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1. 发明授权

US10774034B2 Process for the conversion of ethylene oxide to monoethanolamine and ethylenediamine employing a zeolite 有权
公开(公告)号：US10774034B2
公开(公告)日：2020-09-15
申请号：US16610131
申请日：2018-05-03
申请人： BASF SE
发明人： Alvaro Gordillo , Andrei-Nicolae Parvulescu , Armin Lange De Oliveira , Andreas Kuschel , Juergen Bechtel , Johannes Lieberknecht , Ulrich Müller , Johann-Peter Melder , Christian Gruenanger
IPC分类号： C07C213/04 , B01J29/24 , B01J29/40 , B01J29/70 , C07C215/08 , B01J37/30 , C01B39/26 , C01B39/38 , C07C211/10 , B01J37/08
摘要： The present invention relates to a process for the conversion of ethylene oxide to 2-aminoethanol and/or ethane-1,2-diamine and/or linear polyethylenimines of the formula H2N—(CH2CH2NH)n—CH2CH2—NH2 wherein n≥1 comprising (i) providing a catalyst comprising a zeolitic material comprising YO2 and X2O3, wherein Y is a tetravalent element and X is a trivalent element; (ii) providing a gas stream comprising ethylene oxide and ammonia; (iii) contacting the catalyst provided in (i) with the gas stream provided in (ii) for converting ethylene oxide to 2-aminoethanol and/or ethane-1,2-diamine and/or linear polyethylenimines.

2. 发明授权

US10745285B2 Process for preparing a molecular sieve 有权
公开(公告)号：US10745285B2
公开(公告)日：2020-08-18
申请号：US15984595
申请日：2018-05-21
申请人： ExxonMobil Chemical Patents Inc.
发明人： Wenyih F. Lai , Nicholas S. Rollman , Guang Cao
IPC分类号： C07C6/12 , C01B39/26 , B01J29/18 , B01J29/22 , B01J29/24 , B01J20/18 , B01J20/28 , B01J20/30 , B01J29/40 , B01J29/70 , B01J29/80 , B01J35/00 , B01J35/02 , B01J35/10
摘要： A process for converting a feedstock comprising an organic compound to a conversion product by contacting said feedstock at organic compound conversion conditions with a catalyst comprising a mordenite zeolite having a mesoporous surface area of greater than 30 m2/g and an average primary crystal size as measured by TEM of less than 80 nm.

3. 发明授权

US10723631B2 Methods of producing composite zeolite catalysts for heavy reformate conversion into xylenes 有权
公开(公告)号：US10723631B2
公开(公告)日：2020-07-28
申请号：US16299704
申请日：2019-03-12
申请人： Saudi Arabian Oil Company , Universitat Politecnica De Valencia , Consejo Superior De Investigaciones Cientificas
发明人： Raed Hasan Abudawoud , Avelino Corma Canos , M. Teresa Portilla Ovejero , Vicente J. Margarit Benavent , M. Teresa Navarro Villalba , M. Cristina Martinez Sanchez , Ibrahim M. Al-Zahrani
IPC分类号： C01B39/02 , C07C15/08 , B01J29/80 , C01B39/04 , B01J29/26 , B01J29/48 , B01J37/02 , B01J37/04 , B01J37/08 , C01B39/26 , C01B39/38 , C07C4/18 , C07C6/12 , B01J29/22 , B01J29/18 , B01J35/00 , B01J29/46 , B01J29/24 , B01J29/44 , B01J29/40 , C01B39/40 , B01J29/06
摘要： A method of forming composite zeolite catalyst particles includes combining a silicon source, an aqueous organic structure directing agent having a polyquaternary ammonium compound, water and an aluminum source to form a catalyst gel. The method also includes heating the catalyst gel to form the composite zeolite catalyst particle having an intergrowth region with a mixture of both Mordenite crystals and ZSM-5 crystals. An associated method of making xylene includes feeding heavy reformate to a reactor, the reactor containing the composite zeolite catalyst particles, and producing xylene by simultaneously performing dealkylation and transalkylation of the heavy reformate in the reactor, where each composite zeolite catalyst particle is able to catalyze both the dealkylation and transalkylation reactions.

4. 发明授权

US10583426B2 Carbonylation catalyst and process 有权
公开(公告)号：US10583426B2
公开(公告)日：2020-03-10
申请号：US16018689
申请日：2018-06-26
申请人： BP CHEMICALS LIMITED
发明人： John Glenn Sunley
IPC分类号： B01J29/06 , B01J29/87 , C07C51/347 , C07C51/09 , C07C53/08 , C07C69/14 , C07C51/12 , C07C29/132 , C07C29/153 , C07C29/136 , B01J29/18 , B01J29/24 , B01J29/65 , B01J29/70 , B01J35/10 , B01J37/00 , C01B39/26 , C07C67/37 , C01B39/06 , B01J29/50 , B01J29/88 , C01B39/44 , C01B39/30 , B01J29/86 , C01B39/08
摘要： A catalyst and process for the production of methyl acetate by contacting dimethyl ether and carbon monoxide in the presence of a catalyst which is a zeolite of micropore volume of 0.01 ml/g or less.

5. 发明授权

US10301185B2 Solidothermal synthesis of zeolitic materials and zeolites obtained therefrom 有权
公开(公告)号：US10301185B2
公开(公告)日：2019-05-28
申请号：US15518945
申请日：2015-10-15
申请人： BASF SE
发明人： Stefan Maurer , Ulrich Müller , Feng-Shou Xiao , Xiangju Meng , Qinming Wu
IPC分类号： B01J29/70 , C01B39/48 , B01J29/18 , C01B39/20 , C01B39/26 , C01B39/04 , B01J29/08 , B01J29/40 , B01J29/65 , C01B37/02 , C01B39/08 , C01B39/40
摘要： The present invention relates to a process for the preparation of a zeolitic material comprising YO2 in its framework structure, wherein Y stands for a tetravalent element, wherein said process comprises the steps of: (1) providing a mixture comprising one or more sources for YO2, one or more fluoride containing compounds, and one or more structure directing agents; (2) crystallizing the mixture obtained in step (1) for obtaining a zeolitic material comprising YO2 in its framework structure; wherein the mixture provided in step (1) and crystallized in step (2) contains 35 wt.-% or less of H2O based on 100 wt.-% of YO2 contained in the mixture provided in step (1) and crystallized in step (2), as well as to a zeolitic material comprising YO2 in its framework structure obtainable and/or obtained according to said process, and to a zeolitic material per se comprising SiO2 in its framework structure, wherein in the 29Si MAS NMR spectrum of the as-synthesized zeolitic material the ratio of the total integration value of the peaks associated to Q3 signals to the total integration value of the peaks associated to Q4 signals is in the range of from 0:100 to 20:80, including the use of the aforementioned zeolitic materials.

6. 发明授权

US10195594B2 Mesoporous MFI-zeolite catalysts, methods of preparing the same and uses 有权
公开(公告)号：US10195594B2
公开(公告)日：2019-02-05
申请号：US14776114
申请日：2014-03-18
申请人： The Coca-Cola Company , BOARD OF TRUSTEES OF MICHIGAN STATE UNIVERSITY
发明人： Shantanu Kelkar , Thomas J. Pinnavaia , Christopher M. Saffron , Robert Kriegel
IPC分类号： B01J29/06 , B01J29/04 , B01J29/40 , C01B39/36 , B01J35/10 , B01J37/30 , B01J37/02 , B01J37/00 , C10G45/68 , C10G3/00 , B01J29/87 , C01B39/02 , C01B39/26 , C01B39/38 , C01B39/40 , B01J37/08 , C10G50/00
摘要： The invention relates to a novel zeolite catalysts, methods of producing the zeolite catalysts and a methods of using such catalyst, including for production of BTEX with improved yield, product selectivity and reduced char production. The present invention relates to novel mesoporous zeolite catalysts, as well as methods of producing the same. The present invention also relates to methods of producing renewable aromatic hydrocarbons using such catalysts.

7. 发明授权

US09738537B2 Crystalline molecular sieves and synthesis thereof 有权
公开(公告)号：US09738537B2
公开(公告)日：2017-08-22
申请号：US15215657
申请日：2016-07-21
申请人： Chevron U.S.A. Inc.
发明人： Stacey Ian Zones
IPC分类号： C01B39/48 , B01D53/02 , B01J29/70 , C01B39/04 , B01J20/18 , B01J20/30 , B01J29/04 , B01J29/18 , B01J29/86 , B01J39/14 , C01B39/00 , C01B39/26 , C01B37/02 , C01B39/12
CPC分类号： C01B39/04 , B01J20/18 , B01J20/3057 , B01J29/041 , B01J29/047 , B01J29/18 , B01J29/70 , B01J29/86 , B01J39/14 , C01B37/02 , C01B39/00 , C01B39/12 , C01B39/265 , C01B39/48
摘要： Crystalline molecular sieves and their synthesis using quaternary N-methyl-diisoalkylammonium cations as organic structure directing agents are disclosed. The structure directing agent has the following structure (1): in which R1 is selected from hydrogen, a methyl group, an ethyl group, a propyl group, and a hydroxymethyl group; and R2, R3, R4 and R5 are independently selected from a methyl group, an ethyl group, and a propyl group.

8. 发明申请

US20170107111A1 WATER-SOLUBLE ELECTROLYZED/SOLVOLYZED CLINOPTILOLITE FRAGMENTS AND NUTRACEUTICAL, PHARMACEUTICAL, AND ENVIRONMENTAL PRODUCTS BASED THEREON 审中-公开
公开(公告)号：US20170107111A1
公开(公告)日：2017-04-20
申请号：US14884669
申请日：2015-10-15
申请人： EnTox Solutions LLC
发明人： Christina Rahm Cook
IPC分类号： C01B39/02 , C25B1/00 , B01J20/16 , C25B1/04 , C01B39/26 , A61K33/06
CPC分类号： C01B39/026 , A61K9/0078 , A61K9/08 , A61K33/06 , A61K33/12 , A61K47/10 , A61K47/18 , B01J20/165 , C01B39/26 , C25B1/00 , C25B1/04 , Y02E60/366
摘要： Methods and processes are provided to make clinoptilolite into a water-soluble solvolyzed form with electrolytes suitable for various administration routes for use in the detoxification and rejuvenation in environment arena, nutraceutical arena, and pharmaceutical arena This process includes oral, topical, tablet, pill formulas, biotech delivery and intravenous. Absorption of water-soluble solvolyzed clinoptilolite fragments can aid in detoxification by binding to heavy metals, viruses and environmental toxins and can reduce reactive oxygen species and inflammation related to metals. The process and method described can provide an increase in energy, increase in growth factors that aid in hair, skin, and nail growth, and can provide an increase in focus, concentration, and memory. Water-soluble solvolyzed, electrolyzed clinoptilolite fragments can be combined with one or more dietary supplements, including various vitamins, minerals, and sleep aids to rejuvenate the cells and the environment during and after detoxification.

9. 发明授权

US08758775B2 Pharmaceutical composition including clinoptilolite 有权
标题翻译：药物组合物包括斜发沸石
公开(公告)号：US08758775B2
公开(公告)日：2014-06-24
申请号：US12066338
申请日：2006-09-08
申请人： Kevin Gast
发明人： Kevin Gast
IPC分类号： A61K33/06 , A61P1/00 , C01B39/26
CPC分类号： A61K33/06 , C01B39/026 , C01B39/26
摘要： The invention is for a method of potentiating clinoptilolite, the method including the steps of: providing fresh or spent clinoptilolite; exposing the clinoptilolite to a saline solution having a sodium ion content of about 10% to liberate impurities from the clinoptilolite; and drying the washed clinoptilolite fraction to render a potentiated clinoptilolite fraction. Preferably, the clinoptilolite is exposed to the saline solution for a period of about 48 hours. The washed clinoptilolite may be dried by filtered, heated air. This allows an optimal cation exchange capacity of the clinoptilolite to be reached. The clinoptilolite has uses as a medicament for a variety of aliments.
摘要翻译：本发明涉及一种增强斜发沸石的方法，该方法包括以下步骤：提供新鲜或消耗的斜发沸石; 将斜发沸石暴露于钠离子含量约10％的盐溶液中以从斜发沸石中释放出杂质; 并干燥洗涤的斜发沸石馏分以产生增强的斜发沸石馏分。优选地，将斜发沸石暴露于盐水溶液约48小时。洗涤的斜发沸石可以通过过滤的加热空气干燥。这允许达到斜发沸石的最佳阳离子交换容量。斜发沸石具有用作各种药物的药物的用途。

10. 发明申请

US20120024776A1 Mesostructured Zeolitic Materials, and Methods of Making and Using the Same 有权
标题翻译：中等结构的沸石材料及其制造和使用方法
公开(公告)号：US20120024776A1
公开(公告)日：2012-02-02
申请号：US13205151
申请日：2011-08-08
申请人： Javier Garcia-Martinez
发明人： Javier Garcia-Martinez
IPC分类号： B01J29/04 , C10G31/00 , B01D15/04 , B01D71/02 , B01D39/00 , C02F5/00 , C01B39/00 , C12N9/00 , B01J29/40 , B01J29/18 , B01J29/08 , B01J35/10 , B01J20/02 , C07C15/04 , C07C11/00 , C01B39/20 , C01B39/26 , C01B39/38 , B01J20/18 , B01J20/28 , B01D15/08 , C10G1/04
CPC分类号： B01J29/40 , B01J20/18 , B01J20/186 , B01J29/005 , B01J29/0308 , B01J29/041 , B01J29/084 , B01J29/106 , B01J29/18 , B01J29/80 , B01J2229/62 , B82Y30/00 , C01B39/02 , C01B39/023 , C01B39/026 , C01B39/04 , C10G1/086 , C10G11/02 , C10G11/05 , C10G11/18 , C10G45/04 , C10G47/02 , C10G2300/1033 , C10G2300/1074 , C10G2300/1096 , C10G2400/02 , C10G2400/20 , Y10T428/26
摘要： One aspect of the present invention relates to mesostructured zeolites. The invention also relates to a method of preparing mesostructured zeolites, as well as using them as cracking catalysts for organic compounds and degradation catalysts for polymers.
摘要翻译：本发明的一个方面涉及介孔结构的沸石。本发明还涉及一种制备介孔结构的沸石的方法，以及它们用作有机化合物的裂化催化剂和聚合物的降解催化剂。

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