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1. 发明授权

US11447870B2 Method for forming water repellent, long-term durable and biomimetic coatings from methyltrimethoxysilane 有权
公开(公告)号：US11447870B2
公开(公告)日：2022-09-20
申请号：US16962003
申请日：2019-01-16
申请人： Georgia Tech Research Corporation
发明人： Cornelia Rosu , Laurens Victor Breedveld , Dennis W. Hess
IPC分类号： C23C18/00 , C23C18/12 , D06M13/503 , D06M13/513
摘要： Embodiments of the present disclosure relates generally to methods of providing biomimetic superhydrophobic coatings to substrates, and more specifically to providing biomimetic inorganic silica or silane-based coatings that enable tunable hierarchical surface structures with high coating-to-substrate adhesion, resistance to various mechanical abradents, durability, shelf stability, and enhanced non-wettability or water-repellency.

2. 发明授权

US11441228B2 Thermal spray powder 有权
公开(公告)号：US11441228B2
公开(公告)日：2022-09-13
申请号：US16697978
申请日：2019-11-27
申请人： TOYOTA JIDOSHA KABUSHIKI KAISHA
发明人： Noritaka Miyamoto
IPC分类号： B22F7/00 , C23C24/08 , C09D5/00 , C09D5/10 , C23C16/00 , C23C18/00
摘要： A thermal spray powder according to the present disclosure is a thermal spray powder which is used to form a thermal spray film having a characteristic of abradability, the thermal spray powder includes Ni alloy particles, solid lubricant particles, and aluminum flakes, the content of oxygen in the aluminum flakes is within a range of 0.29 mass % to 4.1 mass %, and the coverage of aluminum flakes on the surfaces of the Ni alloy particles is within a range of 60% to 100%.

3. 发明授权

US11047049B2 Low temperature method of forming layered HT-LiCoO2 有权
公开(公告)号：US11047049B2
公开(公告)日：2021-06-29
申请号：US15631723
申请日：2017-06-23
申请人： International Business Machines Corporation
发明人： Kevin W. Brew , Saurabh Singh , Teodor K. Todorov
IPC分类号： C23C18/00 , C23C18/12 , H01M4/04 , H01M4/525 , B01J23/78 , H01M10/0562 , H01M10/0525 , H01M4/131 , H01M4/1391
摘要： Low temperature techniques for forming layered lithium cobalt oxide (LCO) are provided. In one aspect, a method of synthesizing layered LCO includes: forming a metal catalyst layer (e.g., platinum) on a substrate; depositing LCO onto the metal catalyst layer; and annealing the LCO under conditions sufficient to form the layered LCO on the metal catalyst layer. An adhesion layer can be deposited on the substrate, and the metal catalyst layer can be deposited onto the adhesion layer. In another aspect, a structure is provided including: a substrate; a metal catalyst layer (e.g., platinum) disposed on the substrate; and layered LCO formed on the metal catalyst layer. An adhesion layer can be disposed between the substrate and the metal catalyst layer.

4. 发明授权

US10253414B2 Liquid phase atomic layer deposition 有权
公开(公告)号：US10253414B2
公开(公告)日：2019-04-09
申请号：US14871619
申请日：2015-09-30
申请人： Tokyo Electron Limited
发明人： Robert D. Clark
IPC分类号： B05D1/36 , B05D3/12 , C23C18/00 , B05D1/00 , B05D7/00 , B05D1/38
摘要： A processing system and method for depositing a film on a substrate by liquid phase ALD is disclosed in various embodiments. The method includes providing the substrate in a process chamber, spinning on the substrate a first reactant in a first liquid to form a self-limiting layer of the first reactant on the substrate, spinning on the substrate a second reactant in a second liquid, where the second reactant reacts with the self-limiting layer of the first reactant on the substrate to form a film on the substrate, and repeating the spinning steps at least once until the film has a desired thickness. Other embodiments of the invention further include rinsing the substrate to remove excess first and second reactants from the substrate, and heat-treating the substrate during and/or following the film deposition.

5. 发明授权

US10119036B2 Process for the formation of metal oxide nanoparticles coating of a solid substrate 有权
公开(公告)号：US10119036B2
公开(公告)日：2018-11-06
申请号：US13821279
申请日：2011-09-07
申请人： Ovadia Lev , Sergey Sladkevich , Petr Prikhodchenko , Genia Gun
发明人： Ovadia Lev , Sergey Sladkevich , Petr Prikhodchenko , Genia Gun
IPC分类号： B05D3/02 , C09D5/24 , B01J23/14 , B01J23/18 , B01J27/057 , B01J35/00 , B01J37/02 , B05D1/00 , B82Y30/00 , C01B15/04 , C01B15/047 , C04B41/00 , C23C18/00 , C23C18/12 , C01B32/00 , B01J21/08 , B01J21/16
摘要： The present invention provides a process for the formation of a coating comprising peroxynanoparticles of metals selected from the group consisting of: Ga, Ge, As, Se, In, Sn, Sb, Te, Tl, Pb and Bi on a solid substrate, comprising providing a basic solution containing at least a first metal selected from said group and hydrogen peroxide, and contacting said solution with a solid substrate having oxygen-containing chemically reactive groups on its surface.

6. 发明授权

US10033035B2 Method for producing active material composite particles 有权
公开(公告)号：US10033035B2
公开(公告)日：2018-07-24
申请号：US15017129
申请日：2016-02-05
申请人： TOYOTA JIDOSHA KABUSHIKI KAISHA
发明人： Takayuki Uchiyama , Masahiro Iwasaki , Hirokazu Kawaoka
IPC分类号： H01M4/36 , C23C16/56 , H01M4/485 , H01M4/04 , H01M4/1391 , C23C18/00
摘要： An object of the present invention is to provide a method for producing active material composite particles having a dense coating layer. In the present invention, the above object is achieved by providing a method for producing an active material composite particle, the method comprising steps of: a coating step of coating a surface of an active material with a precursor solution of a Li ion conductive oxide to form a precursor layer; a heat treatment step of performing heat treatment on the precursor layer to form a coating layer comprising the Li ion conductive oxide; and a compression shearing treatment step of performing compression shearing treatment on the coating layer.

7. 发明授权

US09644484B2 System and method for providing a film treatment to a surface using inlet bleed heat manifold 有权
公开(公告)号：US09644484B2
公开(公告)日：2017-05-09
申请号：US14485072
申请日：2014-09-12
申请人： General Electric Company
发明人： Sanji Ekanayake , Alston Ilford Scipio
IPC分类号： B05D7/22 , F01D5/28 , B05D3/00 , C23C18/00 , F02C7/30
CPC分类号： F01D5/288 , B05D3/002 , B05D5/08 , B05D7/22 , C23C18/00 , F02C7/30 , F05D2220/32 , F05D2230/90 , F05D2260/95 , F05D2270/11
摘要： Disclosed herein are systems and methods for treating a surface, such as a gas turbine surface, with a filming agent using an inlet bleed heat manifold. A filming control system includes a storage tank configured to contain a filming agent; an inlet bleed heat manifold; and a supply conduit coupled to the storage tank on a first end and the inlet bleed heat manifold on a second end; wherein the filming control system is configured to deliver the filming agent from the storage tank and to discharge the filming agent through the inlet heat bleed manifold and the filming agent includes siloxane, fluorosilane, mercapto silane, amino silane, tetraethyl orthosilicate, succinic anhydride silane, or a combination including at least one of the foregoing.

8. 发明授权

US09567686B2 Aluminum oxide film remover and method for surface treatment of aluminum or aluminum alloy 有权
标题翻译：铝或铝合金表面处理的氧化铝膜去除剂和方法
公开(公告)号：US09567686B2
公开(公告)日：2017-02-14
申请号：US13167075
申请日：2011-06-23
申请人： Toshiaki Shibata , Yoshihito Ii , Hiromu Inagawa
发明人： Toshiaki Shibata , Yoshihito Ii , Hiromu Inagawa
IPC分类号： C23C18/16 , C25D5/44 , C23C18/18 , C23C18/54 , C23G1/22 , C23C18/00
CPC分类号： C25D5/44 , C23C18/1601 , C23C18/1635 , C23C18/1651 , C23C18/18 , C23C18/1824 , C23C18/54 , C23G1/22
摘要： Disclosed herein is an aluminum oxide film remover for removing an oxide film on the surface of aluminum or aluminum alloy, which comprises silver ions and/or copper ions, a solubilizing agent for silver ions and/or copper ions, and a quaternary ammonium hydroxide compound, and has a pH value of 10 to 13.5. A method for surface treatment of aluminum or aluminum alloy is also disclosed, which comprises immersing a workpiece having aluminum or aluminum alloy at least on the surface thereof in the aluminum oxide film remover, and depositing the silver and/or copper contained in the remover on the surface of aluminum or aluminum alloy while removing the aluminum oxide film.
摘要翻译：本发明公开了一种用于除去铝或铝合金表面上的氧化物膜的氧化铝膜去除剂，其包含银离子和/或铜离子，银离子和/或铜离子的增溶剂和季铵氢氧化物，pH值为10〜13.5。还公开了一种用于铝或铝合金表面处理的方法，其中包括至少在其氧化铝膜去除剂的表面上浸入具有铝或铝合金的工件，并将包含在除去器中的银和/或铜沉积在铝或铝合金的表面，同时去除氧化铝膜。

9. 发明授权

US09276234B2 Method of preparing organic light emitting device 有权
标题翻译：制备有机发光装置的方法
公开(公告)号：US09276234B2
公开(公告)日：2016-03-01
申请号：US13607311
申请日：2012-09-07
申请人： Jin-Woo Park
发明人： Jin-Woo Park
IPC分类号： C23C14/00 , C23C18/00 , H01L51/52
CPC分类号： H01L51/5253
摘要： A method of preparing an organic light-emitting device includes forming an organic emission unit on a substrate, and forming a thin film encapsulation layer that contacts an environmental element, and that includes at least one inorganic layer including a low temperature viscosity transition (LVT) inorganic material, wherein the inorganic layer is formed using a process including forming a pre-inorganic layer including the LVT inorganic material by providing the LVT inorganic material onto the organic emission unit on which the environmental element is located, performing a first healing process on the pre-inorganic layer at a temperature greater than a viscosity transition temperature of the LVT inorganic material, and performing a second healing process on the pre-inorganic layer having undergone the first healing process to increase a binding force between the environmental element and the LVT inorganic material, and to increase a binding force among the LVT inorganic material.
摘要翻译：一种制备有机发光器件的方法包括在衬底上形成有机发射单元，并形成与环境元件接触的薄膜封装层，并且包括至少一个包含低温粘度转变（LVT）的无机层，无机材料，其中使用包括通过将LVT无机材料提供到环境要素所位于的有机发射单元上的形成包含LVT无机材料的预无机层的方法形成无机层，对其进行第一愈合处理在大于LVT无机材料的粘度转变温度的温度下的预无机层，并且对已经经历第一愈合过程的前无机层进行第二愈合处理，以增加环境元素和LVT无机物之间的结合力材料，并增加LVT无机材料之间的结合力。

10. 发明授权

US09139929B2 Dehydration of alcohols on a crystalline silicate of low Si/Al ratio 有权
标题翻译：在低Si / Al比的结晶硅酸盐上脱醇
公开(公告)号：US09139929B2
公开(公告)日：2015-09-22
申请号：US13522619
申请日：2011-01-21
申请人： Delphine Minoux , Nikolai Nesterenko , Cindy Adam , Sander Van Donk , Walter Vermeiren
发明人： Delphine Minoux , Nikolai Nesterenko , Cindy Adam , Sander Van Donk , Walter Vermeiren
IPC分类号： C07C1/22 , C25D7/06 , C23C18/00 , C25D17/00
CPC分类号： C07C1/24 , B01J29/65 , B01J29/90 , B01J2229/16 , B01J2229/36 , C07C2529/65 , C07C2529/70 , C07C2529/85 , C23C18/00 , C25D7/0664 , C25D17/00 , Y02P20/52 , Y02P20/584 , C07C11/04
摘要： The present invention (in a first embodiment) relates to a process for the dehydration of an alcohol having at least 2 carbon atoms to make the corresponding olefin, comprising: introducing in a reactor a stream (A) comprising at least an alcohol, optionally water, optionally an inert component, contacting said stream with a catalyst in said reactor at conditions effective to dehydrate at least a portion of the alcohol to make an olefin, recovering from said reactor an olefin containing stream (B), Wherein, the catalyst is a crystalline silicate of the group FER, MWW, EUO, MFS, ZSM-48, MIT or TON having Si/Al under 100, or a dealuminated crystalline silicate of the group FER, MWW, EUO, MFS, ZSM-48, MTT or TON having Si/Al under 100, or a phosphorus modified crystalline silicate of the group FER, MWW, EUO, MFS, ZSM-48, MTT or TON having Si/Al under 100, the WHSV of the alcohol is at least 4 h−1 and/or the temperature ranges from 320° C. to 600° C.
摘要翻译：本发明（在第一实施方案中）涉及使具有至少2个碳原子的醇脱水以制备相应烯烃的方法，包括：在反应器中引入至少包含醇，任选的水，任选的惰性组分，在所述反应器中使所述料流与催化剂接触，在有效使至少一部分醇脱水以制备烯烃的条件下，从所述反应器回收含烯烃的料流（B），其中催化剂为具有Si / Al低于100的组FER，MWW，EUO，MFS，ZSM-48，MIT或TON的结晶硅酸盐，或FER，MWW，EUO，MFS，ZSM-48，MTT或TON组的脱铝结晶硅酸盐 Si / Al低于100，或具有Si / Al低于100的FER，MWW，EUO，MFS，ZSM-48，MTT或TON的磷改性结晶硅酸盐，醇的WHSV为至少4h -1 和/或温度范围为320℃至600℃。

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