core compositions and articles with improved performance for use in castings for gas turbine applications 有权
标题翻译：具有改进性能的核心组合物和制品用于燃气轮机应用的铸件
公开(公告)号：US06345663B1
公开(公告)日：2002-02-12
申请号：US09617013
申请日：2000-07-14
申请人： Frederic Joseph Klug , Robert Arthur Giddings
发明人： Frederic Joseph Klug , Robert Arthur Giddings
IPC分类号： B22D904
CPC分类号： C04B38/0058 , B22C1/22 , C04B35/111 , C04B35/634 , C04B35/63444 , C04B35/65 , C04B2111/00939 , C04B35/10 , C04B38/062
摘要： A method for fabricating a fired ceramic article, a green product, and a fired ceramic article, all for use as a core in the investment casting of directionally solidified eutectic and superalloy material. A ceramic slurry is prepared of alumina, aluminum and a solution of a polymerizable binder in a liquid. The slurry is extruded under low pressure into a closed cavity to form a gelled green product which is subsequently heated in an oxygen-containing atmosphere, wherein the oxygen reacts with the aluminum in the green product to form alumina which advantageously causes an increase in volume of the green product which counters the shrinkage effects of heating. The polymerizable binder is of a type which cross-links with the alumina and upon heating the liquid component of such binder vaporizes and the remaining polymer component subsequently gasifies on further heating to leave desired interstitial pores within the green product, which assist in allowing the oxygen to permeate the green product, which assists in oxidation of the aluminum through the green product. The green product is thereafter sintered to form a substantially dimensionally precise ceramic article suitable for precision-casting of superalloy materials.
摘要翻译：一种烧制陶瓷制品，绿色产品和烧制陶瓷制品的制造方法，全部用作定向凝固的共晶和超合金材料的熔模铸造中的核心。制备氧化铝，铝和可聚合粘合剂在液体中的溶液的陶瓷浆料。将浆料在低压下挤压成封闭的空腔以形成凝胶状绿色产品，随后在含氧气氛中加热，其中氧气与绿色产品中的铝反应形成氧化铝，这有利地导致体积增加这是绿色产品，反映了加热的收缩效应。可聚合粘合剂是与氧化铝交联并且在加热这种粘合剂的液体组分时蒸发的类型，并且剩余的聚合物组分随后在进一步加热下气化以在绿色产品内留下所需的间隙，这有助于允许氧渗透绿色产品，这有助于通过绿色产品氧化铝。然后将绿色产品烧结以形成适用于超级合金材料的精密铸造的基本尺寸精确的陶瓷制品。

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