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1. 发明申请

US20170174607A1 METHODS OF PREPARING a,ß-UNSATURATED OR a-HALO KETONES AND ALDEHYDES 审中-公开
公开(公告)号：US20170174607A1
公开(公告)日：2017-06-22
申请号：US15382782
申请日：2016-12-19
申请人： International Flavors & Fragrances Inc.
发明人： Ian R. Baxendale , James S. Sharley , Amadeo Fernández Miranda , Ana Maria Collado Pérez
IPC分类号： C07C67/317 , C07C67/00 , C07C45/27
CPC分类号： C07C67/317 , C07C45/27 , C07C45/54 , C07C67/00 , C07C67/313 , C07C2101/08 , C07C2101/10 , C07C2101/14 , C07C2101/16 , C07C2102/08 , C07C2601/08 , C07C2601/10 , C07C2601/14 , C07C2601/16 , C07C2602/08 , C07C69/73 , C07C69/145 , C07C69/157 , C07C69/757 , C07C69/738 , C07C49/597 , C07C49/683 , C07C49/687 , C07C49/457 , C07C49/697 , C07C49/227 , C07C47/353
摘要： Copper(II) bromide mediated oxidation of acylated enol and use of the reaction in the synthesis of α,β-unsaturated or α-bromo ketones or aldehydes are disclosed. The method provides an efficient and practical process for manufacturing dehydrohedione (DHH) and many other versatile α,β-unsaturated or α-bromo ketones or aldehydes in large scales to avoid using precious metal compounds.

2. 发明授权

US09650322B2 Method for producing alkoxyhydroxybenzaldehyde 有权
公开(公告)号：US09650322B2
公开(公告)日：2017-05-16
申请号：US15150028
申请日：2016-05-09
申请人： Rhodia Operations
发明人： Laurent Garel
IPC分类号： C07C45/00 , C07C51/00 , C07C41/16 , C07C41/42 , C07C45/54 , C07C51/367
CPC分类号： C07C41/16 , C07C41/42 , C07C45/54 , C07C51/367 , Y02P20/582 , C07C43/23 , C07C59/64 , C07C47/58
摘要： Processes may include producing at least one alkoxyhydroxybenzaldehyde compound from at least one hydroxyphenol compound, wherein processes include the steps of: (i) synthetizing at least one alkoxyphenol from said at least one hydroxyphenol in the presence of at least one O-alkylating agent; (ii) recovering said at least one alkoxyphenol and impurities, wherein said impurities includes a dialkoxybenzene compound; (iii) separating said dialkoxybenzene from the alkoxyphenol; (iv) condensing the alkoxyphenol with glyoxylic acid and obtaining the corresponding mandelic compound; (v) oxidizing said mandelic compound to give the corresponding alkoxyhydroxy-benzaldehyde; and (vi) recovering said alkoxyhydroxybenzaldehyde.

3. 发明申请

US20170044084A1 METHOD OF PRODUCING FARNESYL ACETONE 审中-公开
标题翻译：生产丙烯腈的方法
公开(公告)号：US20170044084A1
公开(公告)日：2017-02-16
申请号：US15307081
申请日：2015-04-29
申请人： BASF SE
发明人： Mathias SCHELWIES , Rocco PACIELLO , Heinz ECKHARDT , Martine DEHN
IPC分类号： C07C45/69
CPC分类号： C07C45/69 , C07C45/54 , C07C45/62 , C07C49/04 , C07C49/203
摘要： The present invention relates to a process for preparing farnesyl acetone.
摘要翻译：本发明涉及制备法呢基丙酮的方法。

4. 发明申请

US20160318836A1 PROCESS FOR THE PRODUCTION OF 2,6-DIMETHYLHEPT-5-ENAL BY BAEYER-VILLIGER OXIDATION 审中-公开
标题翻译：通过BAEYER-VILLIGER氧化生产2,6-二甲基-5-ENAL的方法
公开(公告)号：US20160318836A1
公开(公告)日：2016-11-03
申请号：US15103592
申请日：2015-01-22
申请人： GIVAUDAN SA
发明人： Alan John CHALK , Andreas GOEKE , Martin Alan LOVCHIK
IPC分类号： C07C45/54 , C07C67/44
CPC分类号： C07C45/54 , C07C67/44 , C07C47/21
摘要： Disclosed is a process for the production of 2,6-dimethylhept-5-enal by Baeyer-Villiger oxidation of 3,7-dimethylocta-2,6-dienal in the presence of aqueous H2O2 and SeO2, followed by hydrolysis.
摘要翻译：公开了在H 2 O 2和SeO 2水溶液存在下，通过Baeyer-Villiger氧化3,7-二甲基辛-2,6-二烯的2,6-二甲基庚-5-烯醛的方法，然后进行水解。

5. 发明授权

US09334216B2 Method for producing alkoxyphenol and alkoxy-hydroxybenzaldehyde 有权
标题翻译：制备烷氧基苯酚和烷氧基 - 羟基苯甲醛的方法
公开(公告)号：US09334216B2
公开(公告)日：2016-05-10
申请号：US14417015
申请日：2013-07-12
申请人： RHODIA OPERATIONS
发明人： Laurent Garel
IPC分类号： C07C45/38 , C07C51/353 , C07C41/06 , C07C41/16 , C07C51/367 , C07C45/54
CPC分类号： C07C45/38 , C07C41/06 , C07C41/16 , C07C45/54 , C07C51/353 , C07C51/367 , Y02P20/582 , C07C43/23 , C07C59/64 , C07C47/58 , C07C47/575
摘要： The invention relates to a method for producing alkoxyphenol from hydroxyphenol, comprising an O-alkylation reaction of at least one hydroxyphenol into at least one alkoxyphenol, said reaction being carried out using an O-alkylating agent, an aqueous solvent containing a Bröensted base, and an organic solvent, with a base/O-alkylating agent ratio of between 0.5 and 1.5 in moles of base per mole of O-alkylating agent, an O-alkylating agent/hydroxyphenol ratio of between 0.5 and 2 moles of O-alkylating agent per mole of hydroxyphenol, and an organic solvent/hydroxyphenol ratio of less than 280 mL, preferably between 10 and 250 mL and more preferably still between 50 and 150 mL of organic solvent per mole of hydroxyphenol. The invention also relates to a method for producing at least one alkoxy-hydroxybenzaldehyde from at least one hydroxyphenol compound.
摘要翻译：本发明涉及一种由羟基苯酚生产烷氧基苯酚的方法，其中包括至少一种羟基苯酚与至少一种烷氧基苯酚的O-烷基化反应，所述反应使用O-烷基化试剂，含有布朗斯台德碱的含水溶剂和一种有机溶剂，碱/ O-烷基化剂的比例为每摩尔O-烷基化剂0.5至1.5摩尔碱，O-烷基化剂/羟基苯酚的比例为0.5-2摩尔的O-烷基化剂/ 摩尔的羟基苯酚，有机溶剂/羟基苯酚的比例小于280mL，优选为10至250mL，更优选为50至150mL有机溶剂/摩尔羟基苯酚。本发明还涉及从至少一种羟基苯酚化合物制备至少一种烷氧基 - 羟基苯甲醛的方法。

6. 发明申请

US20150183702A1 METHOD FOR PRODUCING ALKOXYPHENOL AND ALKOXY-HYDROXYBENZALDEHYDE 有权
标题翻译：生产烷基酚和羟基 - 羟基苯甲醛的方法
公开(公告)号：US20150183702A1
公开(公告)日：2015-07-02
申请号：US14417015
申请日：2013-07-12
申请人： RHODIA OPERATIONS
发明人： Laurent Garel
IPC分类号： C07C45/38 , C07C51/353 , C07C41/06
CPC分类号： C07C45/38 , C07C41/06 , C07C41/16 , C07C45/54 , C07C51/353 , C07C51/367 , Y02P20/582 , C07C43/23 , C07C59/64 , C07C47/58 , C07C47/575
摘要： The invention relates to a method for producing alkoxyphenol from hydroxyphenol, comprising an O-alkylation reaction of at least one hydroxyphenol into at least one alkoxyphenol, said reaction being carried out using an O-alkylating agent, an aqueous solvent containing a Bröensted base, and an organic solvent, with a base/O-alkylating agent ratio of between 0.5 and 1.5 in moles of base per mole of O-alkylating agent, an O-alkylating agent/hydroxyphenol ratio of between 0.5 and 2 moles of O-alkylating agent per mole of hydroxyphenol, and an organic solvent/hydroxyphenol ratio of less than 280 mL, preferably between 10 and 250 mL and more preferably still between 50 and 150 mL of organic solvent per mole of hydroxyphenol. The invention also relates to a method for producing at least one alkoxy-hydroxybenzaldehyde from at least one hydroxyphenol compound.
摘要翻译：本发明涉及一种由羟基苯酚生产烷氧基苯酚的方法，其中包括至少一种羟基苯酚与至少一种烷氧基苯酚的O-烷基化反应，所述反应使用O-烷基化试剂，含有布朗斯台德碱的含水溶剂和一种有机溶剂，碱/ O-烷基化剂的比例为每摩尔O-烷基化剂0.5至1.5摩尔碱，O-烷基化剂/羟基苯酚的比例为0.5-2摩尔的O-烷基化剂/ 摩尔的羟基苯酚，有机溶剂/羟基苯酚的比例小于280mL，优选为10至250mL，更优选为50至150mL有机溶剂/摩尔羟基苯酚。本发明还涉及从至少一种羟基苯酚化合物制备至少一种烷氧基 - 羟基苯甲醛的方法。

7. 发明授权

US08987497B2 Process for the oxidation of organic carbonyl compounds 有权
标题翻译：有机羰基化合物的氧化方法
公开(公告)号：US08987497B2
公开(公告)日：2015-03-24
申请号：US14072179
申请日：2013-11-05
申请人： BASF SE
发明人： Nicolas Vautravers , Joaquim Henrique Teles , Andrei-Nicolae Parvulescu , Ulrich Müller
IPC分类号： C07C69/74 , C07D313/04 , C07C51/285 , C07D309/30 , C07D313/00 , B01J23/00 , C07C45/54
CPC分类号： C07D313/04 , B01J23/00 , C07C45/54 , C07C51/285 , C07D309/30 , C07D313/00 , C07C47/21 , C07C57/03
摘要： A process for the oxidation of an organic carbonyl compound comprising reacting the organic carbonyl compound, optionally in the presence of a solvent, with hydrogen peroxide in the presence of a catalyst comprising a tin-containing zeolitic material having an MWW-type framework structure.
摘要翻译：一种有机羰基化合物的氧化方法，包括有机羰基化合物，任选在溶剂存在下，在含有具有MWW型骨架结构的含锡沸石材料的催化剂存在下，与过氧化氢反应。

8. 发明申请

US20140114091A1 METHOD FOR PREPARING 3,3-DIMETHYLBUTYRALDEHYDE 有权
标题翻译：制备3,3-二甲基二氢呋喃的方法
公开(公告)号：US20140114091A1
公开(公告)日：2014-04-24
申请号：US14144452
申请日：2013-12-30
申请人： Jinan Chenghuishuangda Chemical Industry Co., Ltd.
发明人： Junfeng HU , Donghai YU , Qingqian JIANG , Yanjun YANG
IPC分类号： C07C45/41
CPC分类号： C07C45/41 , C07C45/52 , C07C45/54 , C07C67/293 , C07C69/63 , C07C47/02
摘要： A method for preparing 3,3-dimethylbutyraldehyde. The method includes: providing t-butyl chloride and vinyl acetate as raw materials, conducting a catalytic reaction between the t-butyl chloride and vinyl acetate to yield 1-chloro-3,3-dimethyl butyl acetate in the presence of a catalyst, the weight ratio of t-butyl chloride to vinyl acetate being 1: 0.84-0.93; and controlling a temperature at between 100 and 110° C. for conducting hydrolytic disproportionation of 1-chloro-3,3-dimethyl butyl acetate in the presence of the catalyst to yield a mixture comprising 3,3-dimethylbutyraldehyde; and purifying the mixture by distillation to yield 3,3-dimethylbutyraldehyde, in which, the catalyst is aluminum trichloride, p-toluene sulphonic acid, or iron trichloride.
摘要翻译：制备3,3-二甲基丁醛的方法。该方法包括：以叔丁基氯和乙酸乙烯酯为原料，在叔丁基氯与乙酸乙烯之间进行催化反应，得到1-氯-3,3-二甲基丁酸乙酯，在催化剂存在下，叔丁基氯与乙酸乙烯酯的重量比为1:0.84-0.93; 并控制温度在100至110℃之间，以在催化剂存在下进行1-氯-3,3-二甲基丁酸乙酯的水解歧化，得到包含3,3-二甲基丁醛的混合物; 并通过蒸馏纯化混合物，得到3,3-二甲基丁醛，其中催化剂为三氯化铝，对甲苯磺酸或三氯化铁。

9. 发明授权

US08362306B2 Energy densification of biomass-derived organic acids 有权
标题翻译：生物质衍生的有机酸的能量致密化
公开(公告)号：US08362306B2
公开(公告)日：2013-01-29
申请号：US12912387
申请日：2010-10-26
申请人： M. Clayton Wheeler , G. Peter van Walsum , Thomas J. Schwartz , Adriaan van Heiningen
发明人： M. Clayton Wheeler , G. Peter van Walsum , Thomas J. Schwartz , Adriaan van Heiningen
IPC分类号： C07C1/00
CPC分类号： C07C45/54 , C07C5/333 , C07C29/145 , C07C51/412 , C07C11/21 , C07C31/22 , C07C49/12 , C07C59/185
摘要： A process for upgrading an organic acid includes neutralizing the organic acid to form a salt and thermally decomposing the resulting salt to form an energy densified product. In certain embodiments, the organic acid is levulinic acid. The process may further include upgrading the energy densified product by conversion to alcohol and subsequent dehydration.
摘要翻译：有机酸的升级方法包括中和有机酸以形成盐并热分解所得的盐以形成能量致密化产物。在某些实施方案中，有机酸是乙酰丙酸。该方法还可以包括通过转化成醇和随后的脱水来升级能量致密化产物。

10. 发明申请

US20120065347A1 FLUOROCOMPOUND HAVING HIGHLY FLUORINATED NORBORNANE STRUCTURE, FLUOROPOLYMER, AND THEIR PRODUCTION PROCESSES 审中-公开
标题翻译：具有高度氟化的诺贝恩结构，荧光体及其生产工艺的氟化合物
公开(公告)号：US20120065347A1
公开(公告)日：2012-03-15
申请号：US13302824
申请日：2011-11-22
申请人： Yasuhisa MATSUKAWA , Daisuke SHIRAKAWA , Eisuke MUROTANI , Naoko SHIROTA , Yoko TAKEBE
发明人： Yasuhisa MATSUKAWA , Daisuke SHIRAKAWA , Eisuke MUROTANI , Naoko SHIROTA , Yoko TAKEBE
IPC分类号： C08F120/68 , C07C69/753 , C07C53/50 , C07C49/477
CPC分类号： C07C49/477 , C07C29/143 , C07C29/147 , C07C31/44 , C07C35/52 , C07C45/54 , C07C61/40 , C07C67/14 , C07C69/653 , C07C69/753 , C07C2602/42 , C08F220/24
摘要： The present invention provides novel polymers obtained by polymerizing a compound of formula (1) which has a highly fluorinated norbornane structure. The invention also provides compounds represented by formulas (3) and (3A-1) below, as well as the following compounds:
摘要翻译：本发明提供了通过聚合具有高度氟化的降冰片烷结构的式（1）化合物获得的新型聚合物。本发明还提供由下式（3）和（3A-1）表示的化合物以及以下化合物：

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