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    • 9. 发明授权
    • NI-FE magnetic alloy and method for producing thereof
    • NI-FE磁性合金及其制造方法
    • US5500057A
    • 1996-03-19
    • US130369
    • 1993-10-01
    • Tadashi InoueKiyoshi TsuruShinichi OkimotoNaokazu YamamuraTetsuo YamamotoHirohisa Haiji
    • Tadashi InoueKiyoshi TsuruShinichi OkimotoNaokazu YamamuraTetsuo YamamotoHirohisa Haiji
    • C22C19/03C22F1/00C22F1/10H01F1/147H01F1/04
    • H01F1/14708C22C19/03H01F1/14716
    • A Ni-Fe magnetic alloy consists essentially of:77 to 80 wt. % Ni, 3.5 to 5 wt. % Mo, 1.5 to 3 wt. % Cu, 0.1 to 1.1 wt. % Mn, 0.1 wt. % or less Cr, 0.003 wt. % or less S, 0.01 wt. % or less P, 0.005 wt. % or less 0, 0.003 wt. % or less N, 0.02 wt. % or less C, 0.001 to 0.05 wt. % Al, 1 wt. % or less Si, 2.6-6 of the weight ratio of Ca to S, (Ca/S), and the balance being Fe and inevitable impurities, satisfies an equation of 3.2.ltoreq.(2.02.times.[Ni]-11.13.times.[Mo]-1.25.times.[Cu]-5.03.times.[Mn])/ (2.13.times.[Fe]).ltoreq.3.8; and has a Mo segregation ratio defined by a seregration equation satisfying 5% or less, the seregration equation being .vertline.(Mo content in a segregation region-Mo average content)/ (Mo average content).vertline..times.100%.A method for producing a magnetic Ni-Fe alloy comprises the steps of: a first heating step of heating an alloy ingot to 1200.degree. to 1300.degree. C. for 10 to 30 hrs; slabbing the heated ingot at a finishing temperature of 950.degree. C. or more to produce a slab; a second heating step of heating the slab at 1150.degree. to 1270.degree. C. for 1 to 5 hrs: and hot rolling the heated slab at a finishing temperature 950.degree. C. or more.
    • Ni-Fe磁性合金主要由以下组成:77〜80wt。 %Ni,3.5〜5wt。 %Mo,1.5〜3wt。 %Cu,0.1〜1.1wt。 %Mn,0.1wt。 %以下Cr,0.003重量% %以下S,0.01重量% %以下P,0.005重量% %以下0,0.003重量% %以下N,0.02重量% %以下C,0.001〜0.05重量% %Al,1wt。 %以下的Si,2.6〜6(Ca / S)的重量比(Ca / S),余量为Fe和不可避免的杂质,满足3.2的方程式(2.02×[Ni] -11.13×[ Mo] -1.25x [Cu] -5.03x [Mn])/(2.13x [Fe])= 3.8; 并且具有由满足5%以下的对数方程定义的Mo偏析比,所述对数方程为|(偏析区中的Mo含量-Mo平均含量)/(Mo平均含量)| x100%。 一种磁性Ni-Fe合金的制造方法,其特征在于,包括以下步骤:将合金锭加热到1200〜1300℃进行10〜30小时的第一加热工序; 在950℃或更高的终轧温度下对加热的锭进行烧结以制造板坯; 第二加热步骤,在1150℃〜1270℃下加热板坯1〜5小时,并在950℃以上的终轧温度下热轧。
    • 10. 发明授权
    • Method for manufacturing Ni-Fe alloy sheet having excellent DC magnetic
property and excellent AC magnetic property
    • 制造具有优异的直流磁性和优异的交流磁性的Ni-Fe合金薄片的方法
    • US4948434A
    • 1990-08-14
    • US324232
    • 1989-03-14
    • Tadashi InoueTomoyoshi Ohkita
    • Tadashi InoueTomoyoshi Ohkita
    • C22C19/03C22F1/10H01F1/147
    • H01F1/14716C22C19/03C22F1/10
    • A method for manufacturing an Ni-Fe alloy sheet having an excellent DC magnetic property and an excellent AC magnetic property, which comprises the steps of:hot-working a material consisting essentially of:______________________________________ nickel from 76 to 81 wt. %, molybdenum from 3 to 5 wt. %, copper from 1.5 to 3.0 wt. %, boron from 0.0015 to 0.0050 wt. %, ______________________________________ and the balance being iron and incidental impurities, to prepare an Ni-Fe alloy sheet; then subjecting the alloy sheet to a first cold-rolling at a reduction ratio of from 50 to 98%; then subjecting the alloy sheet to a first annealing in a temperature of from 780.degree. to 950.degree. C.; then subjecting the alloy sheet to a second cold-rolling at a reduction ratio of from 75 to 98%; and then subjecting the alloy sheet to a second annealing in a temperature of from 950.degree. to 1,200.degree. C.; thereby imparting an excellent DC magnetic property and an excellent AC magnetic property to the alloy sheet.
    • 一种具有优异的DC磁性和优异的AC磁性的Ni-Fe合金薄板的制造方法,其特征在于包括以下步骤:热处理基本上由以下组成的材料:镍,其为76〜81重量% %, - 钼3〜5wt。 %, - 铜,1.5〜3.0wt。 %, - 硼0.001-0.0050wt。 %, - 余量为铁和杂质,制备Ni-Fe合金板; 然后以50〜98%的还原率对合金板进行第一次冷轧, 然后在780〜950℃的温度下进行第一次退火处理。 然后以75〜98%的压下率对合金板进行第二次冷轧; 然后在950〜1200℃的温度下对合金板进行第二次退火。 从而赋予合金板优异的DC磁特性和优异的AC磁性。