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1. 发明申请

US20170182486A1 METAL-ORGANIC FRAMEWORKS CONTAINING NITROGEN-DONOR LIGANDS FOR EFFICIENT CATALYTIC ORGANIC TRANSFORMATIONS 审中-公开
公开(公告)号：US20170182486A1
公开(公告)日：2017-06-29
申请号：US15129853
申请日：2015-03-30
申请人： The University of Chicago
发明人： Wenbin Lin, Ph.D. , Kuntal Manna , Teng Zhang
IPC分类号： B01J31/16 , C07F5/02 , C07F7/18 , C07C5/03 , C07C41/20 , C07D207/04 , C07D207/06 , C07C209/02 , B01J31/18 , C07C37/07
CPC分类号： B01J31/1691 , B01J31/18 , B01J31/1815 , B01J2531/16 , B01J2531/48 , B01J2531/824 , B01J2531/827 , B01J2531/842 , B01J2531/845 , B01J2531/847 , C07C5/03 , C07C37/07 , C07C41/20 , C07C209/02 , C07D207/04 , C07D207/06 , C07F5/025 , C07F7/1876 , Y02P20/544
摘要： Metal-organic framework (MOFs) compositions based on nitrogen donor-based organic bridging ligands, including ligands based on 1,3-diketimine (NacNac), bipyridines and salicylaldimine, were synthesized and then post-synthetically metalated with metal precursors, such as complexes of first row transition metals. Metal complexes of the organic bridging ligands could also be directly incorporated into the MOFs. The MOFs provide a versatile family of recyclable and reusable single-site solid catalysts for catalyzing a variety of asymmetric organic transformations. The solid catalysts can also be integrated into a flow reactor or a supercritical fluid reactor.

2. 发明授权

US09579632B2 Dehydrogenation catalyst and process 有权
标题翻译：脱氢催化剂和工艺
公开(公告)号：US09579632B2
公开(公告)日：2017-02-28
申请号：US13990440
申请日：2011-12-02
申请人： Jihad M. Dakka , Lorenzo C. DeCaul , Terry E. Helton , Keith H. Kuechler , Jenna L. Wallace
发明人： Jihad M. Dakka , Lorenzo C. DeCaul , Terry E. Helton , Keith H. Kuechler , Jenna L. Wallace
IPC分类号： B01J23/62 , B01J35/00 , B01J37/02 , C07C37/06 , C07C37/07 , B01J21/08 , B01J23/24 , B01J23/32
CPC分类号： B01J23/626 , B01J21/08 , B01J23/24 , B01J23/32 , B01J35/0066 , B01J37/0207 , C07C37/06 , C07C37/07 , Y02P20/52 , C07C39/04
摘要： A catalyst composition comprises (i) a support; (ii) a dehydrogenation component comprising at least one metal or compound thereof selected from Groups 6 to 10 of the Periodic Table of Elements; and (iii) tin or a tin compound, wherein the tin is present in an amount of 0.01 wt % to about 0.25 wt %, the wt % based upon the total weight of the catalyst composition.
摘要翻译：催化剂组合物包含（i）载体; （ii）包含选自元素周期表第6至10族的至少一种金属或其化合物的脱氢组分; 和（iii）锡或锡化合物，其中锡的存在量为0.01重量％至约0.25重量％，基于催化剂组合物的总重量的wt％。

3. 发明授权

US09233887B2 Process for producing a monocycloalkyl-substituted aromatic compound 有权
标题翻译：制备单环烷基取代的芳族化合物的方法
公开(公告)号：US09233887B2
公开(公告)日：2016-01-12
申请号：US13885611
申请日：2011-11-04
申请人： Jihad M. Dakka , Teng Xu , Edward A. Lemon , James R. Lattner , Jane C. Cheng
发明人： Jihad M. Dakka , Teng Xu , Edward A. Lemon , James R. Lattner , Jane C. Cheng
IPC分类号： C07C2/66 , C07C37/07 , C07C37/08 , C07C45/53
CPC分类号： C07C2/66 , C07C37/07 , C07C37/08 , C07C45/53 , C07C2529/08 , C07C2529/18 , C07C2529/70 , Y02P20/127 , C07C13/28
摘要： In a process for producing mono-cycloalkyl-substituted aromatic compound, benzene and cyclic monoolefin are contacted with a catalyst under alkylation conditions to produce an effluent containing mono-cycloalkyl-substituted aromatic compound. The catalyst comprises a molecular sieve.
摘要翻译：在制备单环烷基取代的芳族化合物的方法中，苯和环状单烯烃在烷基化条件下与催化剂接触以产生含有单环烷基取代的芳族化合物的流出物。催化剂包括分子筛。

4. 发明授权

US09035107B2 Dehydrogenation process 有权
标题翻译：脱氢工艺
公开(公告)号：US09035107B2
公开(公告)日：2015-05-19
申请号：US13515057
申请日：2010-12-17
申请人： Teng Xu , Stuart L. Soled , Edward A. Lemon , Joseph E. Baumgartner , Sabato Miseo , George H. Gamble
发明人： Teng Xu , Stuart L. Soled , Edward A. Lemon , Joseph E. Baumgartner , Sabato Miseo , George H. Gamble
IPC分类号： C07C37/06 , B01J23/42 , B01J21/08 , B01J37/02 , C07C5/367 , C07C37/07 , C07C37/08
CPC分类号： B01J23/42 , B01J21/08 , B01J37/0203 , C07C5/367 , C07C37/07 , C07C37/08 , C07C2523/58 , Y02P20/52 , C07C15/04 , C07C39/04
摘要： In a process for the dehydrogenation of dehydrogenatable hydrocarbons, a feed comprising dehydrogenatable hydrocarbons is contacted with a catalyst comprising a support and a dehydrogenation component under dehydrogenation conditions effective to convert at least a portion of the dehydrogenatable hydrocarbons in the feed. The catalyst is produced by a method comprising treating the support with a liquid composition comprising the dehydrogenation component or a precursor thereof and at least one organic dispersant selected from an amino alcohol and an amino acid.
摘要翻译：在可脱氢烃脱氢的方法中，包含可脱氢烃的进料在有效转化进料中至少一部分可脱氢烃的脱氢条件下与包含载体和脱氢组分的催化剂接触。催化剂通过包括用包含脱氢组分或其前体的液体组合物和至少一种选自氨基醇和氨基酸的有机分散体处理载体的方法制备。

5. 发明授权

US09029611B2 Dehydrogenation of cyclohexanone to produce phenol 有权
标题翻译：环己酮脱氢生产苯酚
公开(公告)号：US09029611B2
公开(公告)日：2015-05-12
申请号：US13512796
申请日：2010-12-17
申请人： Teng Xu , Jihad M. Dakka , Christopher L. Becker , Keith H. Kuechler , Francisco M. Benitez , Charles M. Smith , Hari Nair
发明人： Teng Xu , Jihad M. Dakka , Christopher L. Becker , Keith H. Kuechler , Francisco M. Benitez , Charles M. Smith , Hari Nair
IPC分类号： C07C37/06 , C07C2/74 , C07C37/07 , C07C37/08 , C07C45/53 , C07C407/00
CPC分类号： C07C2/74 , C07C37/07 , C07C37/08 , C07C45/53 , C07C407/00 , C07C2529/70 , C07C2529/74 , C07C2601/14 , C07C13/28 , C07C39/04 , C07C49/403 , C07C409/14
摘要： In a process for the dehydrogenation of cyclohexanone to produce phenol, a feed comprising cyclohexanone is contacted with a dehydrogenation catalyst under dehydrogenation conditions comprising a temperature of less than 400° C. and a pressure of less than 690 kPa, gauge, such 0.1 to 50 wt % of the cyclohexanone in said feed is converted to phenol and the dehydrogenation product contains less than 100 ppm by weight of alkylbenzenes.
摘要翻译：在环己酮脱氢生产苯酚的方法中，将包含环己酮的进料与脱氢催化剂在脱氢条件下接触，脱氢条件包括温度低于400℃，压力小于690kPa，表压0.1至50 所述进料中环己酮的重量％转化为苯酚，脱氢产物含有小于100重量ppm的烷基苯。

6. 发明申请

US20140330044A1 Process for Producing Phenol 有权
标题翻译：生产苯酚的方法
公开(公告)号：US20140330044A1
公开(公告)日：2014-11-06
申请号：US14347279
申请日：2012-08-29
申请人： Keith H. Kuechler , James R. Lattner , Christopher L. Becker
发明人： Keith H. Kuechler , James R. Lattner , Christopher L. Becker
IPC分类号： C07C37/07 , C07C49/403
CPC分类号： C07C37/07 , C07C2/74 , C07C37/08 , C07C45/53 , C07C49/403 , C07C407/00 , C07C2529/70 , C07C2601/14 , C07C13/28 , C07C409/14 , C07C39/04
摘要： In a process for producing phenol, cyclohexylbenzene hydroperoxide is cleaved to produce a cleavage effluent stream comprising phenol and cyclohexanone and at least a portion of the cleavage effluent stream is fractionated to produce a first fraction richer in cyclohexanone than the cleavage effluent stream portion and a second fraction richer in phenol and depleted in cyclohexanone as compared with said cleavage effluent stream portion. At least a portion of the second fraction is then contacted with a dehydrogenation catalyst in a dehydrogenation reaction zone under dehydrogenation conditions effective to convert at least a portion of the cyclohexanone in said second fraction portion into phenol and cyclohexanol.
摘要翻译：在生产苯酚的方法中，将环己基苯氢过氧化物切割以产生包含苯酚和环己酮的裂解流出料流，并将至少一部分裂解流出物流分馏以产生比裂解流出物流部分富含环己酮的第一馏分，第二馏分与所述裂解流出物流部分相比，苯酚中的馏分比较富含，耗尽环己酮。然后在有效将至少一部分所述第二级分部分中的环己酮转化成苯酚和环己醇的脱氢条件下，至少部分第二馏分与脱氢催化剂在脱氢反应区中接触。

7. 发明申请

US20140066663A1 Dehydrogenation Catalyst and Process 有权
标题翻译：脱氢催化剂和工艺
公开(公告)号：US20140066663A1
公开(公告)日：2014-03-06
申请号：US13990440
申请日：2011-12-02
申请人： Jihad M. Dakka , Lorenzo C. DeCaul , Terry E. Helton , Keith H. Kuechier , Jenna L. Waliace
发明人： Jihad M. Dakka , Lorenzo C. DeCaul , Terry E. Helton , Keith H. Kuechier , Jenna L. Waliace
IPC分类号： B01J23/62 , C07C37/06 , C07C37/07
CPC分类号： B01J23/626 , B01J21/08 , B01J23/24 , B01J23/32 , B01J35/0066 , B01J37/0207 , C07C37/06 , C07C37/07 , Y02P20/52 , C07C39/04
摘要： A catalyst composition comprises (i) a support; (ii) a dehydrogenation component comprising at least one metal or compound thereof selected from Groups 6 to 10 of the Periodic Table of Elements; and (iii) tin or a tin compound, wherein the tin is present in an amount of 0.01 wt % to about 0.25 wt %, the wt % based upon the total weight of the catalyst composition.
摘要翻译：催化剂组合物包含（i）载体; （ii）包含选自元素周期表第6至10族的至少一种金属或其化合物的脱氢组分; 和（iii）锡或锡化合物，其中锡的存在量为0.01重量％至约0.25重量％，基于催化剂组合物的总重量的wt％。

8. 发明授权

US08487140B2 Process for producing phenol 有权
标题翻译：苯酚生产工艺
公开(公告)号：US08487140B2
公开(公告)日：2013-07-16
申请号：US12996219
申请日：2009-07-14
申请人： John S. Buchanan , Jon E. Stanat , Tan-Jen Chen , Jihad M. Dakka , James R. Lattner
发明人： John S. Buchanan , Jon E. Stanat , Tan-Jen Chen , Jihad M. Dakka , James R. Lattner
IPC分类号： C07C37/07 , C07C37/08
CPC分类号： C07C37/06 , C07C2/74 , C07C37/08 , C07C45/53 , C07C407/00 , C07C2601/14 , C07C13/28 , C07C39/04 , C07C49/403 , C07C409/14
摘要： In a process for producing phenol, cyclohexylbenzene is oxidized to produce cyclohexylbenzene hydroperoxide and then the resultant cyclohexylbenzene hydroperoxide is cleaved to produce an effluent stream comprising phenol and cyclohexanone. At least a portion of the effluent stream is then fed to at least one dehydrogenation reaction zone, where the effluent stream portion is contacted with a dehydrogenation catalyst under conditions effective to convert at least part of the cyclohexanone in the effluent portion into phenol and hydrogen.
摘要翻译：在生产苯酚的方法中，将环己基苯氧化生产环己基苯氢过氧化物，然后将所得的环己基苯氢过氧化物切割以产生包含苯酚和环己酮的流出物流。然后将至少一部分流出物流送入至少一个脱氢反应区，其中流出物流部分与脱氢催化剂在有效地将流出物部分中的至少一部分环己酮转化为酚和氢的条件下接触。

9. 发明申请

US20050137409A1 Processes for preparing benzoquinones and hydroquinones 审中-公开
标题翻译：制备苯醌和氢醌的方法
公开(公告)号：US20050137409A1
公开(公告)日：2005-06-23
申请号：US11008029
申请日：2004-12-09
申请人： Sunil Ashtekar , Pramod Kumbhar , Jan-Pleun Lens , Rathinam Mahalingam , Nadkarni Pradeep , Jegadeesh Thampi
发明人： Sunil Ashtekar , Pramod Kumbhar , Jan-Pleun Lens , Rathinam Mahalingam , Nadkarni Pradeep , Jegadeesh Thampi
IPC分类号： B01J27/122 , C07C37/07 , C07C39/08 , C07C46/08 , C08G64/04 , C07C50/04 , C07C45/27
CPC分类号： B01J27/122 , C07C37/07 , C07C46/08 , C08G64/04 , C07C50/02 , C07C39/08
摘要： A process for the preparation of benzoquinones and hydroquinones includes oxidizing an aromatic hydroxy compound with oxygen or an oxygen containing gas, a copper containing catalyst, and optionally a promoter to form the benzoquinone. A reduction reaction is employed to form the hydroquinone.
摘要翻译：制备苯醌和氢醌的方法包括用氧或含氧气体氧化芳族羟基化合物，含铜催化剂和任选的助催化剂以形成苯醌。采用还原反应形成氢醌。

10. 发明授权

US6039955A Nontoxic extract of Larrea tridentata and method of making the same 失效
标题翻译：无毒提取物及其制备方法
公开(公告)号：US6039955A
公开(公告)日：2000-03-21
申请号：US329359
申请日：1999-06-10
申请人： Robert A. Sinnott , W. Dennis Clark , Kenneth Frank DeBoer
发明人： Robert A. Sinnott , W. Dennis Clark , Kenneth Frank DeBoer
IPC分类号： A23L1/30 , A61K36/00 , A61K36/185 , A61K36/28 , A61K36/29 , A61K45/06 , A61P29/00 , C07C37/07 , A61K35/78
CPC分类号： C07C37/07 , A23L33/10 , A23L33/105 , A61K36/185 , A61K36/28 , A61K36/29 , A61K45/06 , Y10S514/885 , Y10S514/886 , Y10S514/969
摘要： A nontoxic, therapeutic agent having pharmacological activity comprising concentrated extract of Larrea tridentata plant material and ascorbic acid, an ascorbic acid ester, an ascorbic acid salt, butylated hydroxyanisole, butylated hydroxytoluene, hydrogen sulfide, hypophosphorous acid, monothioglycerol, potassium bisulfite, propyl gallate, sodium bisulfite, sodium hydrosulfite, sodium thiosulfate, sulfur dioxide, sulfurous acid, a tocopherol or vitamin E is made by a process in which the plant material is extracted using an organic solvent, preferably acetone, and is then saturated with one of the listed reducing agents acid to reduce the toxic NDGA quinone, which naturally occurs in the plant material, to NDGA itself. Additional amounts of ascorbic acid, an ascorbic acid ester, an ascorbic acid salt, butylated hydroxyanisole, butylated hydroxytoluene, hydrogen sulfide, hypophosphorous acid, monothioglycerol, potassium bisulfite, propyl gallate, sodium bisulfite, sodium hydrosulfite, sodium thiosulfate, sulfur dioxide, sulfurous acid, a tocopherol, or vitamin E may be added to the extract to inhibit the natural oxidation of the NDGA into the toxic NDGA quinone in vivo, or during processing or storage. The resulting extract is usefull in the treatment of viral diseases caused by viruses from the Herpesviridae family or viruses which require the Sp1 class of proteins to initiate viral replications. The resulting compound can also be used as an anti-inflammatory when the inflammatory diseases are mediated by the effects of leukotrienes. The listed reducing agents can also be used to stabilize NDGA as a therapeutic agent or a food additive.
摘要翻译：具有药理活性的无毒性治疗剂，其包含三氯氰菊酯植物材料和抗坏血酸的浓缩提取物，抗坏血酸酯，抗坏血酸盐，丁基化羟基苯甲醚，丁基化羟基甲苯，硫化氢，次磷酸，一硫代甘油，亚硫酸氢钾，没食子酸丙酯，亚硫酸氢钠，连二亚硫酸钠，硫代硫酸钠，二氧化硫，亚硫酸，生育酚或维生素E是通过使用有机溶剂，优选丙酮萃取植物材料的方法制备的，然后用列出的还原剂药剂酸降低有毒的NDGA醌，其自然发生在植物材料中，对NDGA本身。附加量的抗坏血酸，抗坏血酸酯，抗坏血酸盐，丁基化羟基苯甲醚，丁基化羟基甲苯，硫化氢，次磷酸，一硫代甘油，亚硫酸氢钾，没食子酸丙酯，亚硫酸氢钠，连二亚硫酸钠，硫代硫酸钠，二氧化硫，亚硫酸，生育酚或维生素E可以加入到提取物中以抑制NDGA在体内或在加工或储存过程中自然氧化成有毒的NDGA醌。所得的提取物可用于治疗由疱疹病毒科家族病毒引起的病毒性疾病或需要Sp1类蛋白质启动病毒复制的病毒。当炎性疾病由白细胞三烯的作用介导时，所得化合物也可用作抗炎剂。列出的还原剂也可用于稳定NDGA作为治疗剂或食品添加剂。

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