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1. 发明申请

US20180057685A1 FLAME-RETARDANT RESIN COMPOSITION 审中-公开
公开(公告)号：US20180057685A1
公开(公告)日：2018-03-01
申请号：US15627765
申请日：2017-06-20
申请人： ASAHI KASEI KABUSHIKI KAISHA
发明人： Chihiro MAEDA , Mihoko YAMAMOTO , Akira MITSUI
IPC分类号： C08L71/10 , C07F9/6581 , C08L23/12 , C08L25/06 , C08L77/00
CPC分类号： C08L71/10 , C07F9/145 , C07F9/301 , C07F9/4056 , C07F9/657172 , C07F9/65746 , C07F9/65812 , C08L23/12 , C08L25/06 , C08L71/12 , C08L77/00 , C08L77/06 , C08L2201/02 , C08K5/0066 , C08L81/04 , C08K5/5399 , C08K5/5313
摘要： Provided is a resin composition having excellent flame retardance, molding processability, and post-heat aging flame retardance. A flame-retardant resin composition contains: (A) a polyphenylene ether; (B) at least one thermoplastic resin selected from the group consisting of (B-1) a polystyrene resin, (B-2) a polyamide resin, (B-3) a polypropylene resin, and (B-4) a polyphenylene sulfide resin; and (C) a flame retardant. The (A) component has a content of less than 50 mass % when the flame-retardant resin composition minus ash content is taken to be 100 mass %. The flame-retardant resin composition has a flame retardance level of V-0 as measured by a UL 94 vertical burning test. A molded article formed from the flame-retardant resin composition exhibits a rate of change of chloroform-insoluble content of no greater than 15 mass % before and after being subjected to aging in which the molded article is left for 1,000 hours at 150° C. in an atmospheric environment.

2. 发明授权

US09752010B2 Phosphorus-containing compounds useful for making halogen-free, ignition-resistant polymers 有权
公开(公告)号：US09752010B2
公开(公告)日：2017-09-05
申请号：US15207225
申请日：2016-07-11
申请人： Blue Cube IP LLC
发明人： Anteneh Z. Worku , Michael J. Mullins
IPC分类号： C08K5/51 , C07F9/6571 , C08K5/527 , C08K5/5393 , C08K5/5313 , C09J11/06 , C07F9/28 , C08J5/24 , C09D163/04 , C09J163/04 , H05K1/03 , C08K5/00
CPC分类号： C08K5/51 , C07F9/28 , C07F9/657172 , C07F9/657181 , C08J5/24 , C08J2363/04 , C08K5/0066 , C08K5/527 , C08K5/5313 , C08K5/5393 , C09D163/04 , C09J11/06 , C09J163/04 , H05K1/0353
摘要： A process for making a phosphorus-containing compound is disclosed. The process comprises contacting a compound of formula (A) wherein RA and RB are selected from optionally substituted aryl, aryloxy, alkyl and alkoxy groups or can be combined to form cyclic structures; and RC is methyl, ethyl, isopropyl, n-butyl, i-butyl, t-butyl, phenyl or benzyl; and a compound of formula (B) wherein R1-R4 are selected from optionally substituted aryl, aryloxy, alkyl and alkoxy groups. The phosphorus-containing compound can then be used as a flame retardants for polymers, especially for epoxy, polyurethane, thermosetting resins and thermoplastic polymers. Such flame retardant-containing polymers can be used to make protective coating formulations and ignition-resistant fabricated articles, such as electrical laminates, polyurethane foams, and various molded and/or foamed thermoplastic products.

3. 发明申请

US20170204130A1 FLAME RETARDANTS, PREPARATION METHODS, AND THERMOPLASTIC COMPOSITIONS THEREOF 审中-公开
公开(公告)号：US20170204130A1
公开(公告)日：2017-07-20
申请号：US15314724
申请日：2014-05-30
申请人： E. I. DU PONT DE NEMOURS AND COMPANY
发明人： Xiao Pan , Zhongning Zhang , Gang Zuo
IPC分类号： C07H15/26 , C08K5/5313 , C09K21/12
CPC分类号： C07H15/26 , C07F9/657172 , C08K5/5313 , C09K21/12
摘要： Disclosed are flame retardants comprising compounds of Formula 1, wherein the polyol is a disaccharide or a C12 sugar alcohol, which has at least one glucose or one fructose unit per molecule, R1 is H or CH3; R2 is H or CH3; m is an integer ranging from 6 to 9; and n is an integer ranging from 2 to 9.Also disclosed are methods for producing the inventive flame retardants, thermoplastic compositions and articles comprising the same, and methods for improving flame retardancy of thermoplastic polymers using the same.

4. 发明授权

US09695299B1 Phosphorous-containing compound, application thereof, and method for preparing the same 有权
公开(公告)号：US09695299B1
公开(公告)日：2017-07-04
申请号：US15135802
申请日：2016-04-22
申请人： National Tsing Hua University
发明人： Ying-Ling Liu , Chih-Yuan Hsu
IPC分类号： C09K21/12 , C08K5/53 , C07F9/6571 , C08G79/04
CPC分类号： C08K5/53 , C07F9/657163 , C07F9/657172 , C08G59/02 , C08G59/3272 , C08G65/22 , C08G79/04
摘要： A phosphorous-containing compound is represented by Formula (I): wherein n is an integer ranging from 1 to 4; R1 represents hydrogen or a linear or branched C1-C4 alkyl group, and a plurality of R1s are the same or different when n is larger than 1; R2 represents hydrogen, or wherein Ep is an epoxy resin moiety; or represents wherein Ar represents a linear or branched C1-C12 alkyl group or a C6-C12 aryl group; and R3 represents hydrogen or methyl.

5. 发明申请

US20170022229A1 NOVEL CYCLIC PHOSPHINATE DERIVATIVES AND METHOD OF PREPARING THE SAME 有权
标题翻译：新型环磷酰胺衍生物及其制备方法
公开(公告)号：US20170022229A1
公开(公告)日：2017-01-26
申请号：US15286408
申请日：2016-10-05
申请人： KNU-INDUSTRY COOPERATION FOUNDATION
发明人： Phil Ho LEE , Seo Hyun SHIN , Dong Jin KANG , Da Han EOM , Yea Rin KIM , Yeon Seok JEONG , Won Seok CHOI
IPC分类号： C07F9/6571
CPC分类号： C07F9/657181 , C07F9/657172 , C07F9/65744
摘要： Provided are novel cyclic phosphinate derivatives and a method of preparing the same, and more particularly, cyclic phosphinate derivatives including benzoxaphosphole oxide derivatives and benzoxaphosphorin oxide derivatives, and a method of preparing the same. The cyclic phosphinate derivative according to the present invention may have pharmacological and physiological activities, be used as the basic skeleton of the natural material, and be used in development of a new drug, and synthesis of various medicines. In addition, with the method of preparing a cyclic phosphinate derivative according to the present invention, various cyclic phosphinate derivatives may be prepared with high yield through a simple synthetic process by performing an intramolecular carbon-oxygen coupling reaction on the phosphinic acid derivative in the presence of a palladium (Pd) catalyst, an oxidant, and a base.
摘要翻译：提供新的环状次膦酸盐衍生物及其制备方法，更具体地说，包括苯并氧磷杂环磷氧化物衍生物和苯并氧磷化磷氧化物衍生物的环状次膦酸盐衍生物及其制备方法。根据本发明的环状次膦酸盐衍生物可具有药理和生理活性，可用作天然物质的基本骨架，并用于开发新药物和各种药物的合成。此外，通过制备本发明的环状次膦酸酯衍生物的方法，可以通过简单的合成方法通过在次膦酸衍生物上进行分子内碳 - 氧偶联反应，在存在的情况下以高收率制备各种环状次膦酸酯衍生物的钯（Pd）催化剂，氧化剂和碱。

6. 发明授权

US09493494B2 Phosphinine oxide derivative and preparation method thereof 有权
标题翻译：氧化膦衍生物及其制备方法
公开(公告)号：US09493494B2
公开(公告)日：2016-11-15
申请号：US14473901
申请日：2014-08-29
申请人： KNU-INDUSTRY COOPERATION FOUNDATION
发明人： Phil Ho Lee , Young Chul Park , In Cheol Jeon , Jung Min Seo , Bo Ram Seo
IPC分类号： C07F9/6584 , C07F9/6571
CPC分类号： C07F9/65846 , C07F9/657163 , C07F9/657172 , C07F9/657181
摘要： Provided are a novel phosphinine oxide derivative and a preparation method thereof, and more specifically, the phosphinine oxide derivative includes an oxaphosphinine oxide derivative and an azaphosphinine oxide derivative.The phosphinine oxide derivative according to the present invention may have a pharmacological activity and a physiological activity, and may be used as a basic framework of a natural product and may be used for development of new drug and synthesis of various medical supplies.In addition, according to the preparation method of the phosphinine oxide derivative according to the present invention, various phosphinine oxide derivatives with a high yield may be prepared by a simple synthesis process using an intramolecular annulation between a phosphinic derivative and an alkyne derivative in the presence of a rhodium (Rh) catalyst or a ruthenium (Ru) catalyst and an oxidant.
摘要翻译：此外，根据本发明的次膦氧化物衍生物的制备方法，可以通过使用在次膦酸衍生物和炔衍生物之间的分子内环状的简单的合成方法，在存在下制备具有高产率的各种次膦酰氧化物衍生物的铑（Rh）催化剂或钌（Ru）催化剂和氧化剂。

7. 发明申请

US20160319107A1 PHOSPHORUS-CONTAINING COMPOUNDS USEFUL FOR MAKING HALOGEN-FREE, IGNITION-RESISTANT POLYMERS 有权
标题翻译：用于制备无卤素，耐点火聚合物的含磷化合物有用
公开(公告)号：US20160319107A1
公开(公告)日：2016-11-03
申请号：US15207225
申请日：2016-07-11
申请人： Blue Cube IP LLC
发明人： Anteneh Z. Worku , Michael J. Mullins
IPC分类号： C08K5/51 , C07F9/28 , H05K1/03 , C08J5/24 , C09J163/04 , C07F9/6571 , C09D163/04
CPC分类号： C08K5/51 , C07F9/28 , C07F9/657172 , C07F9/657181 , C08J5/24 , C08J2363/04 , C08K5/0066 , C08K5/527 , C08K5/5313 , C08K5/5393 , C09D163/04 , C09J11/06 , C09J163/04 , H05K1/0353
摘要： A process for making a phosphorus-containing compound is disclosed. The process comprises contacting a compound of formula (A) wherein RA and RB are selected from optionally substituted aryl, aryloxy, alkyl and alkoxy groups or can be combined to form cyclic structures; and RC is methyl, ethyl, isopropyl, n-butyl, i-butyl, t-butyl, phenyl or benzyl; and a compound of formula (B) wherein R1-R4 are selected from optionally substituted aryl, aryloxy, alkyl and alkoxy groups. The phosphorus-containing compound can then be used as a flame retardants for polymers, especially for epoxy, polyurethane, thermosetting resins and thermoplastic polymers. Such flame retardant-containing polymers can be used to make protective coating formulations and ignition-resistant fabricated articles, such as electrical laminates, polyurethane foams, and various molded and/or foamed thermoplastic products.
摘要翻译：公开了一种制备含磷化合物的方法。该方法包括使其中RA和RB选自任选取代的芳基，芳氧基，烷基和烷氧基的式（A）化合物或可以组合形成环状结构; 乙基，异丙基，正丁基，异丁基，叔丁基，苯基或苄基; 和式（B）的化合物，其中R 1 -R 4选自任选取代的芳基，芳氧基，烷基和烷氧基。然后可以将含磷化合物用作聚合物的阻燃剂，特别是用于环氧树脂，聚氨酯，热固性树脂和热塑性聚合物。这种含阻燃剂的聚合物可用于制备保护性涂料配方和耐点火制造品，例如电层压材料，聚氨酯泡沫以及各种模制和/或发泡热塑性产品。

8. 发明授权

US09217061B2 Phosphorus-containing compounds and their preparation process and use 有权
标题翻译：含磷化合物及其制备方法和用途
公开(公告)号：US09217061B2
公开(公告)日：2015-12-22
申请号：US14069059
申请日：2013-10-31
申请人： CHANG CHUN PLASTICS CO., LTD. , NATIONAL CHUNG HSING UNIVERSITY
发明人： Ching-Hsuan Lin , Tsung Li Lin , Yu-Ting Fang , Kuen-Yuan Hwang , An-Pang Tu
IPC分类号： C08G79/02 , C08G59/10 , C08G59/32 , C08G69/26 , C08G73/10 , C08G69/42 , C07F9/6571 , H05K1/03
CPC分类号： C08G69/42 , C07F9/657172 , C08G59/10 , C08G59/3254 , C08G69/26 , C08G73/10 , H05K1/0346 , H05K1/0393
摘要： A series of novel phosphorus-containing compounds having the formula: is provided in which R1-R4, A, Q and m are as defined in the specification. A process for the preparation of the compound of formula (I) is also provided. A polymer of formula (PA), and preparation process and use thereof, as well as a polymer of formula (PI), and preparation process and use thereof are also provided.
摘要翻译：提供了一系列具有下式的新型含磷化合物，其中R1-R4，A，Q和m如说明书中所定义。还提供了制备式（I）化合物的方法。还提供了式（PA）的聚合物及其制备方法和用途，以及式（PI）的聚合物及其制备方法和用途。

9. 发明授权

US09102696B2 Phosphorus-based (meth)acrylate compound and method of preparing the same 有权
标题翻译：磷系（甲基）丙烯酸酯化合物及其制备方法
公开(公告)号：US09102696B2
公开(公告)日：2015-08-11
申请号：US14166230
申请日：2014-01-28
申请人： SANKO CO., LTD.
发明人： Naoki Komiya , Akira Inoue
IPC分类号： C07F9/6571
CPC分类号： C07F9/657172
摘要： This invention relates to a novel compound having high refractive index suitable for use in optical resin materials, etc., without containing a sulfur atom, and to a method of preparing the same, in which the compound is a phosphorus-based (meth)acrylate compound represented by Formula (I).
摘要翻译：本发明涉及一种适用于不含硫原子的光学树脂材料等具有高折射率的新型化合物及其制备方法，其中该化合物为磷系（甲基）丙烯酸酯由式（I）表示的化合物。

10. 发明授权

US09045508B2 Phosphorus-containing oligomer and method for producing the same, curable resin composition and cured product of the same, and printed wiring board 有权
标题翻译：含磷低聚物及其制造方法，固化性树脂组合物及其固化物及印刷电路板
公开(公告)号：US09045508B2
公开(公告)日：2015-06-02
申请号：US13932345
申请日：2013-07-01
申请人： DIC Corporation
发明人： Koji Hayashi , Yutaka Satou
IPC分类号： C07F9/6574 , C07F9/30 , C07F9/6571 , C08G79/04
CPC分类号： C07F9/65746 , C07F9/306 , C07F9/657172 , C08G79/04 , Y10T428/31522 , Y10T428/31529
摘要： A phosphorus-containing oligomer is represented by formula (1): (R1 represents a hydrogen atom, an alkyl group having 1 to 4 carbon atoms, an alkoxy group having 1 to 4 carbon atoms, or a phenyl group; n is the number of repeating units and an integer of 1 or more; X is a structural unit represented by structural formula (x1) or (x2) below; Y is a hydrogen atom, a hydroxyl group, or a structural unit represented by the formula (x1) or (x2); and, in the formula (x1) or (x2), R2, R3, R4, and R5 each independently represent a hydrogen atom, an alkyl group having 1 to 4 carbon atoms, a phenyl group, or an aralkyl group), wherein the content of components whose n is 2 or more in the formula (1) is in the range of 5% to 90% in peak area in GPC measurement.
摘要翻译：含磷低聚物由式（1）表示：（R 1表示氢原子，碳原子数1〜4的烷基，碳原子数1〜4的烷氧基或苯基），n表示重复单元和1以上的整数; X是由下述结构式（x1）或（x2）表示的结构单元; Y是氢原子，羟基或由式（x1）表示的结构单元或（x2）;在式（x1）或（x2）中，R2，R3，R4和R5各自独立地表示氢原子，碳原子数1〜4的烷基，苯基或芳烷基），其中式（1）中n为2以上的成分的含量在GPC测定中的峰面积为5〜90％的范围。

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