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1. 发明申请

US20180086738A1 PYRAZOLE COMPOUNDS OR SALTS THEREOF, PREPARATION METHOD THEREFOR, HERBICIDAL COMPOSITION AND USE THEREOF 审中-公开
公开(公告)号：US20180086738A1
公开(公告)日：2018-03-29
申请号：US15562633
申请日：2016-03-04
申请人： Qingdao Kingagroot Chemical Compounds Co., Ltd.
发明人： Lei Lian , Yurong Zheng , Song Li , Xuegang Peng , Tao Jin , Qi Cui
IPC分类号： C07D403/12 , C07D403/10 , C07D231/18 , C07D231/12 , C07C22/04 , C07C23/08 , A01N43/56
CPC分类号： C07D403/12 , A01N25/00 , A01N43/56 , C07C22/04 , C07C23/08 , C07D231/12 , C07D231/18 , C07D231/20 , C07D401/14 , C07D403/10
摘要： Disclosed are a pyrazole compound or a salt thereof, a preparation method therefor, a herbicidal composition and use thereof. The pyrazole compound or a salt thereof has a structure as shown in formula (I): wherein, R represents wherein, R′, R″, and R′″ represent hydrogen, C1-C4 alkyl, C1-C4 halogenated alkyl, C1-C4 alkoxy or halogen, R′, R″, and R′″ may be the same or different; R1 represents C1-C3 alkyl; R2 represents hydrogen or C1-C4 alkyl; R3 represents hydrogen or C1-C6 alkyl, optionally substituted phenyl, optionally substituted pyridyl, optionally substituted alkenyl, optionally substituted alkynyl, C1-C6 alkyl carbonyl, C1-C6 alkoxyl carbonyl, C1-C6 alkyl carbonyl methyl, etc. A compound having a pyrazole structure not only has excellent herbicidal effect on barnyard grass, but also is safe to rice in post-emergence application. More surprisingly, it also has good control efficacy on barnyard grass resistant to major herbicides, such as penoxsulam, quinclorac, cyhalofop-butyl, propanil, etc.

2. 发明授权

US09850268B2 Metathesis catalysts and methods thereof 有权
公开(公告)号：US09850268B2
公开(公告)日：2017-12-26
申请号：US14933741
申请日：2015-11-05
申请人： Massachusetts Institute of Technology , Trustees of Boston College
发明人： Amir H. Hoveyda , Hanmo Zhang , Ming Joo Koh , Richard Royce Schrock
IPC分类号： C07C17/275 , C07C45/63 , C07C37/62 , B01J31/22 , C07F11/00 , C07D333/54 , C07D209/10 , C07D209/48 , C07F5/02 , C07F7/18 , C07C17/266 , C07C17/269 , C07C17/278 , C07C17/10 , C07C17/14 , C07C17/361 , C07B37/04 , C07C17/02 , C07J9/00 , C07J51/00 , C07C67/307 , C07C67/333 , C07C41/30
CPC分类号： C07F11/00 , B01J31/2265 , B01J2231/543 , B01J2531/64 , B01J2531/66 , C07B37/04 , C07C17/02 , C07C17/10 , C07C17/14 , C07C17/266 , C07C17/269 , C07C17/275 , C07C17/278 , C07C17/361 , C07C21/14 , C07C21/18 , C07C22/08 , C07C37/62 , C07C41/30 , C07C45/63 , C07C67/307 , C07C67/333 , C07C69/753 , C07C2601/14 , C07C2603/26 , C07D209/10 , C07D209/48 , C07D333/54 , C07F5/025 , C07F7/1804 , C07J9/00 , C07J51/00 , C07C21/19 , C07C21/04 , C07C25/24 , C07C22/04 , C07C22/00 , C07C22/02 , C07C25/28 , C07C43/225 , C07C43/192 , C07C43/17 , C07C69/65 , C07C69/63
摘要： The present application provides, among other things, compounds and methods for metathesis reactions. In some embodiments, the present disclosure provides methods for preparing alkenyl halide with regioselectivity and/or stereoselectivity. In some embodiments, the present disclosure provides methods for preparing alkenyl halide with regioselectivity and Z-selectivity. In some embodiments, the present disclosure provides methods for preparing alkenyl halide with regioselectivity and E-selectivity. In some embodiments, provided technologies are particularly useful for preparing alkenyl fluorides. In some embodiments, a provided compound useful for metathesis reactions has the structure of formula II-a. In some embodiments, a provided compound useful for metathesis reactions has the structure of formula II-b.

3. 发明申请

US20170204022A1 Method for the Preparation of Iodoalkanes 审中-公开
公开(公告)号：US20170204022A1
公开(公告)日：2017-07-20
申请号：US15406029
申请日：2017-01-13
申请人： Hong Kong Baptist University , Yunnan Minzu University
发明人： Zhaoxiang BIAN , Baomin FAN , Chengyuan LIN , Yongyun ZHOU , Jingchao CHEN
IPC分类号： C07B39/00 , C07C17/04 , C07C41/22 , C07C17/02
CPC分类号： C07C41/22 , C07C17/02 , C07C17/04 , C07C17/08 , C07C17/087 , C07C19/07 , C07C22/04 , C07C23/18 , C07C22/00 , C07C23/16 , C07C25/02 , C07C25/13 , C07C43/225
摘要： The present invention relates to an atom economic procedure of preparing iodoalkanes by hydroiodination of alkenes. In particular the present method features the generation of anhydrous hydrogen iodide from atomic hydrogen and iodine in situ by using transition metal precursor and phosphine ligandcatalyst.

4. 发明申请

US20160289350A1 ELECTRORESPONSIVE TECHNOLOGY 审中-公开
标题翻译：电子科技
公开(公告)号：US20160289350A1
公开(公告)日：2016-10-06
申请号：US15034359
申请日：2014-11-14
申请人： NORTH CAROLINA CENTRAL UNIVERSITY
发明人： Darlene K. TAYLOR , Uddhav BALAMI
IPC分类号： C08F12/30 , C08F12/32 , G01N27/327 , C07C43/23
CPC分类号： C08F12/30 , C07C17/16 , C07C29/147 , C07C43/23 , C07C2603/90 , C08F8/36 , C08F12/22 , C08F12/32 , G01N27/3277 , G01N27/3335 , C07C33/20 , C07C22/04
摘要： A styrene based water soluble polymer containing pendant sulfonated calix[4]arene groups has been synthesized by using free radical polymerization combined with post-polymerization sulfonation chemistry. The monomer 25-(4-vinylbenzyl)-26,27,28-hydroxy-calix[4]arene was prepared in 3 steps: (1) reduction of 4-vinyl benzoic acid to the respective alcohol (2) formation of the bromide by the Appel reaction and (3) synthesis of the respective ether by Williamson O-alkylation reaction with calix[4]arene. Polymerization was accomplished by azobisisobutyronitrile (AIBN) initiated free radical polymerization technique. Electro-responsive properties of the sulfonated polymer were studied wherein a response to electrochemical stimulus is observed when guest molecules of methyl viologen are incorporated with polymerized 25-(4-vinylbenzyl)-26,27,28-hydroxy-calix[4]arene.
摘要翻译：通过与后聚合磺化化学结合使用自由基聚合，合成了含有侧链磺化杯[4]芳烃基的苯乙烯基水溶性聚合物。单体25-（4-乙烯基苄基）-26,27,28-羟基 - 杯[4]芳烃分三个步骤制备：（1）将4-乙烯基苯甲酸还原成相应的醇（2）溴化物的形成通过Appel反应和（3）通过与杯[4]芳烃的Williamson O-烷基化反应合成各自的醚。聚合由偶氮二异丁腈（AIBN）引发的自由基聚合技术完成。研究了磺化聚合物的电响应性质，其中当甲基紫精的客体分子与聚合的25-（4-乙烯基苄基）-26,27,28-羟基 - 杯[4]芳烃结合时，观察到对电化学刺激的响应。

5. 发明申请

US20160272598A1 PROCESS FOR THE PREPARATION OF N-IODOAMIDES 有权
标题翻译：制备N-碘代的方法
公开(公告)号：US20160272598A1
公开(公告)日：2016-09-22
申请号：US15034751
申请日：2014-11-05
申请人： TECHNION RESEARCH & DEVELOPMENT FOUNDATION LIMITED
发明人： Gennady NISNEVICH , Kseniya KULBITSKI , Mark GANDELMAN
IPC分类号： C07D263/26 , C07D209/48 , C07D207/46 , C07D233/82 , C07D275/06
CPC分类号： C07D263/26 , C07B39/00 , C07C17/093 , C07C17/10 , C07C17/12 , C07C17/14 , C07C17/363 , C07C29/64 , C07C41/05 , C07C41/22 , C07C67/05 , C07C201/12 , C07C2601/08 , C07C2601/14 , C07C2601/16 , C07C2601/18 , C07C2602/42 , C07D207/46 , C07D209/48 , C07D211/38 , C07D233/74 , C07D233/82 , C07D263/22 , C07D275/06 , C07C43/225 , C07C35/48 , C07C43/192 , C07C33/46 , C07C43/174 , C07C69/63 , C07C22/04 , C07C25/02 , C07C205/12 , C07C25/13 , C07C205/11 , C07C23/10 , C07C23/28 , C07C23/08 , C07C23/14 , C07C23/16 , C07C19/07
摘要： The present invention provides new stable crystalline N-iodoamides -1-iodo-3,5,5-trimethylhydantoin (1-ITMH) and 3-iodo-4,4-dimethyl-2-oxazolidinone (IDMO). The present invention further provides a process for the preparation of organic iodides using N-iodoamides of this invention and recovery of the amide co-products from waste water.
摘要翻译：本发明提供新的稳定的N-碘代酰胺-N-碘代-3,5,5-三甲基乙内酰脲（1-ITMH）和3-碘-4,4-二甲基-2-恶唑烷酮（IDMO）。本发明还提供了使用本发明的N-碘代酰胺制备有机碘化物并从废水中回收酰胺共同产物的方法。

6. 发明申请

US20160152533A1 METHOD FOR THE PREPARATION OF TRICHLOROMETHYL-GROUP-SUBSTITUTED BENZENE 有权
标题翻译：三氯甲烷基取代苯的制备方法
公开(公告)号：US20160152533A1
公开(公告)日：2016-06-02
申请号：US14905775
申请日：2014-09-12
申请人： SHANGHAI FANGLUN NEW MATERIAL TECHNOLOGY CO., LTD.
发明人： Nongyue WANG , Xiongwei QU , Guohua LI , Quanzhong ZHAO , Jianming SHAO , Guoqiang WEN
IPC分类号： C07C17/08
CPC分类号： C07C17/08 , C07C17/093 , C07C17/12 , C07C17/14 , C07C17/383 , C07C51/60 , C07C25/125 , C07C53/44 , C07C22/04 , C07C22/06
摘要： The present application relates to a method for photochlorination, and specifically to photochlorination by a photochemical reaction of an aromatic compound with gaseous chlorine so as to prepare a trichloromethyl-substituted benzene, and to a method using bis-(trichloromethyl)-benzene as the trichloromethyl-substituted benzene to prepare by further reaction bis-(chloroformyl)-benzene. Through the control of temperature, illuminance and consumption of gaseous chlorine, the method of this application can greatly improve the purity of trichloromethyl-substituted benzene and further prepare polymer-grade bis-(chloroformyl)-benzene with low cost. The present application also relates to a method for purifying trichloromethyl-substituted benzene, and specifically to a method for purifying trichloromethyl-substituted benzene via molecular distillation. The present application further relates to a photochlorination reactor for use in photochlorination reactions (such as those of the present application).
摘要翻译：本申请涉及一种光氯化方法，具体涉及通过芳族化合物与气态氯的光化学反应进行光氯化，以制备三氯甲基取代的苯，以及使用双（三氯甲基） - 苯作为三氯甲基的方法通过进一步反应双 - （氯甲酰基） - 苯制备。通过控制气态氯的温度，照度和消耗量，本方法可以大大提高三氯甲基取代苯的纯度，进一步制备聚合物级双（氯甲酰基） - 苯，成本低廉。本申请还涉及三氯甲基取代的苯的纯化方法，特别涉及通过分子蒸馏纯化三氯甲基取代的苯的方法。本申请还涉及用于光氯化反应的光氯化反应器（例如本申请的那些）。

7. 发明授权

US09238609B2 Dicarboxylic acid monomers and methods of making and using the same 有权
标题翻译：二羧酸单体及其制备和使用方法
公开(公告)号：US09238609B2
公开(公告)日：2016-01-19
申请号：US14286024
申请日：2014-05-23
申请人： SABIC Global Technologies B.V.
发明人： Navinchandra Asthana , Kiran Arunkumar Puthamane , Shantaram Narayan Naik , Minor Senthil Kumar , Venkata Ramanarayanan Ganapathy Bhotla , Vinodkumar Vasudevan , Edward J. Nesakumar , Girish Chandra , Ruud van der Heijden , Jan Henk Kamps , Elena Uliyanchenko , Robert R. Gallucci
IPC分类号： C07C51/265 , C08G63/199 , C08G63/64 , C07C2/72 , C07C5/367 , C07C1/30 , C07C1/207 , C08K5/09
CPC分类号： C07C51/265 , C07C1/207 , C07C1/2076 , C07C1/24 , C07C1/30 , C07C1/326 , C07C2/42 , C07C2/72 , C07C5/367 , C07C17/14 , C07C51/43 , C07C2527/054 , C07C2531/10 , C07C2602/08 , C08G63/185 , C08G63/199 , C08G63/64 , C07C13/465 , C07C57/15 , C07C22/04 , C07C15/44
摘要： Disclosed herein are phenylindane dicarboxylic acid (PIDA) monomers, polymer compositions comprising the PIDA monomers, and methods of preparing PIDA monomers. This abstract is intended as a scanning tool for purposes of searching in the particular art and is not intended to be limiting of the present disclosure.
摘要翻译：本文公开了苯基二茚基二羧酸（PIDA）单体，包含PIDA单体的聚合物组合物和制备PIDA单体的方法。该摘要旨在作为用于在特定技术中进行搜索的扫描工具，并不旨在限制本公开。

8. 发明授权

US09115043B2 Process for the preparation of benzonorbornenes 有权
标题翻译：制备苯并降冰片烯的方法
公开(公告)号：US09115043B2
公开(公告)日：2015-08-25
申请号：US13126380
申请日：2009-09-28
申请人： Denis Gribkov , Bjorn Antelmann , Fanny Giordano , Harald Walter , Alain De Mesmaeker
发明人： Denis Gribkov , Bjorn Antelmann , Fanny Giordano , Harald Walter , Alain De Mesmaeker
IPC分类号： C07C211/45 , C07C17/32 , C07C17/23 , C07C17/26 , C07C17/266 , C07C22/02 , C07C201/12 , C07C205/11 , C07C209/36 , C07C205/12
CPC分类号： C07C17/32 , C07C17/23 , C07C17/26 , C07C17/266 , C07C22/02 , C07C22/04 , C07C201/12 , C07C205/06 , C07C205/11 , C07C205/12 , C07C209/365 , C07C2601/10 , C07C2603/66 , C07C211/61
摘要： The present invention relates to a novel a process for the preparation of 9-dichloromethylene-1,2,3,4-tetrahydro-1,4-methano-naphthalen-5-ylamine which process comprises a) reacting cyclopentadiene in the presence of a radical initiator and CXCI3, wherein X is chloro or bromo, to a compound of formula I1, or aa) reacting cyclopentadiene with CXCI3, wherein X is chloro, in the presence of a metal catalyst to a compound of formula I1, wherein X is chloro, b) reacting the compound of formula I1 with a base in the presence of an appropriate solvent to the compound of formula III, c) and converting the compound of formula III in the presence of 1,2-dehydro-6-nitrobenzene to the compound of formula IV, and d) hydrogenating the compound of formula IV in the presence of a metal catalyst.
摘要翻译：本发明涉及一种制备9-二氯亚甲基-1,2,3,4-四氢-1,4-亚甲基 - 萘-5-基胺的新方法，该方法包括：a）使环戊二烯在自由基引发剂和其中X是氯或溴的CXCl 3，或aa）在金属催化剂存在下将环戊二烯与CXCl 3（其中X是氯）在式I化合物中反应，其中X是氯 b）使式I1化合物与碱在适当的溶剂存在下反应，得到式III化合物，c）并在1,2-脱氢-6-硝基苯存在下将式III化合物转化为式Ⅳ化合物，和d）在金属催化剂存在下氢化式Ⅳ化合物。

9. 发明授权

US08962898B2 Optically active ammonium salt compound, production intermediate thereof, and production method thereof 有权
标题翻译：光学活性铵盐化合物及其制备方法及其制备方法
公开(公告)号：US08962898B2
公开(公告)日：2015-02-24
申请号：US13705506
申请日：2012-12-05
申请人： Nippon Soda Co., Ltd.
发明人： Keiji Maruoka , Yasushi Kubota
IPC分类号： C07C25/18 , B01J31/02 , C07B53/00 , C07C22/04 , C07C33/46 , C07C43/225 , C07D223/18 , C07D487/10
CPC分类号： B01J31/0271 , C07B53/00 , C07B2200/07 , C07C22/04 , C07C25/18 , C07C33/46 , C07C43/225 , C07D223/18 , C07D487/10
摘要： An optically active bisbenzyl compound or a racemic bisbenzyl compound represented by formula (2) that has axial chirality: where: R1 represents a halogen, or an optionally substituted: linear, branched, or cyclic C1-8 alkyl, C2-8 alkenyl, C2-8 alkynyl, C6-14 aryl, C3-8 heteroaryl, linear, branched, or cyclic C1-8 alkoxy, or C7-16 aralkyl; R21 each independently represents hydrogen, halogen, nitro, or an optionally substituted: linear, branched, or cyclic C1-8 alkyl, C2-8 alkenyl, C2-8 alkynyl, C6-14 aryl, linear, branched, or cyclic C1-8 alkoxy, or a C7-16 aralkyl; R3 represents hydrogen, or an optionally substituted: C6-14 aryl, a C3-8 heteroaryl, or a C7-16 aralkyl; and Y2 represents a halogen, or an optionally substituted: C1-8 alkylsulfonyloxy, C6-14 arylsulfonyloxy, or C7-16 aralkylsulfonyloxy.
摘要翻译：具有轴向手性的光学活性双苄基化合物或由式（2）表示的外消旋双苄基化合物：其中：R1表示卤素或任选取代的直链，支链或环状C 1-8烷基，C 2-8烯基，C 2 -8炔基，C 6-14芳基，C 3-8杂芳基，直链，支链或环状C 1-8烷氧基或C7-16芳烷基; R 21各自独立地表示氢，卤素，硝基或任选取代的直链，支链或环状C 1-8烷基，C 2-8烯基，C 2-8炔基，C 6-14芳基，直链，支链或环状C 1-8 烷氧基或C7-16芳烷基; R 3表示氢，或任选取代的：C 6-14芳基，C 3-8杂芳基或C 7-16芳烷基; 并且Y2表示卤素或任选取代的C 1-8烷基磺酰氧基，C 6-14芳基磺酰氧基或C 7-16芳烷基磺酰氧基。

10. 发明申请

US20150018578A1 PROCESS FOR PREPARATION OF FINGOLIMOD 有权
标题翻译：制备FINGOLIMOD的方法
公开(公告)号：US20150018578A1
公开(公告)日：2015-01-15
申请号：US14373214
申请日：2013-01-17
申请人： Milind Gharpure , Krishna Narawade , Prem Chand , Shekhar Bhirud
发明人： Milind Gharpure , Krishna Narawade , Prem Chand , Shekhar Bhirud
IPC分类号： C07C209/78 , C07C215/10 , C07C45/30 , C07C209/16 , C07C29/14
CPC分类号： C07C209/78 , C07C17/16 , C07C29/00 , C07C29/14 , C07C45/30 , C07C45/64 , C07C67/293 , C07C209/16 , C07C213/08 , C07C215/10 , C07C215/28 , C07C231/12 , C07C303/28 , C07C309/66 , C07C233/47 , C07C22/04 , C07C69/157 , C07C49/82 , C07C33/20
摘要： The present invention provides a process for preparation of fingolimod, a compound of Formula I or a pharmaceutically acceptable salt thereof, free of regioisomeric impurity compound of Formula IA
摘要翻译：本发明提供了一种制备芬戈莫德，式I化合物或其药学上可接受的盐的方法，其不含式IA的区域异构体杂质化合物

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