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1. 发明授权

US11203726B1 Diamondoid fuels 有权
公开(公告)号：US11203726B1
公开(公告)日：2021-12-21
申请号：US16835639
申请日：2020-03-31
申请人： The United States of America, as represented by the Secretary of the Navy
发明人： Benjamin G. Harvey , Matthew C. Davis
IPC分类号： C10L1/04 , C07C13/615 , C07C7/14 , C10L1/00 , C07C7/11 , C07C2/86 , C07C7/04 , C07C2/56 , C08L45/00 , C07C22/00 , C06B43/00 , C10L10/12
摘要： A diamondoid fuel comprising a cage structure including 10, 14, 18, or 22 carbons. The diamondoid fuel also includes one of one to four cyclopropyl groups bonded to the cage structure or two to four functional groups bonded to the cage structure where the functional groups are an alkyl group, an allyl group, a cyclopropyl group, or combinations thereof. Additionally, at least one functional group is an allyl group and at least one functional group is a cyclopropyl group.

2. 发明授权

US10710941B1 Diamondoid fuels 有权
公开(公告)号：US10710941B1
公开(公告)日：2020-07-14
申请号：US16178273
申请日：2018-11-01
申请人： The United States of America, as Represented by the Secretary of the Navy
发明人： Benjamin G. Harvey , Matthew C. Davis
IPC分类号： C07C13/615 , C07C22/00 , C07C2/56 , C07C2/86 , C08L45/00 , C07C7/11 , C07C7/04 , C07C7/14
摘要： A diamondoid fuel comprising a cage structure including 10, 14, 18, or 22 carbons. The diamondoid fuel also includes one of one to four cyclopropyl groups bonded to the cage structure or two to four functional groups bonded to the cage structure where the functional groups are an alkyl group, an allyl group, a cyclopropyl group, or combinations thereof. Additionally, at least one functional group is an allyl group and at least one functional group is a cyclopropyl group.

3. 发明授权

US10023535B2 Method for the preparation of 1-(2-halogen-ethyl)-4 piperidine-carboxylic acid ethyl esters 有权
公开(公告)号：US10023535B2
公开(公告)日：2018-07-17
申请号：US15520256
申请日：2015-10-22
申请人： LABORATORIO CHIMICO INTERNAZIONALE S.P.A.
发明人： Giorgio Bertolini , Corrado Colli , Aldo Bianchi , Federica Colombo , Stefano Maiorana , Filippo Nisic
IPC分类号： C07D211/62 , C07C22/00 , C07F13/00 , C07D211/06 , C07C209/24
摘要： The present invention refers to a process for the preparation of 1-(2-halogen-ethyl)-4-piperidinecarboxylic acid ethyl esters, in particular of 1-(2-chloroethyl)-4 piperidinecarboxylic acid ethyl ester, a versatile synthesis intermediate, particularly useful as an intermediate compound in the synthesis of umeclidinium.

4. 发明授权

US09133396B2 Liquid crystal compound having negative dielectric anisotropy, and liquid crystal composition 有权
标题翻译：具有负介电各向异性的液晶化合物和液晶组合物
公开(公告)号：US09133396B2
公开(公告)日：2015-09-15
申请号：US14048546
申请日：2013-10-08
申请人： DAXIN MATERIALS CORP.
发明人： Chun-Chih Wang , Yu-Ying Hsieh , Hui-Ju Yu
IPC分类号： C09K19/12 , C09K19/00 , C07C43/20 , C07C22/00 , C09K19/30
CPC分类号： C09K19/30
摘要： A liquid crystal composition includes a liquid crystal compound having a formula (I), where R1 and R2 are independently selected from the group consisting of H, C1-C10 alkyl, C2-C10 alkenyl, C1-C10 alkoxyl, C2-C10 alkenyloxy, C1-C10 ether, C1-C10 aldehyde, C1-C10 ketone, and C1-C10 ester; A is selected from the group consisting of and X1, X2, X3 and X4 are independently selected from the group consisting of H, halogen group, —CF3, —CHF2, —CH2F, —OCF3, —OCHF2 and —OCH2F, at least one of X1, X2, X3 and X4 being halogen group, —CF3, —CHF2, —CH2F, —OCF3, —OCHF2 or —OCH2F.
摘要翻译：液晶组合物包括具有式（I）的液晶化合物，其中R 1和R 2独立地选自H，C 1 -C 10烷基，C 2 -C 10链烯基，C 1 -C 10烷氧基，C 2 -C 10链烯氧基， C1-C10醚，C1-C10醛，C1-C10酮和C1-C10酯; A选自X 1，X 2，X 3和X 4独立地选自H，卤素基，-CF 3，-CHF 2，-CH 2 F，-OCF 3，-OCHF 2和-OCH 2 F，至少一个 X 1，X 2，X 3和X 4为卤素基团，-CF 3，-CHF 2，-CH 2 F，-OCF 3，-OCHF 2或-OCH 2 F。

5. 发明申请

US20150010724A1 FLUOROCARBON, METHOD FOR PREPARING FLUOROCARBON, AND USE THEREOF 审中-公开
标题翻译：氟代烷，氟代烃的制备方法及其用途
公开(公告)号：US20150010724A1
公开(公告)日：2015-01-08
申请号：US14315890
申请日：2014-06-26
申请人： Tokyo Ohka Kogyo Co., Ltd.
发明人： Toshiyuki Ogata , Yasuo Suzuki , Atsushi Matsushita , Tatsuhiro Mitake
IPC分类号： C09J7/02 , C07C22/00 , C09D7/12
CPC分类号： C09J7/401 , C08K5/01 , C08K2201/011 , C09J2427/005 , Y10T428/1429 , Y10T428/2982
摘要： A fluorocarbon including fluorine and carbon in which d50 in a cumulative particle size distribution is 1.0 nm or greater and 4.0 nm or less. A method for producing the fluorocarbon includes a plasma treatment process of generating radicals by producing inductively coupled plasma (ICP) using a fluorocarbon gas.
摘要翻译：包含氟和碳的碳氟化合物，其中累积粒度分布中的d50为1.0nm以上且4.0nm以下。碳氟化合物的制造方法包括使用碳氟化合物气体生成电感耦合等离子体（ICP）来产生自由基的等离子体处理工序。

6. 发明授权

US08822516B2 Process for the preparation of iodides 有权
标题翻译：制备碘化物的方法
公开(公告)号：US08822516B2
公开(公告)日：2014-09-02
申请号：US13703183
申请日：2011-06-09
申请人： Gennady Nisnevich , Mark Gandelman , Kseniya Kulbitski
发明人： Gennady Nisnevich , Mark Gandelman , Kseniya Kulbitski
IPC分类号： A01N43/76 , A61K31/42 , C07D205/04 , C07D263/00 , C07C67/32 , C07C22/00 , C07J9/00
CPC分类号： C07C17/093 , C07C41/22 , C07C67/32 , C07C201/12 , C07C269/06 , C07C2601/02 , C07C2601/04 , C07C2603/62 , C07C2603/90 , C07D205/04 , C07D211/38 , C07J9/00 , C07J9/005 , C07C19/075 , C07C22/04 , C07C25/22 , C07C25/18 , C07C22/00 , C07C19/07 , C07C25/02 , C07C23/46 , C07C43/225 , C07C69/753 , C07C69/74 , C07C69/76 , C07C205/11 , C07C271/22
摘要： This invention is directed to a process for the preparation of high yield alkyl or aryl iodide from its corresponding carboxylic acid using N-iodo amides.
摘要翻译：本发明涉及使用N-碘酰胺从其相应的羧酸制备高产率烷基或芳基碘的方法。

7. 发明授权

US08557142B2 Compounds for a liquid crystal medium and high-frequency components containing said liquid crystal medium 有权
标题翻译：用于液晶介质的化合物和含有所述液晶介质的高频成分
公开(公告)号：US08557142B2
公开(公告)日：2013-10-15
申请号：US13497909
申请日：2010-09-01
申请人： Elvira Montenegro , Christian Jasper , Detlef Pauluth , Volker Reiffenrath , Atsutaka Manabe
发明人： Elvira Montenegro , Christian Jasper , Detlef Pauluth , Volker Reiffenrath , Atsutaka Manabe
IPC分类号： C09K19/30 , C09K19/06 , C09K19/52 , C09K19/00 , C07C19/08 , C07C22/00 , C07C25/00 , C07C25/13 , C07C15/12 , H01Q21/00
CPC分类号： C09K19/18 , C09K19/30 , C09K19/3001 , C09K2019/0407 , C09K2019/183 , C09K2019/186 , C09K2219/11
摘要： The present invention relates to bistolans of the formula I where one or more of the radicals L1 to L3 denote an Rx, where Rx denotes cyclopropyl, cyclobutyl, cyclopentyl or cyclohexyl, and the other parameters are as defined in Claim 1. The invention also encompasses liquid-crystalline media which comprise the title compounds, to components for high-frequency technology which comprise these media, in particular phase shifters and microwave array antennae.
摘要翻译：本发明涉及式I的双酚A，其中一个或多个基团L1至L3表示Rx，其中Rx表示环丙基，环丁基，环戊基或环己基，其它参数如权利要求1中所定义。本发明还包括包含标题化合物的液晶介质，包括这些介质的高频技术部件，特别是移相器和微波阵列天线。

8. 发明授权

US08415468B2 Process for the synthesis of ivabradine and addition salts thereof with a pharmaceutically acceptable acid 有权
标题翻译：将伊伐布拉德及其加成盐与药学上可接受的酸合成的方法
公开(公告)号：US08415468B2
公开(公告)日：2013-04-09
申请号：US13138333
申请日：2010-02-03
申请人： Jean-Louis Peglion , Aimee Dessinges , Bernard Serkiz , Jean-Michel Lerestif , Jean-Pierre Lecouve
发明人： Jean-Louis Peglion , Aimee Dessinges , Bernard Serkiz , Jean-Michel Lerestif , Jean-Pierre Lecouve
IPC分类号： C07D223/16 , C07C303/00 , C07C22/00
CPC分类号： C07D223/16
摘要： Process for the synthesis of ivabradine of formula (I): and addition salts thereof with a pharmaceutically acceptable acid.
摘要翻译：用于合成式（I）的伊伐布拉定的方法及其与药学上可接受的酸的加成盐。

9. 发明授权

US08212090B2 Methods for silver-promoted fluorination of organic molecules 失效
标题翻译：银促进氟化有机分子的方法
公开(公告)号：US08212090B2
公开(公告)日：2012-07-03
申请号：US12634816
申请日：2009-12-10
申请人： Christopher C. Caires , Samira Guccione
发明人： Christopher C. Caires , Samira Guccione
IPC分类号： C07C22/00
CPC分类号： C07C17/206 , C07C22/08
摘要： The methods of the disclosure may be used for the fluorination of organic compounds, and in particular aryl organic compounds other than just benzyl halogens. It is within the scope of the present disclosure, for organic compounds comprising an electrophilic carbon atom and a halogen leaving group to be fluorinated by the methods of the disclosure. One aspect of the disclosure provides methods of introducing a fluorine atom onto an electrophilic carbon atom, comprising mixing an insoluble basic silver salt, an organic molecule containing a leaving group, an aqueous solution of hydrofluoric acid, and a polar solvent:water composition; incubating said mixture at a temperature of about 20° C. to about 35° C., thereby obtaining a fluorinated organic product.
摘要翻译：本公开的方法可用于有机化合物的氟化，特别是除苄基卤素以外的芳基有机化合物。对于通过本公开的方法，包含亲电子碳原子和待离去氟基的卤素离去基团的有机化合物在本公开的范围内。本发明的一个方面提供了将氟原子引入到亲电子碳原子上的方法，包括混合不溶性碱性银盐，含有离去基团的有机分子，氢氟酸水溶液和极性溶剂：水组合物; 在约20℃至约35℃的温度下温育所述混合物，由此得到氟化有机产物。

10. 发明授权

US08088960B2 Process for the production of substituted bromobenzenes 失效
标题翻译：制备取代溴苯的方法
公开(公告)号：US08088960B2
公开(公告)日：2012-01-03
申请号：US12446793
申请日：2007-10-08
申请人： Beat Jau , Colin Ellis , Linhua Wang
发明人： Beat Jau , Colin Ellis , Linhua Wang
IPC分类号： C07C17/00 , C07C22/00
CPC分类号： C07C25/02 , C07C17/093 , C07C25/13
摘要： The present invention relates to a process for the production of compounds of formula (I) wherein X is fluoro, chloro, bromo or iodo and n is 1, 2, 3 or 4, which process comprises reacting a compound of formula (II) wherein the substituents are as defined for formula (I), with inorganic nitrite in an acidic aqueous medium in the presence of bromide and a copper catalyst and wherein the process is carried out as a one-pot reaction.
摘要翻译：本发明涉及制备式（I）化合物的方法，其中X为氟，氯，溴或碘，n为1,2,3或4，该方法包括使式（II）化合物与取代基如式（I）所定义，无机亚硝酸盐在酸性水性介质中，在溴化物和铜催化剂存在下，其中该方法作为一锅反应进行。

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