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1. 发明申请

US20190211149A1 ALKYLENE OXIDE POLYMERIZATION USING A DOUBLE METAL CYANIDE CATALYST COMPLEX AND A MAGNESIUM, GROUP 3 - GROUP 15 METAL OR LANTHANIDE SERIES METAL COMPOUND 审中-公开
公开(公告)号：US20190211149A1
公开(公告)日：2019-07-11
申请号：US16354114
申请日：2019-03-14
申请人： Dow Global Technologies LLC
发明人： David S. Laitar , David A. Babb , Carlos M. Villa , Richard Keaton , Jean-Paul Masy
IPC分类号： C08G65/26 , C07C41/02 , C08G65/34 , C07C41/01
CPC分类号： C08G65/2663 , C07C41/01 , C07C41/02 , C08G65/269 , C08G65/34
摘要： Alkylene oxide polymerizations are performed in the presence of a double metal cyanide polymerization catalyst and certain magnesium, Group 3-Group 15 metal or lanthanide series metal compounds. The presence of the magnesium, Group 3-Group 15 metal or lanthanide series metal compound provides several benefits including more rapid catalyst activation, faster polymerization rates and the reduction in the amount of ultra high molecular weight polymers that are formed. The catalyst mixture is unexpectedly useful in making polyethers having low equivalent weights.

2. 发明授权

US10233284B2 Alkylene oxide polymerization using a double metal cyanide catalyst complex and a magnesium, group 3-group 15 metal or lanthanide series metal compound 有权
公开(公告)号：US10233284B2
公开(公告)日：2019-03-19
申请号：US15382519
申请日：2016-12-16
申请人： Dow Global Technologies LLC
发明人： David S. Laitar , David A. Babb , Carlos M. Villa , Richard Keaton , Jean-Paul Masy
IPC分类号： C08G65/34 , C07C41/02 , C07C41/01 , C08G65/26
摘要： Alkylene oxide polymerizations are performed in the presence of a double metal cyanide polymerization catalyst and certain magnesium, Group 3-Group 15 metal or lanthanide series metal compounds. The presence of the magnesium, Group 3-Group 15 metal or lanthanide series metal compound provides several benefits including more rapid catalyst activation, faster polymerization rates and the reduction in the amount of ultra high molecular weight polymers that are formed. The catalyst mixture is unexpectedly useful in making polyethers having low equivalent weights.

3. 发明申请

US20170101506A1 ALKYLENE OXIDE POLYMERIZATION USING A DOUBLE METAL CYANIDE CATALYST COMPLEX AND A MAGNESIUM, GROUP 3 - GROUP 15 METAL OR LANTHANIDE SERIES METAL COMPOUND 审中-公开
公开(公告)号：US20170101506A1
公开(公告)日：2017-04-13
申请号：US15382519
申请日：2016-12-16
申请人： Dow Global Technologies LLC
发明人： David S. Laitar , David A. Babb , Carlos M. Villa , Richard Keaton , Jean-Paul Masy
IPC分类号： C08G65/26 , C07C41/01 , C08G65/34 , C07C41/02
CPC分类号： C08G65/2663 , C07C41/01 , C07C41/02 , C08G65/269 , C08G65/34
摘要： Alkylene oxide polymerizations are performed in the presence of a double metal cyanide polymerization catalyst and certain magnesium, Group 3-Group 15 metal or lanthanide series metal compounds. The presence of the magnesium, Group 3-Group 15 metal or lanthanide series metal compound provides several benefits including more rapid catalyst activation, faster polymerization rates and the reduction in the amount of ultra high molecular weight polymers that are formed. The catalyst mixture is unexpectedly useful in making polyethers having low equivalent weights.

4. 发明申请

US20160082423A9 ALKYLENE OXIDE CATALYST AND USE THEREOF 审中-公开
公开(公告)号：US20160082423A9
公开(公告)日：2016-03-24
申请号：US13624131
申请日：2012-09-21
申请人： Manuel A. W. Natal , Madan M. Bhasin , Hwaili Soo , Albert C. Liu
发明人： Manuel A. W. Natal , Madan M. Bhasin , Hwaili Soo , Albert C. Liu
IPC分类号： B01J27/055 , B01J23/68 , C07D301/10 , C07C29/10 , B01J35/02 , C07C41/02 , B01J37/02 , B01J23/66 , C07C209/16
CPC分类号： B01J27/055 , B01J21/04 , B01J23/50 , B01J23/58 , B01J23/688 , B01J35/0013 , B01J35/006 , B01J35/023 , B01J37/0203 , B01J37/0205 , B01J37/0244 , B01J37/16 , C07C209/60 , C07D301/10 , Y02P20/52
摘要： A supported silver catalyst and use thereof in a process for producing an alkylene oxide, such as ethylene oxide, by the direct oxidation of an alkylene with oxygen or an oxygen-containing gas, wherein the catalyst provides improved stability and improved resilience to reactor upsets and timely recovery to substantially pre-upset levels of catalyst activity and/or efficiency. In some embodiments, the catalyst also exhibits improved activity. A catalyst capable of producing ethylene oxide at a selectivity of at least 87 percent while achieving a work rate of at least 184 kg/h/m3 at a temperature of no greater than 235° C. when operated in a process where the inlet feed to a reactor containing the catalyst comprises ethylene, oxygen, and carbon dioxide, wherein the concentration of carbon dioxide in the inlet feed is greater than or equal to 2 mole percent.

5. 发明授权

US09120731B2 Process for preparing polyether alcohols 有权
标题翻译：制备聚醚醇的方法
公开(公告)号：US09120731B2
公开(公告)日：2015-09-01
申请号：US13813300
申请日：2011-08-08
申请人： Achim Loeffler , Michael Stoesser , Wolfgang Loth , Ralf Boehling , Sirus Zarbakhsh
发明人： Achim Loeffler , Michael Stoesser , Wolfgang Loth , Ralf Boehling , Sirus Zarbakhsh
IPC分类号： C07C41/02 , C08G65/26
CPC分类号： C07C41/02 , C08G65/2696
摘要： What is proposed is a process for preparing polyether alcohols by conversion of the following reactants: a) one or more alkylene oxides and optionally carbon dioxide and b) one or more H-functional starter substances, in the presence of a catalyst, to form a liquid reaction mixture, in a reaction unit (1), which is characterized in that the reaction unit (1) has internals (2) which form a multitude of microstructured flow channels which bring about multiple splitting of the liquid reaction mixture into component flow paths and recombination thereof in altered arrangement, the multiple splitting and recombination being repeated several times and the microstructured flow channels having a characteristic dimension which is defined as the greatest possible distance of any particle in the liquid reaction mixture from the wall of a flow channel closest to the particle, in the range from 20 to 10 000 μm, the result being that the flow profile of the liquid reaction mixture approximates to ideal plug flow as a result of the microstructured flow channels.
摘要翻译：提出的是通过以下反应物的转化来制备聚醚醇的方法：a）一种或多种环氧烷烃和任选的二氧化碳，和b）一种或多种H官能起始物质，在催化剂存在下，形成液体反应混合物，在反应单元（1）中，其特征在于反应单元（1）具有形成多个微结构流动通道的内部（2），其导致液体反应混合物多次分离成组分流动路径并且其重组在改变的布置中，多次分裂和重组被重复几次，并且微结构流动通道具有被定义为液体反应混合物中任何颗粒与流动通道的壁最接近的最大可能距离的特征尺寸颗粒在20至1000000范围内，其结果是液体反应混合物的流动分布近似于id 作为微结构化流动通道的结果，流动的流动。

6. 发明申请

US20140275633A1 CONTINUOUS PROCESS FOR THE PRODUCTION OF LOW MOLECULAR WEIGHT POLYETHERS WITH A DMC CATALYST 有权
标题翻译：用DMC催化剂生产低分子量聚乙烯的连续方法
公开(公告)号：US20140275633A1
公开(公告)日：2014-09-18
申请号：US13826394
申请日：2013-03-14
申请人： BAYER MATERIALSCIENCE LLC
发明人： Jack Reese , Paul Webb
IPC分类号： C07C41/02 , C07C41/03
CPC分类号： C07C41/03 , C08G65/2609 , C08G65/2663 , C08G65/2696
摘要： Low molecular weight polyoxyalkylene polyether polyols having a hydroxyl content of from about 3.4 to about 12.1% by weight, and OH numbers of from about 112 to about 400 are produced by a continuous process using a DMC catalyst. In the process of the present invention, oxyalkylation conditions are established in a continuous reactor in the presence of a DMC catalyst; alkylene oxide and a low molecular weight starter are continuously introduced into the continuous reactor; a partially oxyalkylated polyether polyol is recovered from the reactor; and the recovered partially oxyalkylated polyether polyol is allowed to further reactor until the unreacted alkylene oxide content of the mixture is reduced to 0.001% or less by weight. The alkoxylation of the present invention must be carried out a pressure sufficiently high to prevent deactivation of the DMC catalyst. Pressures of from 45 to 55 psia are preferred.
摘要翻译：通过使用DMC催化剂的连续方法制备羟基含量为约3.4至约12.1重量％，OH数为约112至约400的低分子量聚氧化烯聚醚多元醇。在本发明的方法中，在DMC催化剂存在下，在连续反应器中建立烷氧基化条件; 环氧烷和低分子量引发剂连续引入连续反应器中; 从反应器回收部分烷氧基化的聚醚多元醇; 将回收的部分烷氧基化聚醚多元醇进一步加入反应器中，直到混合物的未反应的烯化氧含量降低至0.001重量％以下。本发明的烷氧基化必须进行足够高的压力以防止DMC催化剂失活。压力为45至55psia是优选的。

7. 发明申请

US20130345476A1 PROCESS FOR THE PRODUCTION OF LOW MOLECULAR WEIGHT IMPACT POLYETHERS 审中-公开
标题翻译：生产低分子量重力聚合物的方法
公开(公告)号：US20130345476A1
公开(公告)日：2013-12-26
申请号：US13528909
申请日：2012-06-21
申请人： Jack R. Reese
发明人： Jack R. Reese
IPC分类号： C07C41/02 , C07C41/03
CPC分类号： C07C41/03 , C08G65/2609 , C08G65/2663 , C08G65/2696 , C08G65/30 , C07C43/11
摘要： This invention relates to an improved continuous process for the production of low molecular weight polyoxyalkylene polyether polyols. These polyoxyalkylene polyether polyols have a hydroxyl content of from about 3.4 to about 12.1% by weight, and may also be characterized as having an OH number of from about 112 to about 400. The process comprises establishing oxyalkylation conditions in a continuous reactor in the presence of a DMC catalyst; continuously introducing alkylene oxide and a low molecular weight starter into the continuous reactor; recovering a partially oxyalkylated polyether polyol from the reactor; and allowing the recovered partially oxyalkylated polyether polyol to further reactor until the unreacted alkylene oxide content of the mixture is reduced to 0.001% or less by weight.
摘要翻译：本发明涉及用于生产低分子量聚氧化烯聚醚多元醇的改进的连续方法。这些聚氧化烯聚醚多元醇具有约3.4至约12.1重量％的羟基含量，并且还可以表征为具有约112至约400的OH值。该方法包括在存在下在连续反应器中建立烷氧基化条件的DMC催化剂; 将环氧烷和低分子量起始剂连续引入连续反应器中; 从反应器中回收部分烷氧基化聚醚多元醇; 并将回收的部分烷氧基化聚醚多元醇进一步反应，直到混合物的未反应的烯化氧含量降低至0.001重量％以下。

8. 发明申请

US20130131389A1 PROCESS FOR PREPARING POLYETHER ALCOHOLS 有权
标题翻译：制备聚醚醇的方法
公开(公告)号：US20130131389A1
公开(公告)日：2013-05-23
申请号：US13813300
申请日：2011-08-08
申请人： Achim Loeffler , Michael Stoesser , Wolfgang Loth , Ralf Boehling , Sirus Zarbakhsh
发明人： Achim Loeffler , Michael Stoesser , Wolfgang Loth , Ralf Boehling , Sirus Zarbakhsh
IPC分类号： C07C41/02
CPC分类号： C07C41/02 , C08G65/2696
摘要： What is proposed is a process for preparing polyether alcohols by conversion of the following reactants: a) one or more alkylene oxides and optionally carbon dioxide and b) one or more H-functional starter substances, in the presence of a catalyst, to form a liquid reaction mixture, in a reaction unit (1), which is characterized in that the reaction unit (1) has internals (2) which form a multitude of microstructured flow channels which bring about multiple splitting of the liquid reaction mixture into component flow paths and recombination thereof in altered arrangement, the multiple splitting and recombination being repeated several times and the microstructured flow channels having a characteristic dimension which is defined as the greatest possible distance of any particle in the liquid reaction mixture from the wall of a flow channel closest to the particle, in the range from 20 to 10 000 μm, the result being that the flow profile of the liquid reaction mixture approximates to ideal plug flow as a result of the microstructured flow channels.
摘要翻译：提出的是通过以下反应物的转化来制备聚醚醇的方法：a）一种或多种环氧烷烃和任选的二氧化碳，和b）一种或多种H官能起始物质，在催化剂存在下，形成液体反应混合物，在反应单元（1）中，其特征在于反应单元（1）具有形成多个微结构流动通道的内部（2），其导致液体反应混合物多次分离成组分流动路径并且其重组在改变的布置中，多次分裂和重组被重复几次，并且微结构流动通道具有被定义为液体反应混合物中任何颗粒与流动通道的壁最接近的最大可能距离的特征尺寸该颗粒在20至1000000m范围内，结果是液体反应混合物的流动分布近似于id 作为微结构化流动通道的结果，流动的流动。

9. 发明申请

US20120259132A1 PROCESS TO PREPARE AN ETHANOL-DERIVATE 审中-公开
标题翻译：制备乙醇衍生物的方法
公开(公告)号：US20120259132A1
公开(公告)日：2012-10-11
申请号：US13440323
申请日：2012-04-05
申请人： Meindert Jan Lippits , Bernard Egbert Nieuwenhuijs
发明人： Meindert Jan Lippits , Bernard Egbert Nieuwenhuijs
IPC分类号： C07C1/20 , C07C41/14 , C07C27/00 , B01J37/02 , C07C209/00 , B01J23/02 , B01J23/72 , C07D301/22 , C07C41/02
CPC分类号： C07D301/22 , B01J21/04 , B01J23/50 , B01J23/52 , B01J23/66 , B01J23/72 , B01J23/78 , B01J23/83 , B01J23/94 , B01J23/96 , B01J35/0013 , B01J35/0033 , B01J35/006 , B01J35/1019 , B01J37/0201 , B01J37/031 , B01J38/38 , C07C1/24 , C07C41/09 , C07C45/38 , C07C2523/04 , C07C2523/10 , C07C2523/50 , C07C2523/52 , C07C2523/66 , C07C2523/72 , C07C2523/78 , C07C2523/83 , Y02P20/52 , Y02P20/584 , C07C43/06 , C07C47/06 , C07C11/04
摘要： The invention is directed to a process to prepare an ethanol-derivate compound or compounds by reacting ethanol in the presence of molecular oxygen and a catalyst comprising a gamma-alumina carrier, metal nano-particles wherein the metal is selected from silver, copper or gold. The invention is also directed to processes to prepare such a catalyst.
摘要翻译：本发明涉及通过在分子氧存在下使乙醇反应制备乙醇衍生化合物或化合物的方法，所述催化剂包括γ-氧化铝载体，金属纳米颗粒，其中金属选自银，铜或金。本发明还涉及制备这种催化剂的方法。

10. 发明申请

US20120101308A1 METHOD FOR THE PHOSPHINE-INITIALIZED PRODUCTION OF HYPERBRANCHED POLYOLS 有权
标题翻译：磷酸二氢钠多酚生产方法
公开(公告)号：US20120101308A1
公开(公告)日：2012-04-26
申请号：US13380470
申请日：2010-06-30
申请人： Sabrina Montero Pancera , Bernhard Rieger , Thomas Manfred Gunesch
发明人： Sabrina Montero Pancera , Bernhard Rieger , Thomas Manfred Gunesch
IPC分类号： C07C41/02
CPC分类号： C08G65/22 , C08G65/10
摘要： A process for preparing hyperbranched polyols by reacting epoxy alcohols in the presence of phosphines.
摘要翻译：一种通过在膦存在下使环氧醇反应来制备超支化多元醇的方法。

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